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1. 发明授权

US08614356B2 Method for producing toluylenediamine by hydrogenating dinitrotoluene 失效
标题翻译：通过氢化二硝基甲苯生产甲苯二胺的方法
公开(公告)号：US08614356B2
公开(公告)日：2013-12-24
申请号：US13142718
申请日：2009-12-21
申请人： Joana Coelho Tsou , Steffen Oehlenschlaeger , Ekkehard Schwab , Wolfgang Mackenroth , Hartwig Voss , Stefan Maixner , Samuel Neto , Sven Boehmeke , Frederik Van Laar
发明人： Joana Coelho Tsou , Steffen Oehlenschlaeger , Ekkehard Schwab , Wolfgang Mackenroth , Hartwig Voss , Stefan Maixner , Samuel Neto , Sven Boehmeke , Frederik Van Laar
IPC分类号： C07C209/00 , C07C211/00
CPC分类号： C07C209/36 , C07C211/50
摘要： A process for preparing tolylenediamine by hydrogenating dinitrotoluene with hydrogen in the presence of a suspended catalyst in a vertically upright reactor (1), at the upper end of which is arranged a motive jet nozzle (2) through which the reaction mixture drawn off from the reactor bottom, via an external loop, is sprayed into the upper region of the reactor (1) and then flows into a central inserted tube (4) which is arranged in the longitudinal direction of the reactor, flows through the latter from the top downward and flows upward again outside the inserted tube (4) in an internal loop motion, with a heat exchanger (6) in the interior of the reactor (1), through which cooling water flows, and absorbs some of the heat of reaction as it does so, with a feed for the dinitrotoluene at the upper end of the reactor (1) and a feed for the hydrogen at the lower end of the reactor (1), and wherein, in addition to the heat exchanger (6) arranged in the interior of the reactor (1), a further heat exchanger (W) is used in the external loop, in which water absorbs the rest of the heat of reaction by indirect heat exchange with the reaction mixture, which comprises utilizing the heat of reaction to raise steam with a pressure of at least 4 bar gauge by performing the hydrogenation of dinitrotoluene to tolylenediamine at a temperature of ≧180° C.
摘要翻译：一种通过在悬浮催化剂存在下用氢气将二硝基甲苯氢化在垂直直立反应器（1）中来制备甲苯二胺的方法，其上端设置有动力喷嘴（2），反应混合物从其中排出反应器底部通过外部环路喷射到反应器（1）的上部区域中，然后流入沿着反应器的纵向布置的中心插入管（4），其从顶部向下流动并且在反应器（1）的内部具有热交换器（6），内部循环运动再次向外流过插入的管（4），冷却水通过该换热器（6）流过，并吸收一些反应热用反应器（1）上端的二硝基甲苯进料和反应器（1）下端的氢气进料，并且其中除了设置在反应器（1）的下端的热交换器反应器（1）的内部，一个furt 她的热交换器（W）用于外部回路中，其中水通过与反应混合物的间接热交换吸收剩余的反应热，其中包括利用反应热量以至少4的压力升高蒸汽通过在> = 180℃的温度下进行二硝基甲苯氢化成甲苯二胺来测定。

2. 发明申请

US20130146537A1 PROCESS FOR WORKING-UP A REACTION MIXTURE COMPRISING POLYETHER POLYOL 有权
标题翻译：用于加工包含聚醚多元醇的反应混合物的方法
公开(公告)号：US20130146537A1
公开(公告)日：2013-06-13
申请号：US13712536
申请日：2012-12-12
申请人： Vinit CHILEKAR , Hartwig Voss , Jelan Kuhn , Ann De Colvenaer , Andreas Brodhagen
发明人： Vinit CHILEKAR , Hartwig Voss , Jelan Kuhn , Ann De Colvenaer , Andreas Brodhagen
IPC分类号： B01D61/24
CPC分类号： B01D61/246 , B01D11/0288 , B01D11/0292 , B01D11/0415 , B01D61/243 , C07C41/38
摘要： The invention relates to a process for working-up a reaction mixture (5) comprising polyetherol and dissolved alkali metal comprising catalyst, wherein at least alkali metal ions of the dissolved alkali metal comprising catalyst are partially or completely removed from the mixture by a membrane separation process, the process comprising following steps: (a) feeding the reaction mixture (5) comprising polyetherol and dissolved alkali metal comprising catalyst into a first chamber (1) of a separation unit (3), (b) feeding a solvent into a second chamber (7) of the separation unit (3), the first chamber (1) and the second chamber (7) being separated by a membrane (9), (c) transporting at least the alkali metal ions of the alkali metal comprising catalyst from the first chamber (1) into the second chamber by passing through the membrane (9).
摘要翻译：本发明涉及一种用于处理包含聚醚醚和包含催化剂的溶解的碱金属的反应混合物（5）的方法，其中至少包含催化剂的溶解的碱金属的碱金属离子通过膜分离部分或完全从混合物中除去方法包括以下步骤：（a）将包含聚乙烯醇和包含催化剂的溶解的碱金属的反应混合物（5）进料到分离单元（3）的第一室（1）中，（b）将溶剂进料到第二分离单元（3）的室（7），第一室（1）和第二室（7）被隔膜（9）隔开，（c）至少输送包含催化剂的碱金属的碱金属离子从第一腔室（1）通过膜（9）进入第二腔室。

