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1. 发明授权

US06214172B1 Preparation of methylglyoxal dimethyl acetal 失效
标题翻译：甲基乙二醛缩醛的制备
公开(公告)号：US06214172B1
公开(公告)日：2001-04-10
申请号：US08845556
申请日：1997-04-25
申请人： Carsten Gröning , Klaus Ebel , Gerd Kaibel , Jörg Therre , Jürgen Koopmann , Helmuth Menig , Gerhard Fritz , Rainer Dietz
发明人： Carsten Gröning , Klaus Ebel , Gerd Kaibel , Jörg Therre , Jürgen Koopmann , Helmuth Menig , Gerhard Fritz , Rainer Dietz
IPC分类号： B01D336
CPC分类号： C07C45/71 , C07C45/84 , Y02P20/582 , Y10S203/13 , C07C49/175
摘要： In a process for the preparation of methylglyoxal dimethyl acetal from methylglyoxal and methanol in the presence of an acidic ion exchanger, water is introduced in an amount sufficient to form an acidic reaction mixture in which the acetal product and water form an azeotropic mixture, with or without the retention of some methanol reactant. After subjecting a single phase acidic reaction mixture to an azeotropic distillation, it will separate into two distinct liquid phases with a simple recovery of the acetal product from the aqueous phase.
摘要翻译：在酸性离子交换剂存在下，从甲基乙二醛和甲醇制备甲基乙二醛缩二甲醇的方法中，以足以形成酸缩反应混合物的量引入水，其中缩醛产物和水形成共沸混合物，没有保留一些甲醇反应物。在使单相酸性反应混合物进行共沸蒸馏后，将从水相中简单回收缩醛产物，分离成两个不同的液相。

2. 发明授权

US06518464B2 Continuous process for the preparation of acetals 有权
公开(公告)号：US06518464B2
公开(公告)日：2003-02-11
申请号：US09945642
申请日：2001-09-05
申请人： Jörg Therre , Gerd Kaibel , Werner Aquila , Günter Wegner , Hartwig Fuchs
发明人： Jörg Therre , Gerd Kaibel , Werner Aquila , Günter Wegner , Hartwig Fuchs
IPC分类号： C07C4302
CPC分类号： C07C41/56 , C07C41/58 , C07C43/303
摘要： The present invention relates to a continuous process for the preparation of unsaturated acetals by reacting olefinically unsaturated aliphatic compounds with allyl alcohols in a reaction column, where the reactants are only partially reacted in the reaction column, the resulting acetal is concentrated in at least two successive evaporation stages, and the recovered reactants are returned to the reaction column.

3. 发明授权

US06175044B1 Preparation of citral 有权
标题翻译：柠檬醛的制备
公开(公告)号：US06175044B1
公开(公告)日：2001-01-16
申请号：US09404548
申请日：1999-09-24
申请人： Jörg Therre , Gerd Kaibel , Werner Aquila , G{umlaut over (u)}nter Wegner , Hartwig Fuchs
发明人： Jörg Therre , Gerd Kaibel , Werner Aquila , G{umlaut over (u)}nter Wegner , Hartwig Fuchs
IPC分类号： C07C4551
CPC分类号： C07C45/515 , C07C45/513 , C07C45/67 , C07C47/21
摘要： 3,7-Dimethyl-2,6-octadien-1-al of formula I is prepared continuously by: thermally cleaving, in the presence or absence of an acid catalyst, 3-methyl-2-buten-1-al diprenyl acetal of formula II: thereby eliminating 3-methyl-2-buten-1-ol of formula III and yielding cis/trans-prenyl 3-methylbutadienyl ether of formula IV: thermally rearranging the resultant butadienyl ether of formula IV thereby yielding 2,4,4-trimethyl-3-formyl-1,5-hexadiene of formula V: subsequently rearranging intermediate (V) thereby yielding citral product of formula I, which comprises: as the reaction proceeds, continuously distilling the reaction mixture thereby continuously removing prenol, which is formed by degradation of acetal II, and the intermediates of formula IV and V and any citral product which is formed during the reaction; and thermally rearranging said intermediates of formula IV and V at a temperature of 100-200° C. in the absence or presence of said prenol to form citral product.
摘要翻译：通过以下方式连续制备式I的3,7-二甲基-2,6-辛二烯-1-醇：在存在或不存在酸催化剂的情况下，热裂解3-甲基-2-丁烯-1-al阮内烯式II：由此除去式III的3-甲基-2-丁烯-1-醇，得到式IV的顺/反 - 异戊烯基3-甲基丁二烯基醚：热重新排列所得的式IV的丁二烯基醚，由此得到2,4,4 式V的 - 三甲基-3-甲酰基-1,5-己二烯：随后重新排列中间体（V），从而产生式I的柠檬醛产物，其包括：随着反应的进行，连续蒸馏反应混合物，从而连续除去前醇，由缩醛II的降解形成，以及式IV和V的中间体以及在反应期间形成的任何柠檬醛产物; 在不存在或存在所述prenol的情况下，在100-200℃的温度下热处理所述式IV和V的中间体，以形成柠檬醛产物。

