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61. 发明申请

US20100210740A2 MODULAR REACTOR FOR EXOTHERMIC/ENDOTHERMIC CHEMICAL REACTIONS 有权
标题翻译：用于灭菌/内热化学反应的模块化反应器
公开(公告)号：US20100210740A2
公开(公告)日：2010-08-19
申请号：US12520002
申请日：2007-12-18
申请人： Vincenzo PICCOLO , Susi BONOMI , Marzio PIAZZA
发明人： Vincenzo PICCOLO , Susi BONOMI , Marzio PIAZZA
IPC分类号： C07C1/04 , B01J8/22
CPC分类号： B01J8/22 , B01J8/008 , B01J8/1836 , B01J2208/00132 , B01J2219/0002 , B01J2219/0286
摘要： Modular reactor for exothermic/endothermic chemical reactions which take place in three-phase systems, comprising a series of modules, superimposed with respect to each other, fixed to each other by means of coupling flanges, each module consisting of an external cylindrical body and a series of tube bundles, for the circulation of a thermal-exchange fluid, positioned inside said body.
摘要翻译：在三相系统中发生的用于放热/吸热化学反应的模块化反应器，包括通过联接凸缘相互相对重叠的一系列模块，每个模块由外部圆柱体和一系列管束，用于定位在所述体内的热交换流体的循环。

62. 发明授权

US07736598B2 Reactor and method for producing chlorine from HCl 失效
标题翻译：从HCl生产氯的反应器和方法
公开(公告)号：US07736598B2
公开(公告)日：2010-06-15
申请号：US10588511
申请日：2005-02-08
申请人： Lothar Seidemann , Olga Schubert , Martin Sesing , Eckhard Stroefer , Martin Fiene , Christian Walsdorff , Klaus Harth
发明人： Lothar Seidemann , Olga Schubert , Martin Sesing , Eckhard Stroefer , Martin Fiene , Christian Walsdorff , Klaus Harth
IPC分类号： F27B15/14 , F27B15/00 , C01B7/00
CPC分类号： B01J8/34 , B01J8/0055 , B01J8/006 , B01J8/1836 , B01J2208/00132 , B01J2208/0015 , B01J2208/00495 , B01J2219/0286 , C01B7/04
摘要： The invention relates to a reactor and a process for preparing chlorine from hydrogen chloride by gas-phase oxidation by means of oxygen in the presence of a heterogeneous catalyst in a fluidized bed, with gas-permeable plates being located in the fluidized bed. The gas-permeable plates are connected in a thermally conductive manner to a heat exchanger located in the fluidized bed.
摘要翻译：本发明涉及一种反应器和一种通过在流化床中的非均相催化剂存在下通过氧气气相氧化从氯化氢制备氯的方法，气体可渗透板位于流化床中。气体渗透板以导热方式连接到位于流化床中的热交换器。

63. 发明申请

US20100104497A1 METHOD AND APPARATUS FOR PREPARING TUNGSTEN HEXAFLUORIDE USING A FLUIDIZED BED REACTOR 审中-公开
标题翻译：使用流化床反应器制备硝酸铁的方法和装置
公开(公告)号：US20100104497A1
公开(公告)日：2010-04-29
申请号：US12388859
申请日：2009-02-19
申请人： Hyang Ja JANG , Jong Yool Yang , Chul Ho Kim , Young Gu Cho , Jung Eun Lee , Yuichi Ilkubo
发明人： Hyang Ja JANG , Jong Yool Yang , Chul Ho Kim , Young Gu Cho , Jung Eun Lee , Yuichi Ilkubo
IPC分类号： C01B9/08 , F28D21/00
CPC分类号： B01J8/1836 , B01J8/0055 , B01J8/1827 , B01J2208/00212 , C01G41/04
摘要： Disclosed herein are a method of preparing tungsten hexafluoride (WF6) gas by fluidizing tungsten powder with inert gas in a reactor and fluorinating the fluidized tungsten powder with fluorine (F2) or nitrogen trifluoride (NF3) gas, and an apparatus (including fluidized bed reactor) for carrying out the method. The fluidized bed reactor shows a reaction efficiency of higher than 99% when being used to prepare tungsten hexafluoride.
摘要翻译：本文公开了一种通过在反应器中用惰性气体流化钨粉末并用氟（F 2）或三氟化氮（NF 3））氟化氟化流化钨粉末的装置（包括流化床反应器）来制备六氟化钨（WF 6）气体的方法）用于执行该方法。当用于制备六氟化钨时，流化床反应器显示高于99％的反应效率。