3. 发明申请

US20120232267A1 PROCESS FOR CONTINUOUS HYDROGENATION OR HYDROGENATING AMINATION 失效
标题翻译：连续加氢或加氢胺化的方法
公开(公告)号：US20120232267A1
公开(公告)日：2012-09-13
申请号：US13423956
申请日：2012-03-19
申请人： Bram Willem Hoffer , Hartwig Voss , Ekkehard Schwab , Udo Rheude , Gerd Kaibel , Mathias Haake , Jan Eberhardt , Michael Karcher
发明人： Bram Willem Hoffer , Hartwig Voss , Ekkehard Schwab , Udo Rheude , Gerd Kaibel , Mathias Haake , Jan Eberhardt , Michael Karcher
IPC分类号： C07D265/30 , C07C45/62
CPC分类号： C07C45/62 , C07C47/228 , C07C49/04 , C07C47/02
摘要： A process continuously hydrogenating unsaturated compounds, in which particles of a first hydrogenation catalyst are suspended in a liquid phase in which an unsaturated compound is dissolved, the liquid phase, in the presence of a hydrogenous gas at a first partial hydrogen pressure and at a first temperature, is conducted through a packed bubble column reactor in cocurrent counter to the direction of gravity, the effluent from the bubble column reactor is sent to a gas-liquid separation, the liquid phase is sent to a crossfiltration to obtain a retentate and a filtrate, the retentate is recycled into the bubble column reactor and the filtrate, in the presence of a hydrogenous gas at a second partial hydrogen pressure and at a second temperature, is passed over a bed of a second hydrogenation catalyst, the second partial hydrogen pressure is at least 10 bar higher than the first partial hydrogen pressure.
摘要翻译：将第一氢化催化剂的颗粒悬浮在其中溶解有不饱和化合物的液相中的不饱和化合物的液相，在第一部分氢气压力下的氢气存在下的液相，温度，通过与泡沫塔反应器并流反向并流并通过气泡塔反应器进行气液分离，将液相送至交叉过滤以获得滞留物和滤液，将渗余物再循环到泡罩塔反应器中，并且在第二部分氢气压力和第二温度下在氢气存在下将滤液通过第二氢化催化剂床，第二部分氢气压力为比第一部分氢气压力高至少10巴。

