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1. 发明授权

US4992204A Irradiation detection and identification method and compositions useful therein 失效
标题翻译：辐射检测和鉴定方法及其中有用的组合物
公开(公告)号：US4992204A
公开(公告)日：1991-02-12
申请号：US397079
申请日：1989-08-22
申请人： Edward W. Kluger , Patrick D. Moore , John B. Hines , John G. Lever
发明人： Edward W. Kluger , Patrick D. Moore , John B. Hines , John G. Lever
IPC分类号： D06M23/00 , D06Q1/00
CPC分类号： D06Q1/00 , D06M23/00
摘要： A method for tagging one or a mixture of natural or synthetic materials comprising contacting the same with one or a mixture of tagging compounds containing one or more non-ionic luminophore moieties attached to at least one poly(oxyalkylene) moiety by means of a linking moiety; wherein said tagging compound has substantial absorbance within the range of from about 300 to about 400 nm and reemits substantial visible light, said contacting effecting at least a temporary association between said material and said compound wherein said compound is present in an amount between about 0.0001 and about 10 percent by weight of said material.
摘要翻译：用于标记天然或合成材料的一种或混合物的方法，包括使其与含有通过连接部分连接至至少一个聚（氧化烯）部分的一个或多个非离子发光体部分的标记化合物或其混合物接触 ; 其中所述标记化合物具有在约300至约400nm范围内的实质吸光度，并且重新产生显着的可见光，所述接触至少在所述材料和所述化合物之间起暂时的缔合作用，其中所述化合物的存在量为约0.0001至约10重量％的所述材料。

2. 发明授权

US4826978A Reactive, non-yellowing triazine compounds useful as UV screening agents for polymers 失效
标题翻译：用作聚合物的UV屏蔽剂的反应性，不变黄的三嗪化合物
公开(公告)号：US4826978A
公开(公告)日：1989-05-02
申请号：US139342
申请日：1987-12-29
申请人： Cyril A. Migdal , John B. Hines , Edward W. Kluger
发明人： Cyril A. Migdal , John B. Hines , Edward W. Kluger
IPC分类号： C07D251/24 , C08K5/3492 , C07D251/12
CPC分类号： C08K5/3492 , C07D251/24
摘要： Triazine compounds are disclosed which are useful for imparting UV screening properties to polymers of the formula: ##STR1## wherein R is an electron withdrawing group; R.sub.1 is H, ##STR2## where R.sub.3 is an alkyl group having from one to about six carbon atoms; and R.sub.2 is selected from H and CH.sub.3, also disclosed are polymer compositions having improved UV screening properties containing said triazine compounds.
摘要翻译：公开了三嗪化合物，其可用于赋予下式的聚合物的UV屏蔽性能：其中R是吸电子基团; R1是H，其中R3是具有1至约6个碳原子的烷基; 并且R 2选自H和CH 3，还公开了具有包含所述三嗪化合物的改进的UV屏蔽性质的聚合物组合物。

