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1. 发明申请

US20190194545A1 MULTI-PURPOSE REACTOR AND PROCESS FOR THE PREPARATION OF MODIFIED BITUMEN 审中-公开
公开(公告)号：US20190194545A1
公开(公告)日：2019-06-27
申请号：US16292905
申请日：2019-03-05
申请人： SHELL OIL COMPANY
发明人： Roberto BRAN , Cheluva KUMAR , Sachin RAJ , Daryl SCOTT
IPC分类号： C10C3/04 , B01F3/04 , B01F15/00 , B01F7/00 , B01F7/04
CPC分类号： C10C3/04 , B01F3/04588 , B01F7/00633 , B01F7/00758 , B01F7/04 , B01F15/00883 , B01J8/10 , B01J8/222 , B01J10/002 , B01J19/0066 , B01J19/18 , B01J2208/00212 , B01J2219/00094 , B01J2219/182
摘要： A reactor is provided for the preparation of modified bitumen, which reactor comprises a horizontal housing comprising a cylindrical wall and two side walls, wherein a bitumen inlet has been provided at or near one of the side walls of the housing and a bitumen product outlet has been provided at or near the opposite side wall of the housing, wherein a plurality of inlets for the provision of oxygen-containing gas has been provided in the cylindrical wall of the housing between the bitumen inlet and the bitumen product outlet, which multi-purpose reactor is further provided with a mixer arranged inside the housing comprising at least one rotor rotating within at least one stator having a plurality of openings. The reactor is used to prepare modified bitumen by contacting bitumen in the reactor with a modified elevated temperature and pressure.

2. 发明申请

US20180229179A1 OXIDATION CONTROL FOR IMPROVED FLUE GAS DESULFURIZATION PERFORMANCE 审中-公开
公开(公告)号：US20180229179A1
公开(公告)日：2018-08-16
申请号：US15433230
申请日：2017-02-15
申请人： General Electric Technology GmbH
发明人： Raymond Raulfs GANSLEY
IPC分类号： B01D53/14 , B01D53/50 , B01D53/34 , B01J19/00 , B01J10/00
CPC分类号： B01J10/002 , B01D53/346 , B01D53/504 , B01D53/78 , B01D2251/102 , B01D2251/304 , B01D2251/402 , B01D2251/404 , B01D2251/606 , B01D2258/0283 , B01J19/0006 , B01J2219/00164 , B01J2219/00186 , C10G70/00
摘要： A system and method of using the system for controlling oxidation of sulfites to reduce total nitrite and nitrate levels in a slurry is disclosed. The system includes a tank having an inlet for receiving a slurry produced in a wet flue gas desulfurization process. The tank also includes an inlet for receiving a gas. The inlet for receiving the gas is operable to disperse at least a portion of the gas received in the tank through at least a portion of the slurry received in the tank. A sensor is configured to measure a sulfite concentration of the slurry received in the tank to obtain a sulfite concentration measurement. In some embodiments, the sensor is a sulfite analyzer. In other embodiments, the sensor is a virtual analyzer. The system also includes a controller. Software executing on the controller generates an electronic signal affecting an adjustment of a flow rate of gas into the slurry in the tank based at least in part on the sulfite concentration/sulfite concentration measurement.

3. 发明申请

US20180119083A1 Airlift Reactor Assembly with Helical Sieve Plate 审中-公开
公开(公告)号：US20180119083A1
公开(公告)日：2018-05-03
申请号：US15795320
申请日：2017-10-27
申请人： Jiangnan University
发明人： Zhiyong Zheng , Yuqi Chen , Xiaobei Zhan , Minjie Gao
IPC分类号： C12M1/00 , B01J8/08 , B01J19/24 , B01J10/00 , C12M1/08
CPC分类号： C12M29/08 , B01J4/004 , B01J8/08 , B01J8/10 , B01J8/222 , B01J10/002 , B01J19/006 , B01J19/0066 , B01J19/20 , B01J19/24 , B01J19/2405 , B01J2208/00884 , B01J2219/00094 , B01J2219/00768 , B01J2219/00772 , B01J2219/185 , B01J2219/1943 , B01J2219/24 , C12M23/22 , C12M27/20 , C12M27/24
摘要： The present invention discloses an airlift reactor assembly with a helical sieve plate, comprising a reaction tank, wherein a draft tube and a gas sparger are assembled in the reaction tank, the gas sparger is arranged just below an riser section of the draft tube, a helical sieve plate is arranged in the riser section of the draft tube, and a body of the helical sieve plate is helical upwards to guide a part of two/three-phase flow in the riser section, and the body of the helical sieve plate is provided with a plurality of sieve meshes to guide the remaining two/three-phase go through the helical sieve plate in the riser section and to break bubbles. The present invention gives consideration to both macroscopic mixing and microscopic mixing processes. In addition to driving liquid to circularly flow by using ejected gas, the helical sieve plate can be used for breaking large bubbles into small bubbles thereby effectively preventing the bubbles from coalescing, increasing gas holdup and increasing a volumetric oxygen transfer coefficient.

