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    • 42. 发明公开
    • Measurement and endpointing of sample thickness
    • Messung der Probendicke und Endpunkbestimmung
    • EP2367195A2
    • 2011-09-21
    • EP11165381.2
    • 2009-11-02
    • FEI Company
    • Young, RichardPeterson, BrennanMoriarty, MichaelSchampers, Ruud
    • H01J37/304H01J37/305G01N1/28
    • H01J37/3056G01N1/286H01J37/304H01J2237/24455H01J2237/30466H01J2237/31745H01J2237/31749
    • An improved method for TEM sample creation. The use of a SEM-STEM detector in the dual-beam FIB/SEM allows a sample to be thinned using the FIB, while the STEM signal is used to monitor sample thickness. A preferred embodiment of the present invention can measure the thickness of or create S/TEM samples by using a precise endpoint detection method that is reproducible and suitable for automation. Preferred embodiments also enable automatic endpointing during TEM lamella creation and provide users with direct feedback on sample thickness during manual thinning. Preferred embodiments of the present invention thus provide improved methods for endpointing sample thinning and methods to partially or fully automate endpointing to increase throughput and reproducibility of TEM sample creation.
    • 一种改进的TEM样品创建方法。 在双光束FIB / SEM中使用SEM-STEM检测器允许使用FIB对样品进行稀释,而STEM信号用于监测样品厚度。 本发明的一个优选实施例可以通过使用可重复且适合自动化的精确终点检测方法来测量S / TEM样品的厚度或产生S / TEM样品。 优选实施例还可以在TEM薄片创建期间实现自动终点,并且在手动稀疏期间向用户提供关于样品厚度的直接反馈。 因此,本发明的优选实施例提供了用于终止样品稀释的改进方法以及部分或全部自动化终点以提高TEM样品产生的生产量和再现性的方法。
    • 47. 发明公开
    • Method and apparatus for preparing specimen
    • Verfahren und Vorrichtung zur Herstellung von Proben
    • EP1732102A2
    • 2006-12-13
    • EP06252156.2
    • 2006-04-21
    • JEOL Ltd.
    • Yoshioka, TadanoriKawatsu, KiyoshiMiyao, Hirofumi
    • H01J37/304H01J37/305G01N1/28
    • G01N1/32H01J37/304H01J37/3056H01J2237/30466H01J2237/3174
    • A method and apparatus for reliably preparing a good thin-film specimen (3) adapted for TEM (transmission electron microscopy) observation is offered. The apparatus has a high-brightness pixel extraction unit (10) for extracting high-brightness pixels (P nm ) which form a specimen image taken by an imaging unit (8) and which have intensities becoming greater than a given threshold value as the specimen is thinned. The apparatus further includes a decision unit (11) that makes a decision as to whether the high-brightness pixels extracted by the high-brightness pixel extraction unit form a continuous sequence of pixels whose number is in excess of a given number on the specimen image. If the decision is affirmative, the decision unit sends a signal to an ion gun control unit (12) to stop the ion-beam irradiation of the specimen.
    • 提供了一种用于可靠地制备适用于TEM(透射电子显微镜)观察的良好薄膜试样(3)的方法和装置。 该装置具有高亮度像素提取单元(10),用于提取形成由成像单元(8)拍摄的样本图像并且具有大于给定阈值的强度的高亮度像素(Pnm),作为样本 变薄了 该装置还包括判定单元(11),判定由高亮度像素提取单元提取的高亮度像素是否在样本图像上形成数量超过给定数量的连续的像素序列 。 如果判定为肯定,判定单元向离子枪控制单元(12)发送信号,停止对样本的离子束照射。
    • 49. 发明公开
    • Method for making specimen and apparatus thereof
    • Verfahren und Vorrichtung zur Probenherstellung
    • EP0687897A1
    • 1995-12-20
    • EP95109035.6
    • 1995-06-12
    • HITACHI, LTD.
    • Itoh, FumikazuNakata, ToshihikoIshitani, TohruShimase, AkiraYamaguchi, HiroshiKamimura, Takashi
    • G01N1/00H01J37/304
    • H01J37/3056G01N1/32H01J37/226H01J37/3005H01J37/304H01J2237/30466H01J2237/3114H01J2237/31745
    • The present invention is intended to provide a method and an apparatus for making a specimen for use in observation through a transparent electron microscope, including a step for milling part of the specimen into a thin film part, which can be observed through a transparent electron microscope, by scanning and irradiating a focused ion beam onto the specimen, a step for observing a mark for detection of position provided on the specimen as a secondary charged particle image by scanning and irradiating a charged particle beam onto the specimen without irradiating the charged particle beam onto the portion to be milled into the thin film part during the step for milling, and a step for compensating positional drift of the focused ion beam during said step for milling in accordance with a result of the observation.
      The present invention provides an effect to strikingly raise the efficiency of TEM observation since a specimen for use in TEM observation can be made by precisely milling a thin film part of the specimen even though positional drift of the focused ion beam is caused during milling.
    • 本发明旨在提供一种通过透明电子显微镜制造用于观察的样本的方法和装置,包括将部分样品切成薄膜部分的步骤,其可以通过透明电子显微镜观察 通过将聚焦离子束扫描并照射到样本上,通过扫描并将带电粒子束照射到样本上而不照射带电粒子束来观察用于检测在样本上提供的位置的标记作为二次带电粒子图像的步骤 在用于研磨的步骤期间在待研磨到薄膜部分的部分上,以及根据观察结果在所述铣削步骤期间补偿聚焦离子束的位置漂移的步骤。 本发明提供了显着提高TEM观察效率的效果,因为即使在研磨中发生聚焦离子束的位置漂移,也可以通过精确地研磨试样的薄膜部分来进行TEM观察用的试样。