3. 发明授权

US5591833A Colorants and intermediates therefor having branched poly(oxyalkylene)moieties, and their manufacture 失效
标题翻译：具有支链聚（氧化烯）部分的着色剂和中间体及其制备
公开(公告)号：US5591833A
公开(公告)日：1997-01-07
申请号：US104276
申请日：1993-08-10
申请人： John B. Hines , David J. Moody , Edward W. Kluger
发明人： John B. Hines , David J. Moody , Edward W. Kluger
IPC分类号： C09B69/00 , C09B69/10 , D06P5/13
CPC分类号： C09B69/00
摘要： Colorants and compositions useful as a fugitive or permanent colorant for a variety of substrates, or as intermediates for their manufacture, and having one or more improved properties of enhanced aqueous washability, compatibility with and non-extractibility from thermoplastic resins, or reactivity with resins having reactive functionality, said composition having the formula C(Z).sub.1-8 wherein:C is the residue of a reactant having from 1-8 nucleophilic site residues to which the Z moieties are attached; said Z moieties containing at least about 60 weight percent of poly(oxyalkylene) which is comprised of(a) at least one glycidol residue segment of 2-6 glycidol residues attached to a nucleophilic site of C, wherein said poly(oxyalkylene) contains a total of from 2-20 glycidol residues,(b) and wherein said poly(oxyalkylene) further contains the residues of one or more other epoxide reactants of ethylene oxide (EO), propylene oxide (PO), or butylene oxide (BO), or mixtures thereof, wherein said poly(oxyalkylene) contains a total of from about 10 to about 600 of said EO, PO or BO residues, or mixtures thereof, at least about 75 mole percent of which are EO residues,(c) and with the provisions that the ratio of the total of --0--PO-- and --O--BO-- linkages of all glycidol residues to the total of all functional oxy linkages of said glycidol residues is less than one, and the molar ratio of EO residues to glycidol residues is from 4 to 75.
摘要翻译：可用作各种底物的挥发性或永久性着色剂的着色剂和组合物，或作为其制造的中间体，并且具有一种或多种改进的水性洗涤性，与热塑性树脂的相容性和不可萃取性的改进性能，或与具有所述组合物具有式C（Z）1-8，其中：C是具有与Z部分连接的1-8个亲核位点残基的反应物的残基; 所述Z部分包含至少约60重量％的聚（氧化烯），其由（a）至少一个连接到C的亲核位点的2-6个缩水甘油残基的缩水甘油残基部分组成，其中所述聚（氧化烯）含有总共2-20个缩水甘油残基，（b），其中所述聚（氧化烯）还含有环氧乙烷（EO），环氧丙烷（PO）或环氧丁烷（BO））的一种或多种其它环氧化物反应物的残基，或其混合物，其中所述聚（氧化烯）含有总共约10至约600的所述EO，PO或BO残基或其混合物，其至少约75摩尔％为EO残基，（c）和所有缩水甘油残基的-O-PO-和-O-BO-键的总和与所述缩水甘油残基的所有功能氧键的总和的比例小于1，EO残基与缩水甘油残基为4-75。

4. 发明授权

US4962142A Reactive, non-yellowing triazine compounds useful as UV screening agents for polymers 失效
标题翻译：用作聚合物的UV屏蔽剂的反应性，不变黄的三嗪化合物
公开(公告)号：US4962142A
公开(公告)日：1990-10-09
申请号：US270871
申请日：1988-11-14
申请人： Cyril A. Migdal , John B. Hines , Edward W. Kluger
发明人： Cyril A. Migdal , John B. Hines , Edward W. Kluger
IPC分类号： C07D251/24 , C08K5/3492
CPC分类号： C07D251/24 , C08K5/3492
摘要： Triazine compounds are disclosed which are useful for imparting UV screening properties to polymers of the formula: ##STR1## wherein R is an electron withdrawing group; R.sub.1 is H, ##STR2## where R.sub.3 is an alkyl group having from one to about six carbon atoms; and R.sub.2 is selected from H and CH.sub.3, also disclosed are polymer compositions having improved UV screening properties containing said triazine compounds.
摘要翻译：公开了三嗪化合物，其可用于赋予下式的聚合物的UV屏蔽性能：其中R是吸电子基团; R1是H，其中R3是具有1至约6个碳原子的烷基; 并且R 2选自H和CH 3，还公开了具有包含所述三嗪化合物的改进的UV屏蔽性质的聚合物组合物。

