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1. 发明授权

US09096497B2 Process for preparing EDDN and EDMN 有权
标题翻译：制作EDDN和EDMN的过程
公开(公告)号：US09096497B2
公开(公告)日：2015-08-04
申请号：US13598769
申请日：2012-08-30
申请人： Hermann Luyken , Sebastian Ahrens , Gordon Brasche , Jens Baldamus , Robert Baumann , Randolf Hugo , Stephanie Jaegli , Johann-Peter Melder , Jörg Pastre , Boris Buschhaus
发明人： Hermann Luyken , Sebastian Ahrens , Gordon Brasche , Jens Baldamus , Robert Baumann , Randolf Hugo , Stephanie Jaegli , Johann-Peter Melder , Jörg Pastre , Boris Buschhaus
IPC分类号： C07C209/48 , C07C253/00 , C07C231/10 , C07C213/00 , C07C253/06 , C07C253/30 , C07C211/14
CPC分类号： C07C253/00 , C07C209/48 , C07C213/00 , C07C231/10 , C07C253/06 , C07C253/30 , C07C255/25 , C07C255/16 , C07C215/14 , C07C211/14
摘要： A process for preparing EDDN and/or EDMN by conversion of FA, HCN and EDA, the reaction being effected in the presence of water, and, after the conversion, water being depleted from the reaction mixture in a distillation column, which comprises performing the distillation in the presence of an organic solvent which has a boiling point between water and EDDN and/or EDMN at the distillation pressure existing in the column or which forms a low-boiling azeotrope with water.
摘要翻译：通过转化FA，HCN和EDA来制备EDDN和/或EDMN的方法，反应在水存在下进行，并且在转化后，在蒸馏塔中从反应混合物中消耗水，其包括进行在存在于塔中的蒸馏压力下或与水形成低沸点共沸物的有机溶剂存在下进行蒸馏，所述有机溶剂具有水与EDDN和/或EDMN之间的沸点。

2. 发明授权

US09012638B2 Process for preparing EDDN and/or EDMN by conversion of FACH and EDA 有权
标题翻译：通过转换FACH和EDA来制备EDDN和/或EDMN的过程
公开(公告)号：US09012638B2
公开(公告)日：2015-04-21
申请号：US13599325
申请日：2012-08-30
申请人： Hermann Luyken , Sebastian Ahrens , Gordon Brasche , Jens Baldamus , Robert Baumann , Randolf Hugo , Stephanie Jaegli , Johann-Peter Melder , Jörg Pastre , Boris Buschhaus
发明人： Hermann Luyken , Sebastian Ahrens , Gordon Brasche , Jens Baldamus , Robert Baumann , Randolf Hugo , Stephanie Jaegli , Johann-Peter Melder , Jörg Pastre , Boris Buschhaus
IPC分类号： C07D241/04 , C07C253/30 , C07C209/48 , C07D295/00
CPC分类号： C07C253/30 , C07C209/48 , C07C211/14 , C07C255/25
摘要： A process for reacting formaldehyde cyanohydrin (FACH) with ethylenediamine (EDA) in a reactor with limited backmixing at a temperature in the range from 20 to 120° C., wherein the residence time in the reactor is 300 seconds or less.
摘要翻译：在20〜120℃的温度范围内，在反应器中使甲醛羟化氢（FACH）与乙二胺（EDA）反应的反应器的方法，其中在反应器中的停留时间为300秒以下。

