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1. 发明申请

US20190100486A1 METHOD AND CATALYST FOR PREPARING ANILINE COMPOUNDS AND USE THEREOF 审中-公开
公开(公告)号：US20190100486A1
公开(公告)日：2019-04-04
申请号：US16142369
申请日：2018-09-26
申请人： Seasons Biotechnology (Taizhou) Co., Ltd.
发明人： Qiang JIA , Chi MA , Tianhua MA , Zhengwei YANG
IPC分类号： C07C209/36 , C07C213/02 , C07C319/20 , C07C253/30 , C07D295/135 , B01J21/18 , B01J23/28
CPC分类号： C07C209/36 , B01J21/18 , B01J23/28 , C07C209/365 , C07C213/02 , C07C253/30 , C07C319/20 , C07D295/135 , C07C211/46 , C07C211/47 , C07C211/52 , C07C217/84 , C07C323/37 , C07C255/58 , C07C255/59
摘要： The present invention provides a method for preparing aniline compounds, and also provides a kind of catalyst and use thereof. This method for synthesizing an aniline compound in the invention includes following steps: use molybdenum oxide and activated carbon as catalyst, hydrazine hydrate as reducing agent, then reduce aromatic nitro compounds to aniline compounds. This method is green and high efficiency, and easy to be applied in industry.

2. 发明申请

US20180186732A1 METHOD FOR PRODUCING 4-(TRIFLUOROMETHYLSULFONYL)PHENOL COMPOUND 审中-公开
公开(公告)号：US20180186732A1
公开(公告)日：2018-07-05
申请号：US15737492
申请日：2016-07-19
申请人： SUMITOMO CHEMICAL COMPANY, LIMITED
发明人： Yuta HONDA , Yohei TANAKA , Kazuya UEKI
IPC分类号： C07C315/02 , C07C315/04 , C07C317/22 , C07C317/36 , C07C209/36 , C07C201/08
CPC分类号： C07C315/02 , C07C53/128 , C07C201/08 , C07C209/36 , C07C315/04 , C07C317/22 , C07C317/36 , C07C2523/42
摘要： A compound represented by formula (4): can be produced by adding a heterogeneous transition metal catalyst to a solution containing a compound represented by formula (3): obtained by performing a nitration reaction by adding a nitrating agent to a solution containing a compound represented by formula (2): obtained by oxidizing a compound represented by formula (1): with hydrogen peroxide in the presence of sodium tungstate and a saturated C8 carboxylic acid, then adding water to the resultant mixture, and separating the resultant solution.

3. 发明授权

US09676622B2 Process for producing hydrogen or heavy hydrogens, and hydrogenation (protiation, deuteration or tritiation) of organic compounds using same 有权
公开(公告)号：US09676622B2
公开(公告)日：2017-06-13
申请号：US14459673
申请日：2014-08-14
申请人： Shiono Chemical Co., Ltd.
发明人： Hironao Sajiki , Yasunari Monguchi , Yoshinari Sawama , Shinichi Kondo
IPC分类号： C01B3/10 , C01B3/08 , C01B4/00 , C07B31/00 , C07B35/02 , C07B35/06 , C07B59/00 , C07C1/26 , C07C5/09 , C07C5/10 , C07C29/143 , C07C29/17 , C07C41/20 , C07C41/24 , C07C41/26 , C07C45/61 , C07C209/36 , C07C213/02 , C07C221/00
CPC分类号： C01B3/10 , C01B3/08 , C01B4/00 , C01B2203/0277 , C01B2203/1047 , C01B2203/1064 , C07B31/00 , C07B35/02 , C07B35/06 , C07B59/00 , C07B2200/05 , C07C1/26 , C07C5/09 , C07C5/10 , C07C29/143 , C07C29/17 , C07C41/20 , C07C41/24 , C07C41/26 , C07C45/61 , C07C209/36 , C07C213/02 , C07C221/00 , C07C2523/745 , C07C2601/14 , Y02E60/364 , C07C215/68 , C07C211/58 , C07C217/84 , C07C225/22 , C07C33/20 , C07C43/2055 , C07C33/22 , C07C43/205 , C07C43/23 , C07C49/807 , C07C15/18 , C07C13/28 , C07C15/24 , C07C15/52 , C07C9/15
摘要： An object is to provide a process for providing hydrogen or heavy hydrogens conveniently without the necessity of large-scale equipment and a process capable of performing hydrogenation (protiation, deuteration or tritiation) reaction conveniently without the use of an expensive reagent and a special catalyst. The production process includes a process for producing hydrogen or heavy hydrogens, containing subjecting water or heavy water to mechanochemical reaction in the presence of a catalyst metal, and a process for producing a hydrogenated (protiated, deuterated or tritiated) organic compound, containing subjecting an organic compound and water or heavy water to mechanochemical reaction in the presence of a catalyst metal.