4. 发明授权

US08197645B2 Process for separating propylene glycol from aqueous compositions 有权
标题翻译：从水性组合物中分离丙二醇的方法
公开(公告)号：US08197645B2
公开(公告)日：2012-06-12
申请号：US12159321
申请日：2006-12-13
申请人： Armin Diefenbacher , Hans-Georg Goebbel , Stefan Bitterlich , Hartwig Voss , Henning Schultz , Anna Forlin , Renate Patrascu
发明人： Armin Diefenbacher , Hans-Georg Goebbel , Stefan Bitterlich , Hartwig Voss , Henning Schultz , Anna Forlin , Renate Patrascu
IPC分类号： B01D1/26 , B01D3/14 , C07C29/80 , C07C31/18
CPC分类号： B01D1/26 , B01D1/02 , B01D3/148 , B01D3/322 , C07C29/80 , Y10S159/08 , Y10S203/17 , C07C31/205
摘要： The present invention relates to a process for separating at least one propylene glycol from a mixture (M) comprising water and said propylene glycol, said process comprising (I) evaporating the mixture in at least two evaporation and/or distillation stages at decreasing operating pressures of the evaporators and/or distillation columns obtaining mixture (M′) and mixture (M″); (II) separating the mixture (M′) obtained in (I) in at least one further distillation step, obtaining a mixture (M-I) comprising at least 70 wt.-% of water and a mixture (M-II) comprising less than 30 wt.-% of water.
摘要翻译：本发明涉及从包含水和所述丙二醇的混合物（M）中分离至少一种丙二醇的方法，所述方法包括（I）在降低的操作压力下在至少两个蒸发和/或蒸馏阶段蒸发混合物的蒸发器和/或蒸馏塔获得混合物（M'）和混合物（M“）; （II）将在（I）中获得的混合物（M'）在至少一个另外的蒸馏步骤中分离，得到包含至少70重量％的水的混合物（MI）和包含少于 30重量％的水。

5. 发明申请

US20110197762A1 Template-Free Clathrasils And Clathrasil Membranes 失效
标题翻译：无模板的Clathrasils和Clathrasil膜
公开(公告)号：US20110197762A1
公开(公告)日：2011-08-18
申请号：US13121839
申请日：2009-09-28
申请人： Hartwig Voss , Jörg Therre , Hermann Gies , Bernd Marler
发明人： Hartwig Voss , Jörg Therre , Hermann Gies , Bernd Marler
IPC分类号： B01D53/22 , C01B33/12 , C01B39/02 , C01B37/02 , C30B7/10
CPC分类号： B01D71/027 , B01D53/047 , B01D53/228 , B01D67/0039 , B01D67/0051 , B01D69/02 , B01D71/028 , B01D2253/106 , B01D2256/24 , B01D2257/108 , B01D2257/11 , B01D2257/406 , B01D2257/80 , B01D2323/08 , B01D2323/10 , C01B37/00 , C01B37/02 , C01B39/52
摘要： The present invention relates to template-free clathraslls whose framework comprises essentially SO2, wherein the crystals of the ciathrasils have the platelet-like morphology of a sheet silicate. The present invention further relates to a process for preparing these template-free clathrasils and also to their use as absorbent, as seed crystals for the synthesis of ciathrasil membranes of the same zeolite type and in the form of dense layers which function as gas separation membranes having a molecular sieving action.
摘要翻译：本发明涉及其基本上包含SO 2的框架的无模板的层合体，其中所述硅胶的晶体具有片状硅酸盐的片状形态。本发明还涉及一种制备这些无模板的层状螯合物的方法，并且还涉及它们作为吸收剂的用途，作为用于合成相同沸石类型的以及用作气体分离膜的致密层形式的晶体具有分子筛选作用。

6. 发明申请

US20100003203A1 METHOD OF PRODUCING SURFACE-MODIFIED NANOPARTICULATE METAL OXIDES, METAL HYDROXIDES AND/OR METAL OXYHYDROXIDES 审中-公开
标题翻译：生产表面改性的纳米材料金属氧化物，金属氢氧化物和/或金属氧化物的方法
公开(公告)号：US20100003203A1
公开(公告)日：2010-01-07
申请号：US12445166
申请日：2007-10-10
申请人： Andrey Karpov , Hartmut Hibst , Jutta Kissel , Bernd Bechtloff , Hartwig Voss , Kerstin Schierle-Arndt , Valerie Andre
发明人： Andrey Karpov , Hartmut Hibst , Jutta Kissel , Bernd Bechtloff , Hartwig Voss , Kerstin Schierle-Arndt , Valerie Andre
IPC分类号： A61K8/19 , A01N59/00 , A01N59/20 , A01N59/16 , C08K3/22 , A61Q17/04 , C01F7/02 , C01F5/02 , C01F5/14 , C01F17/00 , C01G49/02 , C01G45/02 , C01G53/04 , C01G51/04 , C01G3/02 , C01G25/02 , C01G23/04 , C01G9/02
CPC分类号： C09C1/043 , A61K8/0241 , A61K8/27 , A61K8/86 , A61K2800/614 , A61Q17/04 , B82Y30/00 , C01G1/02 , C01G3/02 , C01G9/02 , C01G23/053 , C01G25/02 , C01G45/02 , C01G49/02 , C01G51/04 , C01G53/04 , C01P2004/64
摘要： The present invention relates to methods of producing surface-modified nanoparticulate particles at least of one metal oxide, metal hydroxide and/or metal oxide hydroxide, and aqueous suspensions of these particles. The invention further relates to the surface-modified nanoparticulate particles, obtainable by these methods, at least of one metal oxide, metal hydroxide and/or metal oxide hydroxide and aqueous suspensions of these particles, and to their use for cosmetic sunscreen preparations, as stabilizer in plastics and as antimicrobial active ingredient.
摘要翻译：本发明涉及至少形成一种金属氧化物，金属氢氧化物和/或金属氢氧化物的表面改性纳米颗粒颗粒和这些颗粒的水悬浮液的方法。本发明还涉及通过这些方法可获得的至少一种金属氧化物，金属氢氧化物和/或金属氧化物氢氧化物和这些颗粒的水性悬浮液的表面改性的纳米颗粒颗粒，以及它们用于化妆品防晒制剂作为稳定剂的用途在塑料中作为抗微生物活性成分。