3. 发明申请

US20130053538A1 PROCESS FOR PREPARING EDFA AND/OR EDMFA AND DETA AND/OR TETA 审中-公开
标题翻译：制备EDFA和/或EDMFA和DETA和/或TETA的方法
公开(公告)号：US20130053538A1
公开(公告)日：2013-02-28
申请号：US13598750
申请日：2012-08-30
申请人： Hermann Luyken , Sebastian Ahrens , Gordon Brasche , Jens Baldamus , Robert Baumann , Randolf Hugo , Stephanie Jaegli , Johann-Peter Melder , Jörg Pastre , Boris Buschhaus
发明人： Hermann Luyken , Sebastian Ahrens , Gordon Brasche , Jens Baldamus , Robert Baumann , Randolf Hugo , Stephanie Jaegli , Johann-Peter Melder , Jörg Pastre , Boris Buschhaus
IPC分类号： C07C213/00 , C08G59/00 , C08G69/00 , C07C253/30 , C07C209/48
CPC分类号： C07C209/48 , C07C231/02 , C07C253/06 , C08G69/26 , C08G69/28 , C07C233/36 , C07C255/25 , C07C211/14
摘要： A process for reacting ethylenediamine (EDA) with formaldehyde to give ethylenediamine-formaldehyde adduct (EDFA) and/or ethylenediamine-monoformaldehyde adduct (EDMFA), which comprises performing the reaction of FA with EDA at a temperature in the range from 20 to 70° C.
摘要翻译：一种使乙二胺（EDA）与甲醛反应得到乙二胺 - 甲醛加合物（EDFA）和/或乙二胺单甲醛加合物（EDMFA）的方法，其包括在20至70℃的温度下进行FA与EDA的反应 C。

4. 发明申请

US20130053537A1 PROCESS FOR REGENERATING RANEY CATALYSTS 审中-公开
标题翻译：用于再生RANEY催化剂的方法
公开(公告)号：US20130053537A1
公开(公告)日：2013-02-28
申请号：US13598712
申请日：2012-08-30
申请人： Hermann Luyken , Sebastian Ahrens , Gordon Brasche , Jens Baldamus , Robert Baumann , Randolf Hugo , Stephanie Jaegli , Johann-Peter Melder , Jörg Pastre , Boris Buschhaus
发明人： Hermann Luyken , Sebastian Ahrens , Gordon Brasche , Jens Baldamus , Robert Baumann , Randolf Hugo , Stephanie Jaegli , Johann-Peter Melder , Jörg Pastre , Boris Buschhaus
IPC分类号： B01J25/04 , C08G59/00 , C07C209/48
CPC分类号： B01J25/04 , B01J38/02 , B01J38/10 , B01J38/58 , B01J38/64 , B01J38/66 , C07C209/48 , Y02P20/584 , C07C211/14
摘要： A process for regenerating Raney catalysts by treating the catalyst with liquid ammonia with a water content of less than 5% by weight and with hydrogen having a partial pressure of 0.1 to 40 MPa in the temperature range from 50 to 350° C. for at least 0.1 hour.
摘要翻译：通过用水含量小于5重量％的液氨和在50至350℃的温度范围内分压为0.1至40MPa的氢处理催化剂来再生阮内催化剂的方法，至少 0.1小时。

5. 发明申请

US20130053536A1 PROCESS FOR PREPARING EDDN AND/OR EDMN AND A PROCESS FOR PREPARING DETA AND/OR TETA 审中-公开
标题翻译：制备EDDN和/或EDMN的方法和制备DETA和/或TETA的方法
公开(公告)号：US20130053536A1
公开(公告)日：2013-02-28
申请号：US13598715
申请日：2012-08-30
申请人： Hermann Luyken , Sebastian Ahrens , Gordon Brasche , Jens Baldamus , Robert Baumann , Randolf Hugo , Stephanie Jaegli , Johann-Peter Melder , Jörg Pastre , Boris Buschhaus
发明人： Hermann Luyken , Sebastian Ahrens , Gordon Brasche , Jens Baldamus , Robert Baumann , Randolf Hugo , Stephanie Jaegli , Johann-Peter Melder , Jörg Pastre , Boris Buschhaus
IPC分类号： C07C253/00 , C07C231/10 , C08G59/02 , C07C209/48
CPC分类号： C07C209/48 , C07C253/00 , C08G59/502 , C07C211/14 , C07C255/25
摘要： A process for preparing EDDN and/or EDMN by a) conversion of FA, HCN and EDA, the conversion being effected in the presence of water, b) depleting water from the reaction mixture obtained in stage a), and c) treating the mixture from stage b) with an absorbent in the presence of an organic solvent, wherein the adsorbent is a solid acidic adsorbent.
摘要翻译： a）通过a）转化FA，HCN和EDA来制备EDDN和/或EDMN的方法，转化在水存在下进行，b）从步骤a）中获得的反应混合物中消耗水，和c）处理混合物从阶段b）与有机溶剂存在下的吸收剂，其中吸附剂是固体酸性吸附剂。