64. 发明申请

US20100098850A1 APPARATUS AND METHOD FOR TOP REMOVAL OF GRANULAR MATERIAL FROM A FLUIDIZED BED DEPOSITION REACTOR 有权
标题翻译：从流化床沉积反应器顶部去除颗粒材料的装置和方法
公开(公告)号：US20100098850A1
公开(公告)日：2010-04-22
申请号：US12647283
申请日：2009-12-24
申请人： Stephen Michael Lord
发明人： Stephen Michael Lord
IPC分类号： B05D7/00
CPC分类号： F27B15/09 , B01J8/0025 , B01J8/0055 , B01J8/1809 , B01J8/1836 , B01J2208/0061 , B01J2208/00761 , B07B9/00 , F27D17/008
摘要： A method of operating a fluidized bed deposition reactor to provide top removal of granular material, including production product is set forth. The vertical generally cylindrical reactor has at least one gas inlet at the lower end, at least one gas and solids outlet at the upper end and a gas/granular product separator connected to the gas and solids outlet. A heated reaction zone located in the lower portion of the reactor includes a fluidized bed; the bed being fluidized to establish a bubbling fluidized bed with a defined stable height. A disengaging space is provided above the stable bed height. A reaction gas is added to the bottom of the reactor, the reaction gas depositing a reaction product coating on the granular particles, the coating being abraded off the granules. The combined flow rate of the fluidizing gas and the reaction gas is adjusted so that a majority of the granular particles are retained in the reactor while maintaining bubbling. The height of the bed is increased and the disengaging height above the bed is decreased until the bursting of bubbles near the surface of the bed throws granular particles through the gas and solids outlet to the gas/granular product separator. The flow rates of the gases are controlled to maintain a balance between particles removed by the separator and the average rate of granular particle size increase as adjusted for attrition.
摘要翻译：阐述了一种操作流化床沉积反应器以提供包括生产产品在内的颗粒材料的顶部除去的方法。垂直的大致圆柱形反应器在下端具有至少一个气体入口，在上端具有至少一个气体和固体出口以及连接到气体和固体出口的气体/颗粒产物分离器。位于反应器下部的加热反应区包括流化床; 床被流化以建立具有确定的稳定高度的鼓泡流化床。在稳定床高度之上设置脱离空间。将反应气体加入到反应器的底部，反应气体在颗粒状颗粒上沉积反应产物涂层，涂层被磨碎掉。调节流化气体和反应气体的组合流量，使得大部分颗粒颗粒保持在反应器中同时保持起泡。床的高度增加，并且床上方的脱离高度降低，直到床表面附近的气泡爆裂将粒状颗粒通过气体和固体出口引入气体/颗粒状产物分离器。控制气体的流速以保持通过分离器除去的颗粒和平均颗粒粒度增加速率之间的平衡，以便调节磨损。

65. 发明申请

US20100048955A1 PROCESS FOR PREPARING AROMATIC AMINES IN A FLUIDIZED-BED REACTOR 失效
标题翻译：在流化床反应器中制备芳族氨基酸的方法
公开(公告)号：US20100048955A1
公开(公告)日：2010-02-25
申请号：US12441907
申请日：2007-09-14
申请人： Lothar Seidemann , Lucia Koenigsmann , Christian Schneider , Ekkehard Schwab , Dieter Stuetzer , Celine Liekens
发明人： Lothar Seidemann , Lucia Koenigsmann , Christian Schneider , Ekkehard Schwab , Dieter Stuetzer , Celine Liekens
IPC分类号： C07C209/36
CPC分类号： C07C209/36 , B01J8/006 , B01J8/1836 , B01J8/1845 , B01J8/1872 , B01J8/34 , B01J19/32 , B01J2208/00132 , B01J2219/3221 , B01J2219/32213 , B01J2219/3222 , B01J2219/32227 , B01J2219/32408 , B01J2219/32416 , B01J2219/32466 , B01J2219/32475 , C10G45/20 , C07C211/46
摘要： A process for preparing aromatic amines by catalytic hydrogenation of the corresponding nitro compound in a fluidized-bed reactor, in which a gaseous reaction mixture comprising the nitro compound and hydrogen flows from the bottom upward through a heterogeneous particulate catalyst forming a fluidized bed, wherein the fluidized bed is provided with internals which divide the fluidized bed into a plurality of cells arranged horizontally in the fluidized-bed reactor and a plurality of cells arranged vertically in the fluidized-bed reactor, with the cells having cell walls which are permeable to gas and have openings which ensure an exchange number of the heterogeneous, particulate catalyst in the vertical direction in the range from 1 to 100 liters/hour per liter of reactor volume, is proposed.
摘要翻译：一种通过在流化床反应器中催化氢化相应硝基化合物制备芳族胺的方法，其中包含硝基化合物和氢气的气态反应混合物从底部向上流过形成流化床的非均相颗粒催化剂，其中流化床设置有将流化床分成在流化床反应器中水平布置的多个单元的内部，以及在流化床反应器中垂直排列的多个单元，其中单元具有可渗透气体的单元壁，具有确保每升反应器体积在1至100升/小时范围内的异相颗粒催化剂在垂直方向上的交换数量的开口。