4. 发明授权

US06723883B1 Continuous method for production of cinnamaldehyde and dihydrocinnamaldehyde derivatives 有权
标题翻译：连续生产肉桂醛和二氢肉桂醛衍生物的方法
公开(公告)号：US06723883B1
公开(公告)日：2004-04-20
申请号：US10110532
申请日：2002-04-15
申请人： Jörg Therre , Andreas Kramer , Andreas Weiper-Idelmann , Michael Schulik , Regina Benfer , Jürgen Schossig , Mathias Haake , Hans-Georg Göbbel
发明人： Jörg Therre , Andreas Kramer , Andreas Weiper-Idelmann , Michael Schulik , Regina Benfer , Jürgen Schossig , Mathias Haake , Hans-Georg Göbbel
IPC分类号： C07C4573
CPC分类号： C07C45/74 , C07C45/62 , C07C45/73 , C07C47/228 , C07C47/232
摘要： The present invention relates to a continuous process for the preparation of cinnamaldehyde or cinnamaldehyde derivatives by continuous reaction of benzaldehyde derivatives with alkanals in the presence of bases and optionally subsequent continuous hydrogenation in a circulation reactor in the presence of a suspension catalyst and hydrogen to give dihydrocinnamaldehyde derivatives.
摘要翻译：本发明涉及一种连续的制备肉桂醛或肉桂醛衍生物的方法，其通过在碱存在下苯甲醛衍生物与链烷烃的连续反应和任选地在循环反应器中在悬浮催化剂和氢存在下连续氢化得到二氢肉桂醛衍生品

5. 发明授权

US06180839B2 Continuous preparation of dimethylvinylcarbinol by isomerizing prenol 失效
标题翻译：通过异构化prenol连续制备二甲基乙烯基甲醇
公开(公告)号：US06180839B2
公开(公告)日：2001-01-30
申请号：US09265923
申请日：1999-03-10
申请人： Matthias Kiefer , Wolfgang Siegel , Jörg Therre , Melanie Pahl , Werner Aquila , Ulrich Sch{umlaut over (a)}fer-L{umlaut over (u)}derssen
发明人： Matthias Kiefer , Wolfgang Siegel , Jörg Therre , Melanie Pahl , Werner Aquila , Ulrich Sch{umlaut over (a)}fer-L{umlaut over (u)}derssen
IPC分类号： C07C2700
CPC分类号： C07C29/56 , C07C33/03
摘要： A process is described for the continuous preparation of dimethylvinylcarbinol (DMVC) by continuously reacting prenol with the aqueous solution of a protic acid in the still or in the lower part of a rectification column while distilling off the DMVC formed in the form of an azeotropic mixture with water, which comprises a) during the reaction ensuring that as far as possible no liquid two-phase mixture forms in the reaction mixture, b) distilling off the DMVC which forms at a reflux ratio of at least 2, as a result of which there is virtually no more prenol present in the distillate from the column, and c) setting the reaction volume and/or the amount of prenol added per hour and/or the concentration of protons in the reaction mixture in such a manner that the quotient, defined as residence time concentration coefficient, of the reaction volume and the volume of prenol added per hour multiplied by the concentration of protons in the reaction mixture has a value between 0.001 h·mol/l and 1 h·mol/l. In this connection, the formation of a liquid two-phase mixture in the reaction mixture is prevented, in addition to avoiding too large a prenol excess, by continuously taking from the reaction mixture a partial stream, passing it over a phase separation vessel, completely or at least largely removing there the small quantities, formed in the course of the reaction, of organic by-products which are insoluble or only partially soluble in water, and returning the aqueous phase to the reaction volume.
摘要翻译：描述了通过在精馏塔的静止或下部连续地反应预先醇与质子酸的水溶液连续反应制备二甲基乙烯基甲醇（DMVC）的方法，同时蒸馏出以共沸混合物形式形成的DMVC 在反应过程中包含a）的水，确保尽可能在反应混合物中形成液体两相混合物，b）蒸发形成回流比至少为2的DMVC，结果是在那里在柱的馏出物中基本上没有更多的prenol存在，并且c）使反应体积和/或每小时加入的prenol的量和/或反应混合物中的质子浓度设定为使得定义为停留时间浓度系数，反应体积和每小时加入的prenol体积乘以反应混合物中质子浓度的值为0.001 h.mol / l和 1 h.mol / l。在这方面，防止反应混合物中的液体两相混合物的形成，除了避免过多的过量的过量以外，通过连续取出反应混合物的一部分流，将其通过在相分离容器中，完全或至少大部分在反应过程中形成的少量去除不溶或仅部分溶于水的有机副产物，并将水相返回到反应体积中。