4. 发明授权

US09944964B2 Processes for increasing bioalcohol yield from biomass 有权
公开(公告)号：US09944964B2
公开(公告)日：2018-04-17
申请号：US15431558
申请日：2017-02-13
申请人： Cavitation Technologies, Inc.
发明人： Roman Gordon , Igor Gorodnitsky , Maxim A. Promtov , Vijayanand Suryakant Moholkar
IPC分类号： C12P19/14 , C12P19/02
CPC分类号： C12P19/14 , A23K10/37 , A23K50/10 , B01F5/0644 , B01F5/0646 , B01F5/0652 , B01F5/0653 , B01F5/0682 , B01F5/0688 , B01F13/1025 , B01F13/1027 , B01J10/002 , B01J19/0066 , B01J19/008 , B01J19/02 , B01J19/2415 , B01J2219/0218 , B01J2219/0231 , B01J2219/0245 , C10L1/02 , C10L1/023 , C11B3/001 , C11B3/006 , C11B3/04 , C11B3/16 , C11C3/003 , C12N1/38 , C12P7/10 , C12P19/02 , C12P2201/00 , Y02E50/16 , Y02P60/877
摘要： A process for increasing alcohol yield from biomass (the form or agro- or forest residue, grains, hops, etc.), involving multiple hydrodynamic cavitation treatments of biomass filtrate—both before and after fermentation. Carbohydrates extracted from biomass are subjected to a first cavitation treatment to promote additional conversion into carbohydrates. The carbohydrates are then combined with bacterial species and nutrients, and allowed to ferment. The fermentation product is subjected to a second hydrodynamic cavitation treatment to promote further conversion of carbohydrates into bioalcohol. After distillation, the bioalcohol is subjected to a second hydrodynamic cavitation treatment to increase its purity.

5. 发明授权

US09944753B2 Continuous polyamidation process—I 有权
公开(公告)号：US09944753B2
公开(公告)日：2018-04-17
申请号：US15037633
申请日：2014-11-20
申请人： Ernest Keith Marchildon , Karen A. Surgenor , Bryan D. Kaushiva
发明人： Ernest Keith Marchildon , Karen A. Surgenor , Bryan D. Kaushiva
IPC分类号： C08G69/28 , C08L77/00 , B01J14/00 , B01J10/00 , B01J19/00 , B01J19/18 , B01J19/24 , B01J4/00
CPC分类号： C08G69/28 , B01J4/002 , B01J10/002 , B01J14/00 , B01J19/0006 , B01J19/006 , B01J19/0066 , B01J19/18 , B01J19/245 , B01J2219/00186 , B01J2219/002 , B01J2219/00202 , B01J2219/00231 , C08L77/00
摘要： A continuous process for the manufacture of a polyamide, the process comprising the steps of: (i) flowing a stream A comprising a molten dicarboxylic acid, or a molten dicarboxylic acid-rich mixture comprising a dicarboxylic acid and a diamine, through a first stage and at least one more reaction stage of a vertical multistage reactor, wherein the first stage is at the top of the reactor; (ii) counter-currently flowing a stream B comprising a diamine as either a vapor or a diamine-rich liquid through at least one of the stages below the first reaction stage of said vertical multistage reactor; (iii) accumulating a liquid phase material P comprising polyamide at and/or below the final stage of said reactor; wherein said reactor is equipped with internal features suitable for effecting contact between counter-currently flowing streams A and B; and wherein said process further comprises the step of agitating said liquid phase material P by injecting a gaseous stream C comprising steam, or at least one inert gas, or a mixture of steam and at least one inert gas into the reactor at or below the final stage of the reactor. The invention further provides a vertical multistage reactor configured to implement said process.

6. 发明授权

US09694334B2 Gas diffusion system and method for introducing a gas stream in an apparatus, in particular a passivating gas stream in a urea plant 有权
公开(公告)号：US09694334B2
公开(公告)日：2017-07-04
申请号：US14902814
申请日：2014-07-04
申请人： SAIPEM S.p.A.
发明人： Paolo Minola
IPC分类号： B01F3/00 , B01F3/04 , B01J4/00 , B01J10/00 , B01J19/00 , B01J19/24 , C07C273/00 , C07C273/02 , C07C273/04
CPC分类号： B01J4/002 , B01F3/04248 , B01F3/04262 , B01F2003/0429 , B01F2003/04304 , B01F2003/04319 , B01F2003/04368 , B01J10/002 , B01J19/24 , B01J2219/1946 , B01J2219/24 , C07C273/02 , C07C273/04 , Y02P20/142
摘要： A gas diffusion system configured to feed a gas stream, in particular a passivating gas stream, into an apparatus, in particular a decomposer, of a urea plant; the system extends along an axis and has a gas feed conduit having an outlet from which the gas flows substantially parallel to the axis, and a diffuser assembly configured to diffuse the gas supply from the conduit; the diffuser assembly is shaped so as to intercept the gas stream flowing axially from the outlet, and divert the gas stream substantially radially with respect to the axis and uniformly about the axis.