4. 发明申请

US20170128927A1 METHOD FOR SELF-REGULATION OF A SYSTEM 审中-公开
公开(公告)号：US20170128927A1
公开(公告)日：2017-05-11
申请号：US15321993
申请日：2015-06-23
申请人： BASF SE
发明人： Dominik GARELLA , Viviana SILVA , Tobias LANG , Javier GARCIA PALACIOS
IPC分类号： B01J35/00 , B01J8/00 , B01J8/02 , C07C209/36 , B01J8/18 , B01J8/08 , B01J23/00 , B01J23/755 , B01J8/42
CPC分类号： B01J35/0033 , B01J8/001 , B01J8/0285 , B01J8/082 , B01J8/087 , B01J8/1809 , B01J8/1836 , B01J8/42 , B01J19/087 , B01J23/002 , B01J23/755 , B01J37/0036 , B01J37/03 , B01J37/04 , B01J37/088 , B01J2208/00017 , B01J2208/00663 , B01J2208/065 , B01J2219/0801 , B01J2219/085 , B01J2219/0871 , B01J2219/0892 , B01J2523/00 , C07C209/36 , B01J2523/17 , B01J2523/842 , B01J2523/847
摘要： The invention relates to a method for self-regulation of a system comprising the steps of: (I) utilizing a magnetic field to transport magnetizable and/or magnetic particles out of a control volume or to localize said particles in the control volume, (II) changing magnetic properties of the magnetizable and/or magnetic particles, which are ferromagnetic or paramagnetic, in the control volume by changing a temperature Tp of the magnetizable and/or magnetic particles or by changing the composition of the magnetizable and/or magnetic particles.

5. 发明授权

US09512103B2 Synthesis of thiohydantoins 有权
公开(公告)号：US09512103B2
公开(公告)日：2016-12-06
申请号：US14666933
申请日：2015-03-24
申请人： Sloan-Kettering Institute for Cancer Research
发明人： Ouathek Ouerfelli , Anna Dilhas , Guangbin Yang , Hong Zhao
IPC分类号： C07C255/46 , C07D401/04 , C07C209/36 , C07C213/08 , C07C253/00 , C07C253/30 , C07D213/61 , C07D213/64 , C07D213/72 , C07D213/74 , C07D213/84 , C07C231/12
CPC分类号： C07D401/04 , C07C209/36 , C07C213/08 , C07C227/18 , C07C231/12 , C07C253/00 , C07C253/30 , C07C2601/04 , C07D213/61 , C07D213/64 , C07D213/643 , C07D213/72 , C07D213/74 , C07D213/76 , C07D213/84 , C07C211/52 , C07C217/58 , C07C255/46
摘要： A novel synthesis of the anti-androgen, A52, which has been found to be useful in the treatment of prostate cancer, is provided. A52 as well as structurally related analogs may be prepared via the inventive route. This new synthetic scheme may be used to prepare kilogram scale quantities of pure A52.