6. 发明申请

US20120271068A1 REACTION OF GLYCOLALDEHYDE WITH AN AMINATING AGENT 有权
标题翻译：甘氨酸与氨基化剂的反应
公开(公告)号：US20120271068A1
公开(公告)日：2012-10-25
申请号：US13516479
申请日：2010-12-14
申请人： Wolfgang Mägerlein , Johann-Peter Melder , Jörg Pastre , Jan Eberhardt , Thomas Krug , Mirko Kreitschmann
发明人： Wolfgang Mägerlein , Johann-Peter Melder , Jörg Pastre , Jan Eberhardt , Thomas Krug , Mirko Kreitschmann
IPC分类号： C07C213/02
CPC分类号： C07C209/26 , C07C213/00 , C07C215/08 , C07C211/10
摘要： The present invention relates to a process for reacting glycolaldehyde with an aminating agent in the presence of hydrogen and of a catalyst, the catalyst being activated by reducing a catalyst precursor or by reducing a passivated catalyst, which comprises effecting the reaction in the presence of a solvent and contacting the glycolaldehyde with the activated catalyst.
摘要翻译：本发明涉及一种在氢气和催化剂存在下使乙醇醛与胺化剂反应的方法，该催化剂通过还原催化剂前体而被还原或通过还原钝化的催化剂来活化，其包括在存在下进行反应溶剂并使乙醇醛与活化的催化剂接触。

7. 发明授权

US07351860B2 Method and device for producing formic acid formates and use of said formates 失效
标题翻译：用于生产甲酸甲酸盐和所述甲酸盐的使用的方法和装置
公开(公告)号：US07351860B2
公开(公告)日：2008-04-01
申请号：US10524268
申请日：2003-07-30
申请人： Christoph Adami , Jörn Karl , Alexander Hauk , Ralf Böhling , Jörg Pastre , Robert Lenz
发明人： Christoph Adami , Jörn Karl , Alexander Hauk , Ralf Böhling , Jörg Pastre , Robert Lenz
IPC分类号： C07C53/00
CPC分类号： C07C51/412 , C07C53/06
摘要： The invention relates to a method for producing formic acid formates, whereby (a) formic acid methyl ester is partially hydrolysed with water; (b) formic acid methyl ester and methanol are separated by distillation from the reaction mixture obtained in step (a), forming a current containing formic acid and water; (c) the current obtained in step (b), containing the formic acid methyl ester and optionally methanol, is converted into a current containing formate and water, by (i) reaction with a basic compound having a pKa value of the corresponding acid of the corresponding dissociation step of =3, measured at 25° C. in an aqueous solution, in presence of water, and (ii) separation by distillation of the methanol; and (d) the current obtained in step (b), containing formic acid and water, and the current obtained in step (c), containing formate and water, are combined to form a mixture containing the formic acid formate and water. The invention also relates to a device for producing said formic acid formates and to the use of the same.
摘要翻译：本发明涉及甲酸甲酸盐的制备方法，其中（a）甲酸甲酯用水部分水解; （b）甲酸甲酯和甲醇通过蒸馏从步骤（a）中获得的反应混合物分离，形成含有甲酸和水的电流; （c）将含有甲酸甲酯和任选的甲醇的步骤（b）中获得的电流转化成含有甲酸盐和水的电流，通过（i）与具有pK aa的碱性化合物反应，在水溶液中，在水的存在下，在25℃下测定相应解离步骤的相应酸的相应值，和（ii）通过蒸馏甲醇分离; 和（d）将包含甲酸和水的步骤（b）中得到的电流和步骤（c）中得到的含有甲酸盐和水的电流合并形成含有甲酸甲酸盐和水的混合物。本发明还涉及用于生产所述甲酸甲酸盐的装置及其用途。