6. 发明授权

US08574344B2 Template-free clathrasils and clathrasil membranes 失效
标题翻译：无模板的垫圈和垫层膜
公开(公告)号：US08574344B2
公开(公告)日：2013-11-05
申请号：US13121839
申请日：2009-09-28
申请人： Hartwig Voβ , Jörg Therre , Hermann Gies , Bernd Marler
发明人： Hartwig Voβ , Jörg Therre , Hermann Gies , Bernd Marler
IPC分类号： B01D53/22 , B01D71/02 , C01B33/12 , C01B37/02
CPC分类号： B01D71/027 , B01D53/047 , B01D53/228 , B01D67/0039 , B01D67/0051 , B01D69/02 , B01D71/028 , B01D2253/106 , B01D2256/24 , B01D2257/108 , B01D2257/11 , B01D2257/406 , B01D2257/80 , B01D2323/08 , B01D2323/10 , C01B37/00 , C01B37/02 , C01B39/52
摘要： The present invention relates to template-free clathrasils whose framework comprises essentially SiO2, wherein the crystals of the clathrasils have the platelet-like morphology of a sheet silicate. The present invention further relates to a process for preparing these template-free clathrasils and also to their use as absorbent, as seed crystals for the synthesis of clathrasil membranes of the same zeolite type and in the form of dense layers which function as gas separation membranes having a molecular sieving action.
摘要翻译：本发明涉及无模板的层状砂浆，其框架基本上包含SiO 2，其中层状砂浆的晶体具有片状硅酸盐的片状形态。本发明还涉及一种制备这些无模板的层状蓝宝石的方法，并且还涉及它们作为吸收剂的用途，作为用于合成相同沸石型和作为气体分离膜的致密层形式的晶体的晶种具有分子筛选作用。

7. 发明申请

US20110197762A1 Template-Free Clathrasils And Clathrasil Membranes 失效
标题翻译：无模板的Clathrasils和Clathrasil膜
公开(公告)号：US20110197762A1
公开(公告)日：2011-08-18
申请号：US13121839
申请日：2009-09-28
申请人： Hartwig Voss , Jörg Therre , Hermann Gies , Bernd Marler
发明人： Hartwig Voss , Jörg Therre , Hermann Gies , Bernd Marler
IPC分类号： B01D53/22 , C01B33/12 , C01B39/02 , C01B37/02 , C30B7/10
CPC分类号： B01D71/027 , B01D53/047 , B01D53/228 , B01D67/0039 , B01D67/0051 , B01D69/02 , B01D71/028 , B01D2253/106 , B01D2256/24 , B01D2257/108 , B01D2257/11 , B01D2257/406 , B01D2257/80 , B01D2323/08 , B01D2323/10 , C01B37/00 , C01B37/02 , C01B39/52
摘要： The present invention relates to template-free clathraslls whose framework comprises essentially SO2, wherein the crystals of the ciathrasils have the platelet-like morphology of a sheet silicate. The present invention further relates to a process for preparing these template-free clathrasils and also to their use as absorbent, as seed crystals for the synthesis of ciathrasil membranes of the same zeolite type and in the form of dense layers which function as gas separation membranes having a molecular sieving action.
摘要翻译：本发明涉及其基本上包含SO 2的框架的无模板的层合体，其中所述硅胶的晶体具有片状硅酸盐的片状形态。本发明还涉及一种制备这些无模板的层状螯合物的方法，并且还涉及它们作为吸收剂的用途，作为用于合成相同沸石类型的以及用作气体分离膜的致密层形式的晶体具有分子筛选作用。