5. 发明授权

US5043013A Washable ink compositions 失效
标题翻译：可洗油墨组合物
公开(公告)号：US5043013A
公开(公告)日：1991-08-27
申请号：US394346
申请日：1989-08-15
申请人： Edward W. Kluger , Patrick D. Moore , Judy A. Wagner
发明人： Edward W. Kluger , Patrick D. Moore , Judy A. Wagner
IPC分类号： C09B69/00 , C09D11/16
CPC分类号： C09D11/17 , C09B69/00
摘要： A washable aqueous ink composition having a viscosity of from about 1.0 to about 6.0 centipoises and containing from about 10 to about 50% by weight of one or more polymeric colorants of the formula: ##STR1## wherein: X is a polar group such as sulfonic acids, sulfonic acid salts, sulfonamides, sulfonates or the like;R is alkylene; Y is H, alkanoyl, carbamoyl, or the like;R.sub.1 is nitrogen, oxygen, sulfur, or a sulfur-containing divalent linking group;a is an integer of from six to about forty;b and c are each independently selected from one or two;d is an integer of from one to four; the product of (a) (b) (c) is an integer of from 6 to about 40;and CHROM is a chromophore such as nitro, nitroso, monoaxo, disazo and trisazo, diarylmethane, triarylmethane, xanthane, acridine, methine, thiazole, indamine, azine, oxazine, or anthraquinone, wherein the (RO).sub.a moiety is bonded to a carbocyclic aromatic ring of the (CHROM) through R.sub.1.
摘要翻译：一种可洗涤的水性油墨组合物，其粘度为约1.0至约6.0厘泊并含有约10至约50重量％的一种或多种下式的聚合着色剂：{R1 [（RO）aY] b} c其中： X是极性基团，例如磺酸，磺酸盐，磺酰胺，磺酸盐等; R为亚烷基; Y是H，烷酰基，氨基甲酰基等; R1是氮，氧，硫或含硫二价连接基团; a是从6到大约40的整数; b和c各自独立地选自一个或两个; d是1到4的整数; （a）（b）（c）的产物为6至约40的整数; CHROM是硝基，亚硝基，单键，双偶氮和三偶氮，二芳基甲烷，三芳基甲烷，呫吨，吖啶，次甲基，噻唑，茚胺，吖嗪，恶嗪或蒽醌的发色团，其中（RO）a部分键合到碳环（CHROM）的芳环通过R1。

6. 发明授权

US4761502A Polyalkyleneoxytrifluoromethylaniline compounds 失效
标题翻译：聚亚烷基氧三氟甲基苯胺化合物
公开(公告)号：US4761502A
公开(公告)日：1988-08-02
申请号：US904459
申请日：1986-09-08
申请人： Edward W. Kluger , Patrick D. Moore , Joe T. Burchette
发明人： Edward W. Kluger , Patrick D. Moore , Joe T. Burchette
IPC分类号： C08G65/28 , C07C87/28 , C07C87/60
CPC分类号： C07C217/50 , C07C217/08 , C07C217/28
摘要： Polyalkyleneoxytrifluoromethylaniline compounds are provided of the formula: ##STR1## wherein R.sub.1 is independently selected from H, a lower alkyl group containing from 1 to about 10 carbon atoms, CH.sub.2 Cl, CH.sub.2 Br, CH.sub.2 OH, phenyl or ##STR2## where R.sub.5 is H or a lower alkyl group containing from 1 to about 9 carbon atoms; R.sub.2 is selected from H, a lower alkyl group containing from 1 to about 9 carbon atoms, alkylaryl containing from 7 to about 11 carbon atoms, cyanoalkyl, or acyl; R.sub.3 is selected from a lower alkyl group containing from 1 to about 9 carbon atoms, cyanoalkyl, acetoxyalkyl or ##STR3## wherein R.sub.1 and R.sub.2 are as given above; R.sub.4 is H, CF.sub.3, a lower alkyl group containing from 1 to about 9 carbon atoms, Cl or Br and n is 0 or an integer from 1 to about 125.
摘要翻译：聚亚烷基氧基三氟甲基苯胺化合物由下式提供：其中R 1独立地选自H，含有1至约10个碳原子的低级烷基，CH 2 Cl，CH 2 Br，CH 2 OH，苯基或者其中R 5是H或低级含有1至约9个碳原子的烷基; R2选自H，含有1至约9个碳原子的低级烷基，含有7至约11个碳原子的烷基芳基，氰基烷基或酰基; R3选自含有1至约9个碳原子的低级烷基，氰基烷基，乙酰氧基烷基或其中R 1和R 2如上所定义; R 4为H，CF 3，含有1至约9个碳原子的低级烷基，Cl或Br，n为0或1至约125的整数。

