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    • 31. 发明公开
    • Method and device for controlling reactive sputtering deposition
    • Verfahren und Vorrichtung zur Steuerung reaktiver Sputterabscheidung
    • EP2881974A1
    • 2015-06-10
    • EP13197009.7
    • 2013-12-12
    • Institute of Solid State Physics, University of Latvia
    • Purans, Juris
    • H01J37/32C23C14/52G01N23/223H05H1/00H01J37/34
    • H01J37/32972C23C14/52G01N23/223G01N2223/638H01J37/32981H01J37/3405H05H1/005
    • The present invention relates to the methods and devices for controlling a reactive sputtering deposition of a selected material. The proposed device comprises: a vacuum chamber; a means for supplying of an inert and reactive gas into the vacuum chamber; a means adapted for providing a command to the means for supplying of an inert and/or reactive gas into the vacuum chamber; a source adapted for generating plasma and/or creating a flux of sputtered particles of material; a means adapted for holding or placing on it a substrate to be subjected to sputtering of a film of a selected material; an X-ray source adapted to expose a sputtering target by an X-ray beam; an X-ray fluorescence polycapillary confocal probe adapted to be placed inside of the vacuum chamber and comprising an X-ray optic, where the probe is adapted to collect the X-ray fluorescence signals from a part of the sputtering target and direct them to a signal detecting unit; an X-ray energy sensitive detector being optically connected with the polycapillary confocal probe such as to enable the X-ray optic to direct X-ray fluorescence beam towards the detector from the optic's input end facing the surface of the sputtering target; where the X-ray energy sensitive detector being connected at least with the means for processing the detected signals or interpreting the signals received on the state of oxidation of the target.
    • 本发明涉及用于控制所选材料的反应溅射沉积的方法和装置。 所提出的装置包括:真空室; 用于将惰性和反应性气体供应到真空室中的装置; 适于向惰性和/或反应性气体供应到真空室中的装置提供指令的装置; 适于产生等离子体和/或产生溅射的材料颗粒的流量的源; 适于将其放置在要被溅射所选材料的薄膜的基底上的装置; 适于通过X射线束曝光溅射靶的X射线源; X射线荧光多毛细共聚焦探针,其适于放置在真空室的内部并且包括X射线光学元件,其中探针适于从溅射靶的一部分收集X射线荧光信号并将其引导到 信号检测单元; X射线能量敏感检测器与多毛细共聚焦探针光学连接,以使X射线光学器件可以从面向溅射靶表面的光学器件输入端向检测器引导X射线荧光束; 其中X射线能量敏感检测器至少与用于处理检测到的信号的装置相连,或解释在目标氧化状态下接收的信号。