7. 发明申请

US20160332979A1 FURAN-2,5-DICARBOXYLIC ACID PURGE PROCESS 审中-公开
公开(公告)号：US20160332979A1
公开(公告)日：2016-11-17
申请号：US15217319
申请日：2016-07-22
申请人： EASTMAN CHEMICAL COMPANY
发明人： Kevin John Fontenot , Mesfin Ejerssa Janka , Kenny Randolph Parker , Ashfaq Shahanawaz Shaikh , Lee Reynolds Partin , Charles Edwan Sumner, JR. , Shane Kipley Kirk , Paula Moody , Bradford Russell Bowers , Michael Charles Morrow
IPC分类号： C07D307/68 , B01J23/889 , B01J10/00
CPC分类号： B01J27/32 , B01D11/04 , B01D11/0446 , B01D17/00 , B01J10/002 , B01J23/8892 , B01J27/128 , B01J35/12 , B01J38/12 , C07D307/68 , Y02P20/584
摘要： Disclosed is an oxidation process to produce a crude carboxylic acid product carboxylic acid product. The process comprises oxidizing a feed stream comprising at least one oxidizable compound to generate a crude carboxylic acid slurry comprising furan-2,5-dicarboxylic acid (FDCA) and compositions thereof. Also disclosed is a process to produce a dry purified carboxylic acid product by utilizing various purification methods on the crude carboxylic acid.

8. 发明申请

US20160289384A1 CONTINUOUS POLYAMIDATION PROCESS - II 有权
标题翻译：连续聚酰胺工艺 - 二
公开(公告)号：US20160289384A1
公开(公告)日：2016-10-06
申请号：US15037635
申请日：2014-11-20
申请人： INVISTA NORTH AMERICA S.A R.L.
发明人： Ernest Keith MARCHILDON , Karen A. SURGENOR , Bryan D. KAUSHIVA
IPC分类号： C08G69/28
CPC分类号： C08G69/28 , B01J4/002 , B01J10/002 , B01J14/00 , B01J19/0006 , B01J19/006 , B01J19/18 , B01J19/245 , B01J2219/00186 , B01J2219/002 , B01J2219/00202 , B01J2219/00231
摘要： A continuous process for the manufacture of a polyamide, the process comprising the steps of: (i) flowing a stream A comprising a moltendicarboxylic acid, or a molten dicarboxylic acid-rich mixture comprising a dicarboxylic acid and a diamine, through a first stage and at least one more reaction stage of a vertical multistage reactor, wherein the first stage is at the top of the reactor; (ii) counter-currently flowing a stream B comprising a diamine as either a vapour or a diamine-rich liquid through at least one of the stages below the first reaction stage of said vertical multistage reactor; (iii) accumulating a liquid phase material P comprising polyamide at and/or below the final stage of said reactor; wherein said reactor is equipped with internal features suitable for effecting contact between counter-currently flowing streams A and B; and wherein the process further comprises controlling the viscosity of said liquid phase material P by directly controlling the chemical equilibrium of the polyamidation reaction or by controlling stream B so that the amounts of diamine and dicarboxylic acid introduced into the reactor during the process are stoichiometrically imbalanced. The invention further provides a vertical multistage reactor configured to implement said process.
摘要翻译：一种用于制造聚酰胺的连续方法，该方法包括以下步骤：（i）使包含二羧酸和二胺的含有糠醛二羧酸或熔融的富含二甲酸的混合物的流A通过第一阶段和至少一个垂直多级反应器的反应阶段，其中第一级位于反应器的顶部; （ii）将包含二胺的流B逆流地流过位于所述垂直多级反应器的第一反应级之下的至少一个级的蒸气或二胺富液体; （iii）在所述反应器的最后阶段和/或之下积聚包含聚酰胺的液相材料P; 其中所述反应器配备有适于实现逆向流动流A和B之间的接触的内部特征; 并且其中所述方法还包括通过直接控制聚酰胺化反应的化学平衡或通过控制流B来控制所述液相材料P的粘度，使得在该方法期间引入反应器中的二胺和二羧酸的量是化学计量不平衡的。本发明还提供了一种被配置为实现所述过程的立式多级反应器。