7. 发明授权

US07595424B2 Method for producing aromatic amines or aliphatic amino alcohols 失效
标题翻译：芳胺或脂族氨基醇的制备方法
公开(公告)号：US07595424B2
公开(公告)日：2009-09-29
申请号：US11816658
申请日：2006-02-22
申请人： Dominic Vanoppen , Frederik Van Laar , Thomas Beuermann , Georg Krug , Steffen Oehlenschlaeger , Ekkehard Schwab , Hartwig Voss , Konrad Morgenschweis , Ulrich Penzel , Dietrich Tittelbach-Helmrich
发明人： Dominic Vanoppen , Frederik Van Laar , Thomas Beuermann , Georg Krug , Steffen Oehlenschlaeger , Ekkehard Schwab , Hartwig Voss , Konrad Morgenschweis , Ulrich Penzel , Dietrich Tittelbach-Helmrich
IPC分类号： C07C209/36
CPC分类号： B01J19/0033 , B01J8/006 , B01J8/007 , B01J8/22 , B01J19/002 , B01J2208/00637 , B01J2219/002 , B01J2219/00225 , B01J2219/00263 , C07C209/36 , G01N21/31 , C07C211/51
摘要： The invention relates to a process for preparing aromatic amines by hydrogenation of nitroaromatics in the presence of catalysts, in which a fluid reaction mixture which comprises amines and from which the catalysts are separated off is formed in a reactor. After the catalysts have been separated off, a measurement of the absorption of UV/VIS radiation by the reaction mixture is carried out to determine the concentration of nitro and nitroso compounds in the reaction mixture.
摘要翻译：本发明涉及通过在催化剂存在下氢化硝基芳族化合物来制备芳族胺的方法，其中在反应器中形成包含胺并在其中分离催化剂的流体反应混合物。催化剂分离后，进行反应混合物对UV / VIS辐射吸收的测定，以确定反应混合物中硝基和亚硝基化合物的浓度。

8. 发明申请

US20080047427A1 Membrane Production Method 有权
标题翻译：膜生产方法
公开(公告)号：US20080047427A1
公开(公告)日：2008-02-28
申请号：US10585719
申请日：2005-01-13
申请人： Stefan Bitterlich , Hartwig Voss , Gunter Schuch , Armin Diefenbacher , Manfred Noack , Ronald Schaefer , Ingolf Voigt , Hannes Richter , Juergen Caro
发明人： Stefan Bitterlich , Hartwig Voss , Gunter Schuch , Armin Diefenbacher , Manfred Noack , Ronald Schaefer , Ingolf Voigt , Hannes Richter , Juergen Caro
IPC分类号： B05D5/00 , B01D53/22
CPC分类号： B01D69/10 , B01D67/0051 , B01D71/024 , B01D71/028 , B01D2323/10 , Y10S55/05
摘要： A process for the production of membranes which contain at least one solid layer on one side of a porous substrate by treating, with a synthesis solution forming the solid layer, that side of the substrate which is to be coated is described, wherein, in the production of the solid layer on the porous substrate, the space which, viewed from the substrate, is behind that side of the porous substrate which is not to be coated is filled with an inert fluid, the pressure and/or the temperature of the fluid being chosen so that contact of the synthesis solution with that side of the porous substrate which is not to be coated is substantially prevented.
摘要翻译：一种制备膜的方法，其通过用形成固体层的合成溶液处理待涂覆的基材的侧面来描述在多孔基材的一侧上含有至少一个固体层，其中在在多孔基材上生产固体层，从基材观察到的未被涂覆的多孔基材的该侧后面的空间填充有惰性流体，流体的压力和/或温度被选择为使得合成溶液与不被涂覆的多孔基材的那一侧的接触被基本上防止。

