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1. 发明申请

US20090203874A1 METHOD FOR PRODUCING POLYETHER POLYOLS 失效
标题翻译：生产聚醚多元醇的方法
公开(公告)号：US20090203874A1
公开(公告)日：2009-08-13
申请号：US12302162
申请日：2007-05-22
申请人： Achim Löffler , Wolfgang Loth , Ralf Böhling , Thomas Ostrowski , Michael Stösser , Hartwig Voss , Axel Schimpf
发明人： Achim Löffler , Wolfgang Loth , Ralf Böhling , Thomas Ostrowski , Michael Stösser , Hartwig Voss , Axel Schimpf
IPC分类号： C08G65/02 , C08G65/28
CPC分类号： C08G65/2696 , C08G18/4866
摘要： A process for preparing polyether polyols by reaction of the following starting materials: a) one or more alkylene oxides and, if appropriate, carbon dioxide and also b) one or more H-functional starter substances, in the presence of a catalyst, in a reaction unit having a plurality of parallel layers A, B which are microstructured so that each layer has a multiplicity of channels which are arranged parallel to one another and form a continuous flow path from one side of the plate to the opposite side of this, wherein a distribution device for introduction of the starting materials and the catalyst is provided at one end of the channels of the layers A and a collection device for the reaction mixture is provided at the other end of these is proposed.
摘要翻译：一种通过以下原料反应制备聚醚多元醇的方法：a）一种或多种环氧烷烃，如果合适的话，二氧化碳，以及b）一种或多种H官能起始物质，在催化剂存在下，在反应单元具有多个平行层A，B，它们被微结构化，使得每个层具有多个彼此平行布置的通道，并形成从板的一侧到其相反侧的连续流动路径，其中在层A的通道的一端设置用于引入起始材料和催化剂的分配装置，并且在另一端提供了用于反应混合物的收集装置。

2. 发明授权

US08034980B2 Method for producing polyether polyols 失效
标题翻译：聚醚多元醇的制备方法
公开(公告)号：US08034980B2
公开(公告)日：2011-10-11
申请号：US12302162
申请日：2007-05-22
申请人： Achim Loeffler , Wolfgang Loth , Ralf Boehling , Thomas Ostrowski , Michael Stoesser , Hartwig Voss , Axel Schimpf
发明人： Achim Loeffler , Wolfgang Loth , Ralf Boehling , Thomas Ostrowski , Michael Stoesser , Hartwig Voss , Axel Schimpf
IPC分类号： C07C43/00 , B01J19/00
CPC分类号： C08G65/2696 , C08G18/4866
摘要： A process for preparing polyether polyols by reaction of the following starting materials: a) one or more alkylene oxides and, if appropriate, carbon dioxide and also b) one or more H-functional starter substances, in the presence of a catalyst, in a reaction unit having a plurality of parallel layers A, B which are microstructured so that each layer has a multiplicity of channels which are arranged parallel to one another and form a continuous flow path from one side of the plate to the opposite side of this, wherein a distribution device for introduction of the starting materials and the catalyst is provided at one end of the channels of the layers A and a collection device for the reaction mixture is provided at the other end of these is proposed.
摘要翻译：通过以下原料反应制备聚醚多元醇的方法：a）一种或多种环氧烷烃，如果合适的话，二氧化碳，以及b）一种或多种H官能起始物质，在催化剂存在下，在反应单元具有多个平行层A，B，它们被微结构化，使得每个层具有多个彼此平行布置的通道，并形成从板的一侧到其相反侧的连续流动路径，其中在层A的通道的一端设置用于引入起始材料和催化剂的分配装置，并且在另一端提供了用于反应混合物的收集装置。

