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    • 1. 发明申请
    • COMPOUND MONOCRYSTAL MANUFACTURING METHOD AND APPARATUS
    • 复合单晶制造方法和装置
    • WO1995033873A1
    • 1995-12-14
    • PCT/JP1995001069
    • 1995-06-01
    • KABUSHIKI KAISHA KOBE SEIKO SHOFUJIKAWA, TakaoUEHARA, KazuhiroSAKASHITA, YoshihikoSUZUKI, KazuyaOKADA, HiroshiKAWANAKA, TakaoOOMOTO, Seiichiro
    • KABUSHIKI KAISHA KOBE SEIKO SHO
    • C30B11/06
    • C30B11/00C30B29/48Y10T117/102
    • The manufacturing method according to the present invention has the steps of thermally melting a raw material in a raw material storage container (14), which is provided on the inner side of heating means (3a), by these heating means (3a) provided in a furnace casing (1), and then cooling and solidifying a molten liquid (62) of the raw material from the lower side thereof to grow a monocrystal (61), and is characterized in that a non-gas-permeable air-tight chamber (4) surrounding the raw material storage container (14) on the inner side of the heating means (3a) is provided, a uniform pressure passage (10) allowing the interior and exterior of the air-tight chamber (4) to communicate with each other being formed in the portion of the air-tight chamber (4) which is downwardly away from the heating means (3a) to surround the raw material storage container (14) with this air-tight chamber (4), a region of the uniform pressure passage (10) being maintained in a low temperature condition of not higher than a melting point of a high dissociation pressure component of the raw material, whereby the raw material in the container (14) is heated to grow a monocrystal.
    • 根据本发明的制造方法具有如下步骤:通过这些加热装置(3a)设置在加热装置(3a)的内侧的原料储存容器(14)中的原料热熔融 炉壳(1),然后从原料的下侧冷却固化原料的熔融液(62),生长单晶(61),其特征在于,不透气的气密室 (4)围绕加热装置(3a)的内侧的原料储存容器(14)设置有均匀的压力通道(10),其允许气密室(4)的内部和外部与 彼此形成在气密室(4)的向下远离加热装置(3a)的部分中,以与该气密室(4)包围原料储存容器(14),区域 均匀的压力通道(10)保持在低温条件o f不高于原料的高解离压成分的熔点,由此容器(14)中的原料被加热以生长单晶。
    • 9. 发明申请
    • PYRIDAZINONE DERIVATIVES OR THEIR SALTS, PROCESSES FOR THEIR PRODUCTION, AND ANTI-SHOCK AGENTS CONTAINING THEM
    • 吡咯烷酮衍生物或其生产商,其生产工艺和包含它们的抗震剂
    • WO1995007264A1
    • 1995-03-16
    • PCT/JP1994001380
    • 1994-08-22
    • ISHIHARA SANGYO KAISHA LTD.SHIGEHARA, ItaruODAWARA, ShinjiOKADA, HiroshiKIMURA, HirohikoOMATSU, MasatoNAKAYAMA, HitoshiHIGUCHI, RieTAKENAMI, Taki
    • ISHIHARA SANGYO KAISHA LTD.
    • C07D237/24
    • C07D401/12C07D237/14C07D237/24C07D405/14C07D417/12
    • A pyridazinone derivative of formula (I) or a pharmaceutically acceptable salt thereof, wherein Q is -CH2- or -CO-, A is a furanyl group which may be substituted, a thienyl group which may be substituted, a pyridyl group which may be substituted, a pyridyl N-oxide group which may be substituted, a thiazolyl group which may be substituted, or a phenyl group which may be substituted, R is a hydrogen atom, an alkyl group which may be substituted, an alkenyl group which may be substituted, an alkynyl group which may be substituted, or a phenyl group which may be substituted, R is a hydrogen atom, a cyano group, an alkyl group which may be substituted, a hydroxyl group, an alkoxy group, a dioxanyl group which may be substituted by an alkyl group, -CH=N-R , -S(O)nR , -N(R )R , or -COR , R is a hydrogen atom, a cyano group, a nitro group, an alkoxy group, a carboxyl group or an alkoxycarbonyl group, R is a hydrogen atom, or an alkyl group which may be substituted, R is an alkoxy group, or a pyridylmethyl group, R is an alkyl group which may be substituted, or an alkenyl group, each of R and R independently is a hydrogen atom, an alkyl group, an alkylsulfonyl group, a phenylsulfonyl group which may be substituted, a formyl group, an alkylcarbonyl group which may be substituted by a halogen atom, a cycloalkylcarbonyl group, or a benzoyl group which may be substituted, R is a hydrogen atom, an alkoxy group, a hydroxyl group, or an amino group which may be substituted, n is 0, 1 or 2, provided that when R is a hydrogen atom, an alkyl group or an alkoxy group, and Q is -CH2-, A is a furanyl group which may be substituted, a thienyl group which may be substituted, a pyridyl group which may be substituted, a pyridyl N-oxide group which may be substituted, or a thiazolyl group which may be substituted.
    • 式(I)的哒嗪酮衍生物或其药学上可接受的盐,其中Q是-CH2-或-CO-,A是可被取代的呋喃基,可被取代的噻吩基,可以是 取代的,可被取代的吡啶基N-氧化物基团,可被取代的噻唑基或可被取代的苯基,R 1是氢原子,可被取代的烷基,烯基 可以被取代的炔基,可被取代的炔基或可被取代的苯基,R 2是氢原子,氰基,可被取代的烷基,羟基,烷氧基 ,可被烷基取代的二烷基,-CH = NR 5,-S(O)n R 6,-N(R 7)R 8或-COR 9 R 3为氢原子,氰基,硝基,烷氧基,羧基或烷氧基羰基,R 4为氢原子或可被取代的烷基, 5>我 是烷氧基或吡啶基甲基,R 6是可以被取代的烷基或链烯基,R 7和R 8各自独立地是氢原子,烷基, 烷基磺酰基,可被取代的苯基磺酰基,甲酰基,可以被卤素原子取代的烷基羰基,环烷基羰基或可被取代的苯甲酰基,R 9是氢原子, 烷氧基,羟基或可被取代的氨基,n为0,1或2,条件是当R 2为氢原子,烷基或烷氧基时,Q为-CH 2 - A是可以被取代的呋喃基,可以被取代的噻吩基,可以被取代的吡啶基,可以被取代的吡啶基N-氧化物基或可以被取代的噻唑基。