7. 发明授权

US4912203A Thiophene base colorants useful for coloring thermoset resins 失效
标题翻译：用于着色热固性树脂的噻吩碱着色剂
公开(公告)号：US4912203A
公开(公告)日：1990-03-27
申请号：US194761
申请日：1988-05-17
申请人： Edward W. Kluger , Patrick D. Moore
发明人： Edward W. Kluger , Patrick D. Moore
IPC分类号： C09B29/09 , C08G18/38 , C08G18/50 , C08K5/45 , C09B29/00 , C09B29/36 , C09B67/10 , C09B69/10 , D06P3/26
CPC分类号： C08G18/38 , C08G18/50 , C08K5/45 , C09B29/0059 , C09B69/106 , Y10S8/922 , Y10S8/924 , Y10S8/926 , Y10S8/927 , Y10S8/928
摘要： Thiophene based colorants useful for coloring thermoset resins such as polyurethanes being the formula; ##STR1## wherein R.sub.1, R.sub.2 and R.sub.3 are selected from halogen, carboxylic acid, alkanoyl, aryloyl, carbocyclic forming polymethylene chains, alkyl, aryl, cyano, thioalkyl, dithioalkyl, thioaryl, dithioaryl, thiocyano, carboxyalkyl, carboxyaryl, amidoalkyl, amidodialkyl, amidoaryl, amidodiaryl, oxyalkyl, thioamidoalkyl, thioamidodialkyl, or hydrogen when an adjacent group is isobutyryl; R.sub.4, R.sub.5, and R.sub.7 are selected from hydrogen alkyl, oxyalkyl, sulfonamidoalkyl, sulfonamidoaryl, amidoalkyl, amidodialkyl, amidoaryl, amidodiaryl, halogen, thioalkyl and thioaryl; and R.sub.8 and R.sub.9 are selected from polyalkylene oxide, copolymers of polyalkylene oxides, and hydroxyalkylenes.
摘要翻译：用于着色热固性树脂如聚氨酯的噻吩类着色剂为配方; 其中R 1，R 2和R 3选自卤素，羧酸，烷酰基，芳氧基，形成碳环的多亚甲基链，烷基，芳基，氰基，硫代烷基，二硫代烷基，硫代芳基，二硫代芳基，硫代氰基，羧基烷基，羧基芳基，酰氨基烷基，酰胺基二烷基，酰胺基芳基，酰胺基芳基，烷氧基，硫代酰氨基烷基，硫代酰胺基二烷基或氢;当相邻基团是异丁酰基时; R4，R5和R7选自烷基，烷氧基，亚磺酰氨基烷基，亚磺酰氨基芳基，酰胺基烷基，酰胺基烷基，酰氨基芳基，酰胺基芳基，卤素，硫代烷基和硫代芳基; 并且R8和R9选自聚环氧烷，聚环氧烷和羟烷基的共聚物。