6. 发明授权

US09469594B2 Method for stopping a reaction during the production of aromatic amines from nitroaromatics 有权
标题翻译：在硝基芳族化合物生产芳香胺期间停止反应的方法
公开(公告)号：US09469594B2
公开(公告)日：2016-10-18
申请号：US14394142
申请日：2013-04-12
申请人： Bayer MaterialScience AG
发明人： Michael Merkel , Thomas Knauf , Cliff Andre Peters , Thorsten Schmidt , Karl-Heinz Wilke
IPC分类号： C07C209/36 , C07C209/84
CPC分类号： C07C209/36 , C07C209/84 , C07C211/46 , C07C211/47
摘要： The present invention relates to a method for producing aromatic amines by the hydrogenation of aromatic nitro compounds. This method supplies aromatic nitro compounds and hydrogen to a reactor and contacts them with a hydrogenation catalyst; and stops the supply of aromatic nitro compounds and hydrogen to the reactor. The supply of aromatic nitro compounds and hydrogen to the reactor is stopped to ensure safe shutdown of the reactor.
摘要翻译：本发明涉及通过芳族硝基化合物的氢化生产芳族胺的方法。该方法将芳香族硝基化合物和氢气供给反应器，并与氢化催化剂接触; 并停止向反应器供应芳族硝基化合物和氢气。停止向反应器供应芳族硝基化合物和氢气，以确保反应器的安全关闭。

7. 发明授权

US09447021B2 Process for the purification of aniline from gas phase hydrogenations 有权
标题翻译：从气相氢化中纯化苯胺的方法
公开(公告)号：US09447021B2
公开(公告)日：2016-09-20
申请号：US14385822
申请日：2013-03-18
申请人： Bayer Intellectual Property GmbH
发明人： Michael Merkel , Peter Lehner , Bastian Mahr , Amgad Salah Moussa
IPC分类号： C07C209/84 , C07C209/36
CPC分类号： C07C209/84 , C07C209/36 , C07C211/46
摘要： The present invention relates to a process for the purification of aniline which originates from gas phase hydrogenations. In this process, only a minimum proportion of the aniline has to be evaporated and condensed again. The process is highly efficient in removing compounds which have phenolic hydroxyl groups and results in minimal losses of aniline. This process also reduces the unwanted coupling mechanisms in the division of the overall crude product in the fraction condensation into individual substreams and the subsequent workup of these.
摘要翻译：本发明涉及一种源自气相氢化的苯胺的纯化方法。在这个过程中，只有最小比例的苯胺必须再次蒸发和冷凝。该方法在除去具有酚羟基并且导致苯胺损失最小的化合物中是高效的。该过程还减少了将馏分冷凝中的总体粗产物分成单独的子流体中的不期望的偶联机理以及随后的这些处理。

8. 发明授权

US09308515B2 Optimized introduction of the starting materials for a process for preparing aromatic amines by hydrogenation of nitroaromatics 有权
标题翻译：通过硝基芳族化合物的氢化优化引入用于制备芳族胺的方法的原料
公开(公告)号：US09308515B2
公开(公告)日：2016-04-12
申请号：US14330281
申请日：2014-07-14
申请人： BASF SE
发明人： Gerrit Waters , Johannes Buettner , Andreas Raichle , Markus Hiller , Peter Renze , Michael Herrich , Helmut Rueger , Burkhard Hantel , Arndt Hofmann , Ruediger Fritz , Kathrin Richter , Holgar Braunsberg , Lothar Bruntsch
IPC分类号： B01J19/26 , C07C209/36 , B01J8/22
CPC分类号： B01J19/26 , B01J8/226 , B01J8/228 , B01J2208/00123 , B01J2208/00132 , B01J2208/00141 , B01J2208/0015 , B01J2208/00902 , B01J2208/00911 , B01J2219/00761 , C07C209/36 , C07C211/50
摘要： The invention relates to a process for preparing aromatic amines by hydrogenation of corresponding nitroaromatics by means of hydrogen, and also an apparatus suitable for this purpose. In particular, the invention relates to a process for preparing toluenediamine (TDA) by hydrogenation of dinitrotoluene (DNT).
摘要翻译：本发明涉及通过氢气对相应的硝基芳族化合物进行氢化制备芳族胺的方法，以及适用于该目的的装置。特别地，本发明涉及通过氢化二硝基甲苯（DNT）制备甲苯二胺（TDA）的方法。