8. 发明申请

US20130079492A1 PROCESS FOR PREPARING EDDN AND EDMN 有权
标题翻译：制作EDDN和EDMN的过程
公开(公告)号：US20130079492A1
公开(公告)日：2013-03-28
申请号：US13598769
申请日：2012-08-30
申请人： Hermann Luyken , Sebastian Ahrens , Gordon Brasche , Jens Baldamus , Robert Baumann , Randolf Hugo , Stephanie Jaegli , Johann-Peter Melder , Jörg Pastre , Boris Buschhaus
发明人： Hermann Luyken , Sebastian Ahrens , Gordon Brasche , Jens Baldamus , Robert Baumann , Randolf Hugo , Stephanie Jaegli , Johann-Peter Melder , Jörg Pastre , Boris Buschhaus
IPC分类号： C07C253/00 , C07C231/10 , C07C209/48
CPC分类号： C07C253/00 , C07C209/48 , C07C213/00 , C07C231/10 , C07C253/06 , C07C253/30 , C07C255/25 , C07C255/16 , C07C215/14 , C07C211/14
摘要： A process for preparing EDDN and/or EDMN by conversion of FA, HCN and EDA, the reaction being effected in the presence of water, and, after the conversion, water being depleted from the reaction mixture in a distillation column, which comprises performing the distillation in the presence of an organic solvent which has a boiling point between water and EDDN and/or EDMN at the distillation pressure existing in the column or which forms a low-boiling azeotrope with water.
摘要翻译：通过转化FA，HCN和EDA来制备EDDN和/或EDMN的方法，反应在水存在下进行，并且在转化后，在蒸馏塔中从反应混合物中消耗水，其包括进行在存在于塔中的蒸馏压力下或与水形成低沸点共沸物的有机溶剂存在下进行蒸馏，所述有机溶剂具有水与EDDN和/或EDMN之间的沸点。

9. 发明申请

US20130053584A1 PROCESS FOR PREPARING EDDN AND/OR EDMN BY REACTING EDFA AND/OR EDMFA WITH HCN 有权
标题翻译：通过用HCN反应EDFA和/或EDMFA来制备EDDN和/或EDMFA的方法
公开(公告)号：US20130053584A1
公开(公告)日：2013-02-28
申请号：US13598685
申请日：2012-08-30
申请人： Hermann Luyken , Sebastian Ahrens , Gordon Brasche , Jens Baldamus , Robert Baumann , Randolf Hugo , Stephanie Jaegli , Johann-Peter Melder , Jörg Pastre , Boris Buschhaus
发明人： Hermann Luyken , Sebastian Ahrens , Gordon Brasche , Jens Baldamus , Robert Baumann , Randolf Hugo , Stephanie Jaegli , Johann-Peter Melder , Jörg Pastre , Boris Buschhaus
IPC分类号： C07C253/06 , C07D303/02 , C07C231/10 , C07C209/48
CPC分类号： C07C209/48 , C07C253/06 , C07C255/04 , C07C211/14
摘要： A process for reacting ethylenediamine-formaldehyde adduct (EDFA) and/or ethylene-diamine-monoformaldehyde adduct (EDMFA) with hydrogen cyanide (HCN) in a reactor with limited backmixing at a temperature in the range from 20 to 120° C., wherein the residence time in the reactor is 300 seconds or less.
摘要翻译：在20〜120℃的温度范围内使乙二胺 - 甲醛加合物（EDFA）和/或乙二胺 - 一甲醛加合物（EDMFA）与氰化氢（HCN）在反应器中进行有限回混反应的方法，其中反应器中的停留时间为300秒以下。

10. 发明申请

US20120259139A1 METHOD FOR PREPARING HIGHER ETHANOLAMINES 有权
标题翻译：制备高级乙酰胺的方法
公开(公告)号：US20120259139A1
公开(公告)日：2012-10-11
申请号：US13516521
申请日：2010-12-13
申请人： Wolfgang Mägerlein , Johann-Peter Melder , Jörg Pastre , Jan Eberhardt , Thomas Krug , Mirko Kreitschmann
发明人： Wolfgang Mägerlein , Johann-Peter Melder , Jörg Pastre , Jan Eberhardt , Thomas Krug , Mirko Kreitschmann
IPC分类号： C07C213/00
CPC分类号： C07C215/12 , C07C213/08
摘要： The present invention relates to a process for preparing ethanolamines by reacting glycolaldehyde with monoethanolamine and/or diethanolamine in the presence of a catalyst.
摘要翻译：本发明涉及一种在催化剂存在下使乙醇醛与单乙醇胺和/或二乙醇胺反应制备乙醇胺的方法。

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