9. 发明申请

US20160289383A1 CONTINUOUS POLYAMIDATION PROCESS - I 有权
标题翻译：连续聚酰胺工艺 -
公开(公告)号：US20160289383A1
公开(公告)日：2016-10-06
申请号：US15037633
申请日：2014-11-20
申请人： INVISTA TECHNOLOGIES S.À R.L.
发明人： Ernest Keith MARCHILDON , Karen A. SURGENOR , Bryan D. KAUSHIVA
IPC分类号： C08G69/28
CPC分类号： C08G69/28 , B01J4/002 , B01J10/002 , B01J14/00 , B01J19/0006 , B01J19/006 , B01J19/0066 , B01J19/18 , B01J19/245 , B01J2219/00186 , B01J2219/002 , B01J2219/00202 , B01J2219/00231 , C08L77/00
摘要： A continuous process for the manufacture of a polyamide, the process comprising the steps of: (i) flowing a stream A comprising a molten dicarboxylic acid, or a molten dicarboxylic acid-rich mixture comprising a dicarboxylic acid and a diamine, through a first stage and at least one more reaction stage of a vertical multistage reactor, wherein the first stage is at the top of the reactor; (ii) counter-currently flowing a stream B comprising a diamine as either a vapour or a diamine-rich liquid through at least one of the stages below the first reaction stage of said vertical multistage reactor; (iii) accumulating a liquid phase material P comprising polyamide at and/or below the final stage of said reactor; wherein said reactor is equipped with internal features suitable for effecting contact between counter-currently flowing streams A and B; and wherein said process further comprises the step of agitating said liquid phase material P by injecting a gaseous stream C comprising steam, or at least one inert gas, or a mixture of steam and at least one inert gas into the reactor at or below the final stage of the reactor. The invention further provides a vertical multistage reactor configured to implement said process.
摘要翻译：一种用于制造聚酰胺的连续方法，该方法包括以下步骤：（i）使包含二羧酸和二胺的熔融二羧酸或熔融二羧酸富混合物的流A通过第一阶段以及垂直多级反应器的至少一个反应阶段，其中第一级位于反应器的顶部; （ii）将包含二胺的流B逆流地流过位于所述垂直多级反应器的第一反应级之下的至少一个级的蒸气或二胺富液体; （iii）在所述反应器的最后阶段和/或之下积聚包含聚酰胺的液相材料P; 其中所述反应器配备有适于实现逆向流动流A和B之间的接触的内部特征; 并且其中所述方法还包括通过将包含蒸汽或至少一种惰性气体或蒸汽与至少一种惰性气体的混合物的气流C注入到反应器中或之下而最终搅拌所述液相材料P的步骤反应堆的阶段。本发明还提供了一种被配置为实现所述过程的立式多级反应器。

10. 发明授权

US09302966B2 Thermochemical preparation of monoalcohols from biomass 有权
标题翻译：来自生物质的一元醇的热化学制备
公开(公告)号：US09302966B2
公开(公告)日：2016-04-05
申请号：US14750581
申请日：2015-06-25
申请人： PHILLIPS 66 COMPANY
发明人： Lotero Edgar , Fjare A. Kristi , Sughrue L. Edward
IPC分类号： C07C29/60 , C07C29/17
CPC分类号： C07C29/60 , B01D63/06 , B01J10/002 , B01J10/007 , B01J19/2425 , B01J19/2475 , B01J19/32 , C07C29/172 , C07C31/12 , C07C31/125
摘要： A process for converting polyhydric alcohols to monoalcohols in a counter current column reactor with a metal based catalyst supported on a porous membrane coated over a tubular system that delivers hydrogen where a hydrocarbon (low polarity) liquid solvent is fed at the bottom of the column reactor and an aqueous liquid having polyhydric alcohols therein is fed into the top of the reactor such that the aqueous liquid flows countercurrent to the low polarity solvent liquid and further wherein the low polarity solvent liquid is less dense than the aqueous liquid such that the two liquids are subject to phase separation. Monoalcohols are formed by hydrogenolysis reactions of polyhydric alcohols on the metal catalyst. Monoalcohols phase separate from the aqueous phase to the hydrocarbon solvent. Monoalcohols are further separated from the organic solvent.
摘要翻译：一种在逆流塔式反应器中将多元醇转化为一元醇的方法，其中金属基催化剂负载在涂覆在管状系统上的多孔膜上，该多孔膜输送氢，其中烃（低极性）液体溶剂在塔式反应器的底部进料并且其中含有多元醇的水性液体被供给到反应器的顶部，使得水性液体与低极性溶剂液体逆流流动，并且其中低极性溶剂液体比水性液体致密度低，使得两种液体是经过相分离。单醇通过多元醇在金属催化剂上的氢解反应形成。单醇相与水相分离成烃溶剂。一元醇与有机溶剂进一步分离。

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