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1. 发明申请

US20120330035A1 HYDROTHERMOLYSIS OF MONO- AND/OR OLIGOSACCHARIDES IN THE PRESENCE OF A POLYALKYLENE GLYCOL ETHER 审中-公开
标题翻译：在聚乙烯甘油醚存在下单糖和/或低聚糖的水解
公开(公告)号：US20120330035A1
公开(公告)日：2012-12-27
申请号：US13530890
申请日：2012-06-22
申请人： Alois Kindler , Andrea Schmidt , Alwin Rehfinger , Peter Bassler , Ralf Böhling
发明人： Alois Kindler , Andrea Schmidt , Alwin Rehfinger , Peter Bassler , Ralf Böhling
IPC分类号： C07D319/12 , C07D307/48 , B01J19/00
CPC分类号： B01J19/0093 , B01J2219/00792 , B01J2219/00822 , B01J2219/00824 , B01J2219/00831 , B01J2219/00833 , B01J2219/00869 , B01J2219/00873 , B01J2219/00889
摘要： The present invention relates to a method for the hydrothermolysis of a mono- and/or oligosaccharide-comprising composition which in addition comprises at least one monoalkyl and/or dialkyl ether of a polyalkylene glycol, and also relates to a hydrothermolysis device.
摘要翻译：本发明涉及一种含有单糖和/或寡糖的组合物的水热解方法，该组合物还包含至少一种聚亚烷基二醇的单烷基和/或二烷基醚，还涉及一种水热解装置。

2. 发明申请

US20120197038A1 PROCESS FOR PREPARING ISOCYANATES 失效
标题翻译：制备异氰酸酯的方法
公开(公告)号：US20120197038A1
公开(公告)日：2012-08-02
申请号：US13442401
申请日：2012-04-09
申请人： Ralf Böhling , Sven Küber , Stefan Maixner , Eckhard Stroefer , Jochem Henkelmann , Georg Krug , Werner Bolz
发明人： Ralf Böhling , Sven Küber , Stefan Maixner , Eckhard Stroefer , Jochem Henkelmann , Georg Krug , Werner Bolz
IPC分类号： C07C263/10
CPC分类号： C07C263/10 , B01J2219/00038 , B01J2219/00869 , C07C2601/14 , C07C265/14
摘要： Process for preparing isocyanates by phosgenation of amines, wherein phosgene and amine are brought into contact in at least 2 mixing chambers connected in parallel.
摘要翻译：通过胺的光气化制备异氰酸酯的方法，其中光气和胺在至少两个并联连接的混合室中接触。

3. 发明授权

US07351860B2 Method and device for producing formic acid formates and use of said formates 失效
标题翻译：用于生产甲酸甲酸盐和所述甲酸盐的使用的方法和装置
公开(公告)号：US07351860B2
公开(公告)日：2008-04-01
申请号：US10524268
申请日：2003-07-30
申请人： Christoph Adami , Jörn Karl , Alexander Hauk , Ralf Böhling , Jörg Pastre , Robert Lenz
发明人： Christoph Adami , Jörn Karl , Alexander Hauk , Ralf Böhling , Jörg Pastre , Robert Lenz
IPC分类号： C07C53/00
CPC分类号： C07C51/412 , C07C53/06
摘要： The invention relates to a method for producing formic acid formates, whereby (a) formic acid methyl ester is partially hydrolysed with water; (b) formic acid methyl ester and methanol are separated by distillation from the reaction mixture obtained in step (a), forming a current containing formic acid and water; (c) the current obtained in step (b), containing the formic acid methyl ester and optionally methanol, is converted into a current containing formate and water, by (i) reaction with a basic compound having a pKa value of the corresponding acid of the corresponding dissociation step of =3, measured at 25° C. in an aqueous solution, in presence of water, and (ii) separation by distillation of the methanol; and (d) the current obtained in step (b), containing formic acid and water, and the current obtained in step (c), containing formate and water, are combined to form a mixture containing the formic acid formate and water. The invention also relates to a device for producing said formic acid formates and to the use of the same.
摘要翻译：本发明涉及甲酸甲酸盐的制备方法，其中（a）甲酸甲酯用水部分水解; （b）甲酸甲酯和甲醇通过蒸馏从步骤（a）中获得的反应混合物分离，形成含有甲酸和水的电流; （c）将含有甲酸甲酯和任选的甲醇的步骤（b）中获得的电流转化成含有甲酸盐和水的电流，通过（i）与具有pK aa的碱性化合物反应，在水溶液中，在水的存在下，在25℃下测定相应解离步骤的相应酸的相应值，和（ii）通过蒸馏甲醇分离; 和（d）将包含甲酸和水的步骤（b）中得到的电流和步骤（c）中得到的含有甲酸盐和水的电流合并形成含有甲酸甲酸盐和水的混合物。本发明还涉及用于生产所述甲酸甲酸盐的装置及其用途。