9. 发明申请

US20070232795A1 Method For Producing A Liquid Formulation Of Salts Of Sulphonic-Acid Azo Dyes 有权
标题翻译：制备磺酸偶氮染料盐液的方法
公开(公告)号：US20070232795A1
公开(公告)日：2007-10-04
申请号：US11569263
申请日：2005-05-18
申请人： Gunter-Rudolf Schroder , Jurgen Decker , Helmut Reichelt , Ingo Klopp , Armin Diefenbacher , Hartwig Voss
发明人： Gunter-Rudolf Schroder , Jurgen Decker , Helmut Reichelt , Ingo Klopp , Armin Diefenbacher , Hartwig Voss
IPC分类号： C07C309/13
CPC分类号： C09B67/0073 , C09B35/38 , C09B35/42 , C09B35/52 , C09B37/00 , C09B67/0096
摘要： A process for producing a liquid formulation of salts of sulfonated azo dyes by coupling an at least equimolar amount of diazotized aminoarylsulfonic acids I H2N—Ar—SO3H (I), where Ar is phenylene (which may be monosubstituted by sulfo) or naphthylene (which may be mono- or disubstituted by sulfo and/or monosubstituted by hydroxyl) onto the coupling product of an unsubstituted or methyl-substituted phenylenediamine with itself comprises dissolving the azo dye in a basic medium and then subjecting the solution to a nanofiltration.
摘要翻译：通过偶联至少等摩尔量的重氮化氨基芳基磺酸I <βin-line-formula description =“In-Line Formulas”end =“lead”→> H 2 N-Ar-SO 3 H（I），<β在线公式描述=“在线式”末端=“尾”→其中Ar是亚苯基（其可以被磺基单取代）或亚萘基（其可以被磺基和/或被羟基单取代单取代或被二取代）到未取代或甲基取代的苯二胺与其本身的偶联产物上，包括将偶氮染料溶解在碱性介质然后对该溶液进行纳滤。

10. 发明申请

US20070137485A1 Composite membrane 有权
标题翻译：复合膜
公开(公告)号：US20070137485A1
公开(公告)日：2007-06-21
申请号：US10585703
申请日：2005-01-05
申请人： Stefan Bitterlich , Hartwig Voss , Gunter Schuch , Armin Diefenbacher , Manfred Noack , Ronald Shafer , Ingolf Voigt , Hannes Richter , Jungen Caro
发明人： Stefan Bitterlich , Hartwig Voss , Gunter Schuch , Armin Diefenbacher , Manfred Noack , Ronald Shafer , Ingolf Voigt , Hannes Richter , Jungen Caro
IPC分类号： B01J20/28 , B01J29/04 , B01J29/00 , C01B39/00 , B01J20/00 , B01D53/22
CPC分类号： B01D71/028 , B01D53/228 , B01D67/0051 , B01D69/12 , B01D2323/08 , B01D2325/24 , C07C7/144 , C07C11/08
摘要： Composite membranes comprising at least one porous substrate layer and at least one microporous separation layer, comprising at least one zeolite of the MFI type, are described, the separation layer being produced by a hydrothermal synthesis in which the molar ratio of silicon to aluminum is greater than 120 and the separation layer contains less than 10% by weight of aluminum in elemental or chemically bound form in a zone of at least 100 nm adjacent to the separation layer.
摘要翻译：描述了包含至少一个多孔基材层和至少一个微孔分离层的复合膜，该至少一个微孔分离层包含至少一种MFI型沸石，该分离层是通过其中硅与铝的摩尔比更大的水热合成产生的并且分离层在与分离层相邻的至少100nm的区域中以元素或化学键合的形式含有小于10重量％的铝。

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