9. 发明授权

US09260581B2 Multifunctional porous aramids (aerogels) and fabrication thereof 有权
标题翻译：多功能多孔芳族聚酰胺（气凝胶）及其制造
公开(公告)号：US09260581B2
公开(公告)日：2016-02-16
申请号：US14529823
申请日：2014-10-31
申请人： The Curators of the University of Missouri
发明人： Nicholas Leventis , Chariklia Sotiriou-Leventis , Malik Adnan Saeed
IPC分类号： B01J13/00 , C08J9/28 , C01B31/30 , B01J27/22 , C07C209/36 , C07C45/38 , C07C67/10 , C07C2/86
CPC分类号： C08J9/286 , B01J13/0091 , B01J27/22 , C01B31/301 , C01B32/907 , C07C2/861 , C07C45/38 , C07C67/10 , C07C209/36 , C07C2531/28 , C08J2201/0502 , C08J2205/026 , C08J2377/00
摘要： The present disclosure provides a series of new and improved porous polyamide aerogels derived from multifunctional aromatics that combine the high mechanical strength of aramids with the pore structure of aerogels. The polyamide aerogels have a hyperbranched structure, relatively low density, high porosity and may be derived from functionalized monomers having more aromatic groups than functional groups. The present disclosure also provides a new method for producing the porous polyamide aerogels by polymerizing an aromatic multifunctional carboxylic acid or a ferrocene multifunctional carboxylic acid with a polyfunctional aromatic isocyanate at moderate reaction conditions followed by drying with liquid CO2. Also disclosed are various methods of use of these polyamide aerogels in a variety of applications.
摘要翻译：本公开提供了一系列新的和改进的多功能芳烃衍生的多孔聚酰胺气凝胶，其将芳族聚酰胺的高机械强度与气凝胶的孔结构相结合。聚酰胺气凝胶具有超支化结构，相对低密度，高孔隙率，并且可以衍生自具有比官能团更多的芳族基团的官能化单体。本公开还提供了一种通过在中等反应条件下将芳族多官能羧酸或二茂铁多官能羧酸与多官能芳族异氰酸酯聚合并随后用液体CO 2干燥来生产多孔聚酰胺气凝胶的新方法。还公开了这些聚酰胺气凝胶在各种应用中的各种使用方法。

10. 发明授权

US09115049B2 Process for obtaining pure aniline 有权
标题翻译：获得纯苯胺的方法
公开(公告)号：US09115049B2
公开(公告)日：2015-08-25
申请号：US14045940
申请日：2013-10-04
申请人： BASF SE
发明人： Koenraad Vandewalle , Karen Vercruysse , Leo Denissen , Filip Deberdt , Hendrik De Winne , Bart Van De Voorde , Michael Reiser , Samuel Neto
IPC分类号： C07C209/00 , C07C209/36 , C07C209/84
CPC分类号： C07C209/36 , C07C209/84 , C07C211/46
摘要： A process for obtaining pure aniline contains catalytically hydrogenating nitrobenzene, to obtain a reaction mixture, separating the reaction mixture into a gas phase containing hydrogen and a liquid phase, liquid/liquid phase separating the liquid phase to obtain an aqueous phase and also crude aniline containing water as an organic phase, distillatively pre-purifying the crude aniline by removing the water via an overhead stream of a first distillation column to obtain a first bottom stream, feeding the first bottom stream as a feed stream to a pure column from which a pure aniline stream is taken off at the top and a second bottom stream containing high boilers is taken off, and passing the second bottom stream to incineration, by pumping the second bottom stream through heated pipelines and by adding methanol, ethanol, propanol, and/or acetone to the second bottom stream.
摘要翻译：获得纯苯胺的方法含有催化氢化硝基苯，得到反应混合物，将反应混合物分离成含有氢和液相的气相，液/液相分离液相，得到含水相和粗苯胺水作为有机相，通过经由第一蒸馏塔的塔顶流除去水来蒸馏预纯化粗苯胺，以获得第一底部料流，将第一底部料流作为进料流进料至纯的塔，纯纯将苯胺流从顶部取出，取出含有高锅炉的第二塔底物流，并将第二塔底物流通过加热的管道，并通过加入甲醇，乙醇，丙醇和/或丙酮到第二个底部流。

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