4. 发明申请

US20110003074A1 METHOD FOR THE PRODUCTION OF IRON-DOPED CARBONS 审中-公开
标题翻译：生产碳化硅的方法
公开(公告)号：US20110003074A1
公开(公告)日：2011-01-06
申请号：US12919745
申请日：2009-02-26
申请人： Ralf Böhling , Jörg Pastre , Katrin Freitag
发明人： Ralf Böhling , Jörg Pastre , Katrin Freitag
IPC分类号： B05D5/00
CPC分类号： B01J20/20 , B01J21/18 , B01J23/745 , B01J35/1028 , B01J37/0238 , B09C1/002 , C01B32/354 , C01P2006/12 , C02F1/283 , C02F1/288 , C02F1/705 , C02F2103/06 , C23C14/22 , C23C14/228
摘要： A process for the preparation of a metal-doped support material. The metal-doped support material comprises at least one metal in elemental form on at least one support material which is based on carbon by gas-phase deposition of at least one compound comprising the at least one metal in the oxidation state 0 in combination with carbon monoxide on the at least one support material and thermal decomposition of the at least one compound comprising the at least one metal in the oxidation state 0 in order to obtain the at least one metal in elemental form. During and after the deposition and the decomposition, the support material is not brought into contact with reducing compounds during the preparation.
摘要翻译：一种制备掺杂金属的载体材料的方法。金属掺杂的载体材料在至少一种载体材料上包含至少一种元素形式的金属，所述至少一种载体材料基于碳，通过气相沉积至少一种包含至少一种处于氧化态的金属0的化合物与碳的组合至少一种载体材料上的一氧化物和包含至少一种处于氧化态0的金属的至少一种化合物的热分解，以获得至少一种元素形式的金属。在沉积和分解期间和之后，在制备过程中，载体材料不与还原化合物接触。

5. 发明授权

US07161039B2 Method and device for producing ethylamine and butylamine 失效
标题翻译：制备乙胺和丁胺的方法和装置
公开(公告)号：US07161039B2
公开(公告)日：2007-01-09
申请号：US10495278
申请日：2002-11-12
申请人： Ulrich Steinbrenner , Frank Funke , Ralf Böhling
发明人： Ulrich Steinbrenner , Frank Funke , Ralf Böhling
IPC分类号： C07C209/60
CPC分类号： C07C211/07 , C07C211/04 , C07C211/08 , Y02P20/582
摘要： A process for preparing ethylamines, butylamines and mixed ethyl/butylamines comprising the following steps: (i) Hydroamination of butadiene and ethylene by means of a monoalkylamine and/or a dialkylamine in which alkyl=ethyl and/or butyl in the presence of an alkali metal amide as catalyst, (ii) isomerization of the amines obtained in the hydroamination (i), if appropriate under the following conditions: (iia) prior fractionation into particular fractions and/or (iib) isomerization under hydrogenating conditions and/or (iic) isomerization in the presence of ammonia, (iii) fractionation of the resulting product mixture with isolation of the desired product amines and recycle of the amines suitable as starting material to step (i).
摘要翻译：一种制备乙胺，丁胺和混合乙基/丁胺的方法，包括以下步骤：（i）通过单烷基胺和/或二烷基胺（其中烷基=乙基和/或丁基）在碱存在下水解丁二烯和乙烯金属酰胺作为催化剂，（ii）在以下条件下适当时在水解（i）中获得的胺异构化：（iia）先前分馏成特定馏分和/或（iib）在氢化条件下的异构化和/或）在氨的存在下异构化，（iii）分离所得产物混合物，分离所需产物胺并适合作为步骤（i）的起始原料的胺的再循环。

