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    • 8. 发明公开
    • Method for making specimen and apparatus thereof
    • Verfahren und Vorrichtung zur Probenherstellung
    • EP0687897A1
    • 1995-12-20
    • EP95109035.6
    • 1995-06-12
    • HITACHI, LTD.
    • Itoh, FumikazuNakata, ToshihikoIshitani, TohruShimase, AkiraYamaguchi, HiroshiKamimura, Takashi
    • G01N1/00H01J37/304
    • H01J37/3056G01N1/32H01J37/226H01J37/3005H01J37/304H01J2237/30466H01J2237/3114H01J2237/31745
    • The present invention is intended to provide a method and an apparatus for making a specimen for use in observation through a transparent electron microscope, including a step for milling part of the specimen into a thin film part, which can be observed through a transparent electron microscope, by scanning and irradiating a focused ion beam onto the specimen, a step for observing a mark for detection of position provided on the specimen as a secondary charged particle image by scanning and irradiating a charged particle beam onto the specimen without irradiating the charged particle beam onto the portion to be milled into the thin film part during the step for milling, and a step for compensating positional drift of the focused ion beam during said step for milling in accordance with a result of the observation.
      The present invention provides an effect to strikingly raise the efficiency of TEM observation since a specimen for use in TEM observation can be made by precisely milling a thin film part of the specimen even though positional drift of the focused ion beam is caused during milling.
    • 本发明旨在提供一种通过透明电子显微镜制造用于观察的样本的方法和装置,包括将部分样品切成薄膜部分的步骤,其可以通过透明电子显微镜观察 通过将聚焦离子束扫描并照射到样本上,通过扫描并将带电粒子束照射到样本上而不照射带电粒子束来观察用于检测在样本上提供的位置的标记作为二次带电粒子图像的步骤 在用于研磨的步骤期间在待研磨到薄膜部分的部分上,以及根据观察结果在所述铣削步骤期间补偿聚焦离子束的位置漂移的步骤。 本发明提供了显着提高TEM观察效率的效果,因为即使在研磨中发生聚焦离子束的位置漂移,也可以通过精确地研磨试样的薄膜部分来进行TEM观察用的试样。