8. 发明授权

US4507407A Process for in situ coloration of thermosetting resins 失效
标题翻译：热固性树脂原位着色工艺
公开(公告)号：US4507407A
公开(公告)日：1985-03-26
申请号：US624377
申请日：1984-06-25
申请人： Edward W. Kluger , Patrick D. Moore
发明人： Edward W. Kluger , Patrick D. Moore
IPC分类号： C08G18/00 , C08G18/08 , C08G18/38 , C08G18/50 , C08L75/00 , C08G18/14 , C08G18/32 , C08G18/34
CPC分类号： C08G18/38 , C08G18/50
摘要： A process of coloring polyurethane resins during the production of same with reactive colorants having the formula: ##STR1## wherein R.sub.1, R.sub.2, R.sub.3 are selected from halogen, carboxylic acid, alkanoyl, aryloyl, alkyl, aryl, cyano, sulfonylalkyl, sulfonylaryl, thioalkyl, thioaryl, sulfinylalkyl, sulfinylaryl, dithioalkyl, dithioaryl, thiocyano, amidoalkyl, amidodialkyl, oxyalkyl, oxyaryl, hydrogen, sulfonamidoalkyl, sulfonamidoaryl, sulfonamidodialkyl, sulfonamidodiaryl, carbocyclic forming polymethylene chains, sulfenamidoalkyl, sulfenamidodialkyl, sulfenamidoaryl, sulfenamidodiaryl, sulfinamidoalkyl, sulfinamidodialkyl, sulfinamidoaryl, sulfinamidodiaryl; and A is an organic dyestuff coupler that is resistant to stannous octanoate and flame retardant compounds and which has functionality through reactive substituents thereof.
摘要翻译：在制备具有下式的反应性着色剂时，聚氨酯树脂着色的方法：其中R1，R2，R3选自卤素，羧酸，烷酰基，芳基，烷基，芳基，氰基，磺酰基烷基，磺酰基芳基，硫代烷基硫代芳基，亚磺酰基烷基，亚磺酰基芳基，二硫代烷基，二硫代芳基，硫氰基，酰氨基烷基，酰胺基二烷基，烷氧基烷基，亚磺酰氨基芳基，磺酰氨基二烷基，亚磺酰氨基芳基，碳环多烯基，亚磺酰氨基二芳基; A是有机染料偶合剂，其对辛酸亚锡和阻燃化合物具有抗性，并通过其反应性取代基具有官能团。

9. 发明授权

US4775748A Reactive colorants 失效
标题翻译：反应性着色剂
公开(公告)号：US4775748A
公开(公告)日：1988-10-04
申请号：US058696
申请日：1987-06-01
申请人： Edward W. Kluger , Patrick D. Moore
发明人： Edward W. Kluger , Patrick D. Moore
IPC分类号： C09B29/09 , C08G18/38 , C08G18/50 , C08K5/45 , C09B29/00 , C09B29/36 , C09B67/10 , C09B69/10 , D06P3/26 , C09B29/01 , C09B29/033 , D06P3/24
CPC分类号： C08G18/38 , C08G18/50 , C08K5/45 , C09B29/0059 , C09B69/106 , Y10S8/922 , Y10S8/924 , Y10S8/926 , Y10S8/927 , Y10S8/928
摘要： Novel reactive colorants being the formula: ##STR1## wherein R.sub.1, R.sub.2 and R.sub.3 are selected from halogen, carboxylic acid, alkanoyl, aryloyl, carbocyclic forming polymethylene chains, alkyl, aryl, cyano, thioalkyl, dithioalkyl, thioaryl, dithioaryl, thiocyano, carboxyalkyl, carboxyaryl, amidoalkyl, amidodialkyl, amidoaryl, amidodiaryl, oxyalkyl, thioamidoalkyl, thioamidodialkyl, or hydrogen when an adjacent group is isobutyryl; R.sub.4, R.sub.5, R.sub.6 and R.sub.7 are selected from hydrogen, alkyl, oxyalkyl, oxyaryl, sulfonamidoalkyl, sulfonamidoaryl, amidoalkyl, amidodialkyl, amidoaryl, amidodiaryl, halogen, thioalkyl and thioaryl; and R.sub.8 and R.sub.9 are selected from polyalkylene oxide, copolymers of polyalkylene oxides, and hydroxyalkylenes.
摘要翻译：新型反应性着色剂是下式：其中R 1，R 2和R 3选自卤素，羧酸，烷酰基，芳氧基，碳环形成的多亚甲基链，烷基，芳基，氰基，硫代烷基，二硫代烷基，硫代芳基，二硫代芳基，硫代氰基，，当相邻基团是异丁酰基时，羧基芳基，酰氨基烷基，酰胺基烷基，酰氨基芳基，酰氨基芳基，烷氧基，硫代酰氨基烷基，硫代酰胺基二烷基或氢。 R4，R5，R6和R7选自氢，烷基，烷氧基，氧基芳基，亚磺酰氨基烷基，亚磺酰氨基芳基，酰氨基烷基，酰胺基烷基，酰胺基芳基，酰胺二芳基，卤素，硫代烷基和硫代芳基; 并且R8和R9选自聚环氧烷，聚环氧烷和羟烷基的共聚物。