6. 发明授权

US06492558B2 Preparation of n-butylamines 失效
标题翻译：正丁胺的制备
公开(公告)号：US06492558B2
公开(公告)日：2002-12-10
申请号：US10025539
申请日：2001-12-26
申请人： Frank Funke , Ulrich Steinbrenner , Peter Zehner , Ralf Böhling , Wolfgang Harder
发明人： Frank Funke , Ulrich Steinbrenner , Peter Zehner , Ralf Böhling , Wolfgang Harder
IPC分类号： C07C20960
CPC分类号： C07C209/70 , C07C209/60 , C07C211/02 , C07C211/09 , C07C211/07
摘要： Process for the preparation of n-butylamines where n-butenylamines are firstly prepared by reacting 1,3-butadiene in the form of a 1,3-butadiene containing mixture obtained during the cracking of petroleum fractions or during the dehydrogenation of LPG or LNG or from GTL technology with a primary amine and/or a secondary amine under hydroaminating conditions, and the resulting butenylamine(s) are then reacted in a second process stage under hydrogenating and transalkylating conditions.
摘要翻译：正丁胺的制备方法，其中首先通过在石油馏分裂化期间或在LPG或LNG的脱氢期间获得的1,3-丁二烯混合物形式的1,3-丁二烯反应制备正丁烯基胺，或在氢化条件下从具有伯胺和/或仲胺的GTL技术中获得的丁烯基胺在第二工艺阶段在氢化和烷基转移条件下反应。

7. 发明授权

US06350911B1 Method for producing amines 有权
标题翻译：胺的制备方法
公开(公告)号：US06350911B1
公开(公告)日：2002-02-26
申请号：US09857903
申请日：2001-06-11
申请人： Michael Sander , Ulrich Penzel , Hans Volkmar Schwarz , Eckhard Ströfer , Dieter Stützer , Jörn Müller , Markus Maurer , Peter Zehner , Ekkehard Schwab , Ralf Böhling , Dominic Vanoppen
发明人： Michael Sander , Ulrich Penzel , Hans Volkmar Schwarz , Eckhard Ströfer , Dieter Stützer , Jörn Müller , Markus Maurer , Peter Zehner , Ekkehard Schwab , Ralf Böhling , Dominic Vanoppen
IPC分类号： C07C21100
CPC分类号： C07C209/36 , B01J4/002 , B01J10/002 , B01J19/006 , B01J19/246 , B01J19/2465 , B01J19/2475 , B01J2219/00078 , B01J2219/00081 , B01J2219/00085 , B01J2219/00094 , B01J2219/00777 , C07C211/51
摘要： The invention relates to a process for the preparation of amines by hydrogenation of nitro compounds, which comprises carrying out the hydrogenation in a vertical reactor whose length is greater than its diameter, having a downward-facing jet nozzle arranged in the upper region of the reactor through which the starting materials and the reaction mixture are fed in, and having an outlet at any desired point of the reactor, through which the reaction mixture is fed back to the jet nozzle in an external circuit by means of a conveying means, and having flow reversal in the lower region of the reactor.
摘要翻译：本发明涉及一种通过氢化硝基化合物制备胺的方法，其包括在其长度大于其直径的立式反应器中进行氢化，其具有布置在反应器的上部区域中的面向下的喷嘴原料和反应混合物通过该反应混合物进料，并在反应器的任何所需点处具有出口，反应混合物通过该反应混合物通过输送装置在外部回路中被反馈到喷嘴，并具有在反应器的下部区域的流动反转。