3. 发明申请

US20130023700A1 PROCESS FOR A CONTINUOUS PRODUCTION OF POLYETHEROLS 有权
标题翻译：连续生产聚醚的方法
公开(公告)号：US20130023700A1
公开(公告)日：2013-01-24
申请号：US13551936
申请日：2012-07-18
申请人： Vinit Chilekar , Oliver Bey , Andreas Brodhagen , Achim Löffler , Fatemeh Ahmadnian , Ralf Böhling , Christoph Grossmann , Ulrich Kammel , Ronald Adelmann , Thomas Ostrowski , Milind Joshi , Gerrit Waters , Dirk Meckelnburg
发明人： Vinit Chilekar , Oliver Bey , Andreas Brodhagen , Achim Löffler , Fatemeh Ahmadnian , Ralf Böhling , Christoph Grossmann , Ulrich Kammel , Ronald Adelmann , Thomas Ostrowski , Milind Joshi , Gerrit Waters , Dirk Meckelnburg
IPC分类号： C07C41/02
CPC分类号： C07C41/03 , B01J4/004 , B01J19/248 , B01J2219/00768 , B01J2219/182 , B01J2219/1943 , C08G65/2609 , C08G65/2696 , C07C43/11
摘要： A process for a continuous production of a polyetherol first involves reacting an alcohol with a starter or an alkoxylated precursor, to give a mixture comprising an alcoholate and water. Water is then removed from the mixture. The process further involves feeding the alcoholate into a bubble column and feeding an alkylene oxide into the bottom of a compartment of the bubble column, such that the alkylene oxide rises in the alcoholate. The alkylene oxide then reacts with the alcoholate or a secondary product from the reaction between the alcoholate and alkylene oxide, to give the polyetherol.
摘要翻译：首先连续生产聚乙二醇的方法包括使醇与起始物或烷氧基化前体反应，得到包含醇化物和水的混合物。然后从混合物中取出水。该方法进一步包括将醇化物进料到气泡塔中并将环氧烷进料到泡罩塔的隔室的底部，使得烯化氧在醇化物中上升。然后烯化氧与醇化物或醇化物和环氧烷之间的反应产生的次生物反应，得到聚醚。

4. 发明授权

US08399608B2 Process for the preparation of polyether alcohols from unsaturated starters having active hydrogen atoms 有权
标题翻译：从具有活性氢原子的不饱和起始物制备聚醚醇的方法
公开(公告)号：US08399608B2
公开(公告)日：2013-03-19
申请号：US12681789
申请日：2007-10-25
申请人： Georg Heinrich Grosch , Matthias Zipplies , Thomas Ostrowski , Ulrich Annen , Markus Klumpe
发明人： Georg Heinrich Grosch , Matthias Zipplies , Thomas Ostrowski , Ulrich Annen , Markus Klumpe
IPC分类号： C08G65/10 , C08G65/30 , C08G65/34 , C08F8/06 , C08F6/08
CPC分类号： C08G65/2609 , C08G65/2648 , C08G65/2696
摘要： A process for the preparation of polyether alcohols by reacting at least one alkylene oxide with at least one unsaturated starter having at least one active hydrogen atom per molecule under basic catalysis, that the alkoxylation is carried out in at least two stages, in stage (I) the alkoxylation of the starter or starters being carried out with not more than 10 mol of alkylene oxide per mole of starter with a catalyst concentration of not more than 0.0085 mol of basic catalyst per mole and in stage (II) and the optionally following stages, the alkoxylated starter or starters from stage (I) being reacted with further alkylene oxide at a catalyst concentration of at least 0.01 mol of basic catalyst per mole of starter.
摘要翻译：通过在碱性催化下使至少一种烯化氧与至少一种具有至少一个活性氢原子的不饱和起始物在每个分子中反应来制备聚醚醇的方法，该烷氧基化在至少两个阶段中在阶段（I ）起始物或起动器的烷氧基化作用，每摩尔起始物不超过10摩尔环氧烷烃，每摩尔催化剂浓度不大于0.0085摩尔碱性催化剂和（II）阶段和任选的后续阶段，来自阶段（I）的烷氧基化起始物或起始物与另外的烯化氧反应，每摩尔起始物的催化剂浓度为至少0.01摩尔碱性催化剂。

5. 发明申请

US20120130134A1 PROCESS FOR THE PREPARATION OF POLYETHEROLS FROM ALKYLENE OXIDES 审中-公开
标题翻译：从亚烷基氧化物制备聚醚的方法
公开(公告)号：US20120130134A1
公开(公告)日：2012-05-24
申请号：US13387540
申请日：2010-07-27
申请人： Matthias Schopohl , Thomas Ostrowski , Dirk Meckelnburg , Renata Jovanovic , Achim Loeffler , Hans-Juergen Pallasch , Thorsten Friese , Eckard Schauss , Susanne Szeschkus , Vinit Chilekar , Hans Volkmar Schwarz
发明人： Matthias Schopohl , Thomas Ostrowski , Dirk Meckelnburg , Renata Jovanovic , Achim Loeffler , Hans-Juergen Pallasch , Thorsten Friese , Eckard Schauss , Susanne Szeschkus , Vinit Chilekar , Hans Volkmar Schwarz
IPC分类号： C07C29/04
CPC分类号： C08G65/2696 , C08G65/2663 , C08G65/30
摘要： A process for the preparation of polyetherols, comprising the following steps: a) reaction of at least one starter compound with at least one alkylene oxide and a catalyst to give a crude polyetherol and b) removal of low molecular weight byproducts from the crude polyetherol from step a), wherein the crude polyetherol is treated with a stripping gas in a column having internals.
摘要翻译：一种制备聚醚的方法，包括以下步骤：a）将至少一种起始化合物与至少一种烯化氧和催化剂反应，得到粗的聚乙烯醇，和b）从粗制的聚醚中除去低分子量副产物步骤a），其中在具有内部材料的塔中用脱气处理粗制聚醚。