10. 发明授权

US4751254A Process for in situ coloration of thermosetting resins 失效
标题翻译：热固性树脂原位着色工艺
公开(公告)号：US4751254A
公开(公告)日：1988-06-14
申请号：US5249
申请日：1987-01-20
申请人： Edward W. Kluger , Patrick D. Moore , Joe T. Burchette
发明人： Edward W. Kluger , Patrick D. Moore , Joe T. Burchette
IPC分类号： C08G18/38 , C08G18/50 , C08G18/10
CPC分类号： C08G18/3836 , C08G18/38 , C08G18/5033 , C08G2120/00
摘要： This invention relates to a process for coloring polyurethane resins during the production of same with reactive colorants derived from novel polyalkoxytrifluoroaniline intermediates. These colorants impart increased brightness in shade for both aromatic and heteroaromatic derivatives and increased resistance to stannous octanoate catalyst over conventional polymeric colorants derived for heteroaromatic compounds. These novel colorants have the structure: ##STR1## wherein R.sub.1 is selected from H, a lower alkyl group containing from 1 to about 10 carbon atoms, CH.sub.2 Cl, CH.sub.2 OH, phenyl or ##STR2## where R.sub.6 is H or a lower alkyl group containing from 1 to about 9 carbon atoms; R.sub.2 is selected from OH, NH.sub.2 or SH; R.sub.3 is selected from a lower alkyl group containing from 1 to about 9 carbon atoms, cyanoalkyl, acetoxyalkyl or ##STR3## where R.sub.1 and R.sub.2 are as given above; R.sub.4 is H, CF.sub.3, a lower alkyl group containing from 1 to about 9 carbon atoms, Cl or Br and n is 0 or an integer form 1 to about 125. R.sub.5 is an aromatic or heteroaromatic containing group, said colorants being resistant to stannous octanoate, being characterized as having improved brightness and which have functionality through reactive substituents thereof.
摘要翻译：本发明涉及聚氨酯树脂在与新型聚烷氧基三氟苯胺中间体衍生的反应着色剂生产过程中着色的方法。这些着色剂对于芳族和杂芳族衍生物赋予增加的亮度亮度，并且对于衍生自杂芳族化合物的常规聚合物着色剂，对辛酸亚锡催化剂的耐受性提高。这些新型着色剂具有以下结构：其中R 1选自H，含有1至约10个碳原子的低级烷基，CH 2 Cl，CH 2 OH，苯基或者其中R 6是H或低级烷基， 1至约9个碳原子; R2选自OH，NH2或SH; R3选自含有1至约9个碳原子的低级烷基，氰基烷基，乙酰氧基烷基或其中R 1和R 2如上所定义; R 4是H，CF 3，含有1至约9个碳原子的低级烷基，Cl或Br，n是0或1至约125的整数.R 5是含芳族或杂芳族基团，所述着色剂对亚锡辛酸酯，其特征在于具有改善的亮度，并具有通过其反应性取代基的官能团。

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