8. 发明申请

US20110151517A1 PROCESS FOR THE PREPARATION OF HOMOPOLYSACCHARIDES 有权
标题翻译：制备双歧杆菌的方法
公开(公告)号：US20110151517A1
公开(公告)日：2011-06-23
申请号：US12967099
申请日：2010-12-14
申请人： Jörg Therre , Hartwig Voß , Julia Kristiane Schmidt , Tillmann Faust , Rajan Hollmann
发明人： Jörg Therre , Hartwig Voß , Julia Kristiane Schmidt , Tillmann Faust , Rajan Hollmann
IPC分类号： C12P19/44
CPC分类号： C12P19/04 , B01D61/147 , B01D63/066 , B01D65/02 , B01D71/024 , B01D71/025 , B01D2321/168 , B01D2325/022 , C08B37/0024
摘要： A process for the preparation of aqueous solutions of glucans having a β-1,3-glycosidically-linked main chain and side groups having a β-1,6-glycosidic bond by fermentation of fungal strains. The fungal strains secrete the glucans into the fermentation broth, in an aqueous culture medium, and the separation of the glucans from the fermentation broth is effected using asymmetrical filter membranes.
摘要翻译：一种通过真菌菌株发酵制备具有β-糖苷连接的主链和具有＆bgr--1,6-糖苷键的侧基的葡聚糖水溶液的方法。真菌菌株在水性培养基中将葡聚糖分泌到发酵液中，并且使用不对称的过滤膜从发酵液中分离葡聚糖。

9. 发明授权

US06673960B1 Work-up of distillation residues from the synthesis of toluene diisocyanate 失效
标题翻译：从甲苯二异氰酸酯的合成处理蒸馏残留物
公开(公告)号：US06673960B1
公开(公告)日：2004-01-06
申请号：US09719616
申请日：2000-12-14
申请人： Hans Volkmar Schwarz , Markus Maurer , Michael Sander , Eckhard Ströfer , Rene Leuthold , Burghard Hantel , Siegfried Richter , Jörg Therre
发明人： Hans Volkmar Schwarz , Markus Maurer , Michael Sander , Eckhard Ströfer , Rene Leuthold , Burghard Hantel , Siegfried Richter , Jörg Therre
IPC分类号： C07C26500
CPC分类号： C08G18/5033 , C07C209/62 , C07C263/10 , C07C263/18 , C08G65/26 , C08G65/2612 , C07C211/51 , C07C265/14
摘要： A process for working up distillation residues from the synthesis of tolylene diisocyanate by reaction of the distillation residues with water comprises reacting the TDI distillation residues with water in a continuous or semicontinuous process in a backmixed reactor in the presence of hydrolysate.
摘要翻译：通过蒸馏残余物与水的反应来处理来自甲苯二异氰酸酯的合成的蒸馏残余物的方法包括在水解产物存在下，将反应混合反应器中的TDI蒸馏残余物与水连续或半连续过程反应。

10. 发明授权

US08574873B2 Process for the preparation of homopolysaccharides 有权
标题翻译：制备均聚糖的方法
公开(公告)号：US08574873B2
公开(公告)日：2013-11-05
申请号：US12967099
申请日：2010-12-14
申请人： Jörg Therre , Hartwig Voβ , Julia Kristiane Schmidt , Tillmann Faust , Rajan Hollmann
发明人： Jörg Therre , Hartwig Voβ , Julia Kristiane Schmidt , Tillmann Faust , Rajan Hollmann
IPC分类号： C12N9/24
CPC分类号： C12P19/04 , B01D61/147 , B01D63/066 , B01D65/02 , B01D71/024 , B01D71/025 , B01D2321/168 , B01D2325/022 , C08B37/0024
摘要： A process for the preparation of aqueous solutions of glucans having a β-1,3-glycosidically-linked main chain and side groups having a β-1,6-glycosidic bond by fermentation of fungal strains. The fungal strains secrete the glucans into the fermentation broth, in an aqueous culture medium, and the separation of the glucans from the fermentation broth is effected using asymmetrical filter membranes.
摘要翻译：一种通过发酵真菌菌株制备具有β-1,3-糖苷连接的主链和具有β-1,6-糖苷键的侧基的葡聚糖水溶液的方法。真菌菌株在水性培养基中将葡聚糖分泌到发酵液中，并且使用不对称的过滤膜从发酵液中分离葡聚糖。

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