6. 发明申请

US20060223979A1 Process for preparing polyether polyols 审中-公开
标题翻译：制备聚醚多元醇的方法
公开(公告)号：US20060223979A1
公开(公告)日：2006-10-05
申请号：US11098271
申请日：2005-04-04
申请人： Thomas Ostrowski , Raimund Ruppel , Eva Baum
发明人： Thomas Ostrowski , Raimund Ruppel , Eva Baum
IPC分类号： C08G65/34 , C08L71/08
CPC分类号： C08G65/2663
摘要： A process for preparing polyether polyols comprises A) preparing a polyether polyol precursor, B) preparing a suspension of a DMC catalyst in a polyol, C) activating the DMC catalyst by bringing it into contact with an alkylene oxide, giving an activated DMC catalyst suspension, D) adding the activated DMC catalyst suspension from step C) to the polyether polyol precursor, E) reacting the polyether polyol precursor with alkylene oxide and, if appropriate, an H-functional starter substance in the presence of the activated DMC catalyst.
摘要翻译：制备聚醚多元醇的方法包括：A）制备聚醚多元醇前体，B）制备DMC催化剂在多元醇中的悬浮液，C）通过使其与烯化氧接触来活化DMC催化剂，得到活化的DMC催化剂悬浮液 D）将来自步骤C）的活化DMC催化剂悬浮液加入到聚醚多元醇前体中，E）使聚醚多元醇前体与烯化氧反应，如果合适的话，在活化的DMC催化剂存在下使其反应。

7. 发明申请

US20050107643A1 Preparation of polyether alcohols 审中-公开
标题翻译：聚醚醇的制备
公开(公告)号：US20050107643A1
公开(公告)日：2005-05-19
申请号：US10712707
申请日：2003-11-13
申请人： Thomas Ostrowski , Raimund Ruppel , Eva Baum , Kathrin Harre
发明人： Thomas Ostrowski , Raimund Ruppel , Eva Baum , Kathrin Harre
IPC分类号： C07C43/11 , C08G65/00 , C08G65/10 , C08G65/12 , C08G65/26
CPC分类号： C08G65/2663 , C08G18/4866 , C08G65/2696
摘要： The invention relates to a process for the continuous preparation of polyether alcohols by reaction of alkylene oxides with H-functional starter substances in the presence of DMC catalysts, which comprises, at the beginning of the process a) firstly placing initial charge material and DMC catalyst in a reactor, b) metering in alkylene oxide so that the metering rate which is maintained for continuous operation of the reactor is reached in a time of from 100 to 3 000 seconds, c) metering in starter substance during or after step b) so that the metering rate which is maintained for continuous operation of the reactor is reached in a time of from 5 to 500 seconds, d) after the fill level in the reactor which is desired for continuous operation of the reactor has been reached, taking product off continuously from the reactor while at the same time metering in starter substance and alkylene oxides in such an amount that the fill level in the reactor remains constant and metering in DMC catalyst so that the catalyst concentration necessary for continuous operation of the reactor is maintained in the reactor.
摘要翻译：本发明涉及一种通过在DMC催化剂存在下使烯化氧与H官能起始物质反应来连续制备聚醚醇的方法，该方法在方法开始时包括：a）首先将初始的电荷材料和DMC催化剂在反应器中，b）在环氧烷中计量，使得在100至3000秒的时间内达到维持反应器连续操作的计量速率，c）在步骤b）或之后计量起始物质在5至500秒的时间内达到维持反应器连续运行的计量速率，d）在达到反应器连续运行所需反应器的填充量后，将产品关闭连续地从反应器中同时在起始物质和环氧烷中计量，使得反应器中的填充水平保持恒定并且在DMC cata中计量使得在反应器中保持连续操作反应器所需的催化剂浓度。