8. 发明申请

US20110182798A1 SINGLE-CHAMBER VAPORIZER AND USE THEREOF IN CHEMICAL SYNTHESIS 有权
标题翻译：单室蒸发器及其在化学合成中的应用
公开(公告)号：US20110182798A1
公开(公告)日：2011-07-28
申请号：US13011315
申请日：2011-01-21
申请人： Ralf Böhling , Michael Schipper , Stefan Birnbach , Peter Petersen , Achim Gritsch , Alois Wellisch , Hermann Luyken , Albert Steiner , Peter Zehner
发明人： Ralf Böhling , Michael Schipper , Stefan Birnbach , Peter Petersen , Achim Gritsch , Alois Wellisch , Hermann Luyken , Albert Steiner , Peter Zehner
IPC分类号： C01C3/02 , F22B33/00
CPC分类号： C01C3/0204 , F01K23/064 , F22B27/00 , F22B33/00
摘要： The invention relates to an improved process for vaporizing organic compounds and the further conversion thereof.
摘要翻译：本发明涉及一种汽化有机化合物的改进方法及其进一步转化。

9. 发明申请

US20090203874A1 METHOD FOR PRODUCING POLYETHER POLYOLS 失效
标题翻译：生产聚醚多元醇的方法
公开(公告)号：US20090203874A1
公开(公告)日：2009-08-13
申请号：US12302162
申请日：2007-05-22
申请人： Achim Löffler , Wolfgang Loth , Ralf Böhling , Thomas Ostrowski , Michael Stösser , Hartwig Voss , Axel Schimpf
发明人： Achim Löffler , Wolfgang Loth , Ralf Böhling , Thomas Ostrowski , Michael Stösser , Hartwig Voss , Axel Schimpf
IPC分类号： C08G65/02 , C08G65/28
CPC分类号： C08G65/2696 , C08G18/4866
摘要： A process for preparing polyether polyols by reaction of the following starting materials: a) one or more alkylene oxides and, if appropriate, carbon dioxide and also b) one or more H-functional starter substances, in the presence of a catalyst, in a reaction unit having a plurality of parallel layers A, B which are microstructured so that each layer has a multiplicity of channels which are arranged parallel to one another and form a continuous flow path from one side of the plate to the opposite side of this, wherein a distribution device for introduction of the starting materials and the catalyst is provided at one end of the channels of the layers A and a collection device for the reaction mixture is provided at the other end of these is proposed.
摘要翻译：一种通过以下原料反应制备聚醚多元醇的方法：a）一种或多种环氧烷烃，如果合适的话，二氧化碳，以及b）一种或多种H官能起始物质，在催化剂存在下，在反应单元具有多个平行层A，B，它们被微结构化，使得每个层具有多个彼此平行布置的通道，并形成从板的一侧到其相反侧的连续流动路径，其中在层A的通道的一端设置用于引入起始材料和催化剂的分配装置，并且在另一端提供了用于反应混合物的收集装置。

10. 发明授权

US07323593B2 Method and device for producing formates and the use thereof 失效
标题翻译：用于生产甲酸盐的方法和装置及其用途
公开(公告)号：US07323593B2
公开(公告)日：2008-01-29
申请号：US10524202
申请日：2003-07-30
申请人： Christoph Adami , Jörn Karl , Alexander Hauk , Ralf Böhling , Jörg Pastre , Robert Lenz
发明人： Christoph Adami , Jörn Karl , Alexander Hauk , Ralf Böhling , Jörg Pastre , Robert Lenz
IPC分类号： C07C53/00
CPC分类号： C07C51/43 , C07C51/09 , C07C51/44 , C07C53/02 , C07C53/06
摘要： A process for preparing acid formates which comprises (a) partially hydrolyzing methyl formates with water; (b) separating off by distillation methyl formate and methanol from the reaction mixture obtained in process stage (a), forming a stream comprising formic acid and water; and (c) combining the stream comprising formic acid and water from the process stage (b) and the corresponding formate, forming a mixture comprising the acid formate and water, an apparatus for their preparation and their use.
摘要翻译：一种制备酸甲酯的方法，其包括（a）用水部分水解甲酸甲酯; （b）通过蒸馏甲酸甲酯和甲醇从工艺阶段（a）中获得的反应混合物分离，形成包含甲酸和水的流; 和（c）将来自加工阶段（b）的甲酸和水的流与相应的甲酸酯混合，形成含有甲酸和水的混合物，其制备及其用途的装置。

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