8. 发明授权

US06806393B2 Multimetal cyanide compounds, their preparation and their use 失效
标题翻译：多金属氰化合物，其制备及其用途
公开(公告)号：US06806393B2
公开(公告)日：2004-10-19
申请号：US10447521
申请日：2003-05-29
申请人： Georg Heinrich Grosch , Kathrin Harre , Jörg Erbes , Reinhard Lorenz , Stephan Bauer , Thomas Ostrowski , Eva Baum , Dieter Junge
发明人： Georg Heinrich Grosch , Kathrin Harre , Jörg Erbes , Reinhard Lorenz , Stephan Bauer , Thomas Ostrowski , Eva Baum , Dieter Junge
IPC分类号： C07C4311
CPC分类号： C08G65/2663 , B01J27/26 , B01J35/023
摘要： In multimetal cyanide complexes, more than 30% by weight of the primary particles have a platelet-like habit, i.e. the length and width of the primary particles is at least three times the thickness of the particles.
摘要翻译：在多金属氰化物络合物中，超过30重量％的初级颗粒具有血小板样习惯，即一次颗粒的长度和宽度至少为颗粒厚度的三倍。

9. 发明授权

US06664428B2 Method of producing polyetherpolyols 有权
标题翻译：生产聚醚多元醇的方法
公开(公告)号：US06664428B2
公开(公告)日：2003-12-16
申请号：US10204293
申请日：2002-08-20
申请人： Thomas Ostrowski , Kathrin Harre , Georg Heinrich Grosch , Gerd Höppner , Peter de Vocht , Dirk Leys , Jürgen Winkler , Stephan Bauer
发明人： Thomas Ostrowski , Kathrin Harre , Georg Heinrich Grosch , Gerd Höppner , Peter de Vocht , Dirk Leys , Jürgen Winkler , Stephan Bauer
IPC分类号： C07C4311
CPC分类号： C08G65/2696 , C08G65/2663
摘要： A process for the preparation of polyetherpolyols by reacting diols or polyols with ethylene oxide, propylene oxide, butylene oxide or a mixture thereof in the presence of a multimetal cyanide complex catalyst is proposed, the reaction being carried out in a stirred kettle reactor and the reaction mixture being circulated via an external heat exchanger by means of a pump.
摘要翻译：提出了在多金属氰化物配合物催化剂存在下，通过二醇或多元醇与环氧乙烷，环氧丙烷，环氧丁烷或其混合物反应制备聚醚多元醇的方法，该反应在搅拌釜反应器中进行，反应混合物通过泵通过外部热交换器循环。

10. 发明授权

US09163103B2 Hydrophobically associating copolymers 有权
标题翻译：疏水缔合共聚物
公开(公告)号：US09163103B2
公开(公告)日：2015-10-20
申请号：US14323324
申请日：2014-07-03
申请人： Roland Reichenbach-Klinke , Thomas Pfeuffer , Kati Schmidt , Thomas Ostrowski , Reinhold J. Leyrer , Yulia Fogel , Stefan Friedrich , Peter Gaeberlein , Andrea Orleans , Manfred Schuhbeck , Marcus Guzmann , Marcus Rösch , Bjorn Langlotz
发明人： Roland Reichenbach-Klinke , Thomas Pfeuffer , Kati Schmidt , Thomas Ostrowski , Reinhold J. Leyrer , Yulia Fogel , Stefan Friedrich , Peter Gaeberlein , Andrea Orleans , Manfred Schuhbeck , Marcus Guzmann , Marcus Rösch , Bjorn Langlotz
IPC分类号： C04B24/26 , C04B24/38 , C08F220/58 , C08F220/26 , C08F220/56 , C08F228/02 , C08F230/02 , C09K8/588 , E21B43/16 , C04B16/04 , C08F220/60 , C04B103/00
CPC分类号： C08F220/58 , C04B16/04 , C04B2103/0052 , C04B2103/0053 , C08F220/26 , C08F220/56 , C08F220/60 , C08F228/02 , C08F230/02 , C08F2220/585 , C09K8/588 , E21B43/16
摘要： Water-soluble, hydrophobically associating copolymers which comprise new types of hydrophobically associating monomers. The monomers comprise an ethylenically unsaturated group and a polyether group with block structure comprising a hydrophilic polyalkylene oxide block which consists essentially of ethylene oxide groups, and a terminal, hydrophobic polyalkylene oxide block which consists of alkylene oxides with at least 4, preferably at least 5 carbon atoms.
摘要翻译：包含新型疏水缔合单体的水溶性疏水缔合共聚物。单体包含烯属不饱和基团和具有嵌段结构的聚醚基团，其包含基本上由环氧乙烷基团组成的亲水性聚环氧烷嵌段，以及末端疏水性聚环氧烷嵌段，其由具有至少4个，优选至少5个碳原子。

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