66. 发明授权

US07651668B2 Production method and production device for carbon nano structure 失效
标题翻译：碳纳米结构的生产方法和生产装置
公开(公告)号：US07651668B2
公开(公告)日：2010-01-26
申请号：US11663451
申请日：2005-09-21
申请人： Yoshikazu Nakayama , Hiroyuki Tsuchiya , Yugo Higashi , Toshiki Goto , Keisuke Shiono , Takeshi Nagasaka , Nobuharu Okazaki
发明人： Yoshikazu Nakayama , Hiroyuki Tsuchiya , Yugo Higashi , Toshiki Goto , Keisuke Shiono , Takeshi Nagasaka , Nobuharu Okazaki
IPC分类号： B01J8/18 , F27B15/14 , B01J19/18 , B01J19/00 , C01B31/02
CPC分类号： B82Y40/00 , B01J8/008 , B01J8/1818 , B01J8/1836 , B01J23/825 , B01J23/835 , B01J2208/00212 , B01J2208/00548 , B01J2219/00006 , B82Y30/00 , C01B32/05 , C01B32/162
摘要： A material gas and a catalyst are introduced through a material supplying tube path and a catalyst supplying tube path together with a carrier gas into a reactor equipped on its outer periphery with a heat applicator for thermally decomposing the material gas. The reactor has a convention regulator fitted to the discharge end of the catalyst supplying tube path. The convection regulator covers an edge side of the reactor to regulate gas flow in the reactor so that the flow does not reach the edge side. Due to this, a convection state can be efficiently produced in a reaction region. Consequently, it becomes possible to prevent contamination defect caused by accumulation/adherence of concretion of catalyst, which was generated by aggregation of cooled catalyst in the low-temperature region of the reactor and a decomposition product of the material gas. Thus the efficiency of carbon nanostructure production can be improved.
摘要翻译：将材料气体和催化剂通过材料供给管路和催化剂供给管路与载气一起引入装配在其外周的反应器中，并具有用于热分解原料气体的热施加器。反应器具有安装在催化剂供给管路径的排出端的惯性调节器。对流调节器覆盖反应器的边缘侧，以调节反应器中的气流，使得流不到达边缘侧。由此，可以在反应区域中有效地产生对流状态。因此，可以防止由反应器的低温区域中的冷却的催化剂的聚集产生的催化剂的凝结的累积/粘附引起的污染缺陷和原料气体的分解产物。因此，可以提高碳纳米结构生产的效率。

67. 发明授权

US07651547B2 Fluidized bed method and plant for the heat treatment of solids containing titanium 有权
标题翻译：流化床方法和用于热处理含钛固体的设备
公开(公告)号：US07651547B2
公开(公告)日：2010-01-26
申请号：US10540376
申请日：2003-12-10
申请人： Dirk Nuber , Michael Ströder , Werner Stockhausen , Ali-Naghi Beyzavi , Lothar Formanek , Martin Hirsch
发明人： Dirk Nuber , Michael Ströder , Werner Stockhausen , Ali-Naghi Beyzavi , Lothar Formanek , Martin Hirsch
IPC分类号： B01J8/24 , C22B1/10 , C22B5/14
CPC分类号： B01J8/1818 , B01J8/1836 , B01J8/26 , B01J2208/00548 , B01J2208/00725 , C21B13/0033 , C22B1/10 , C22B5/14 , C22B34/1204 , C22B34/1209 , F27B15/02 , F27B15/10 , Y02P10/136
摘要： The present invention relates to a method and a plant for the heat treatment of solids containing titanium and possibly further metal oxides, in which fine-grained solids are heated to a temperature of 700 to 950° C. in a fluidized bed reactor (1). To improve the energy utilization, it is proposed to introduce a first gas or gas mixture from below through a gas supply tube (3) into a mixing chamber (7) of the reactor (1), the gas supply tube (3) being at least partly surrounded by a stationary annular fluidized bed (10) which is fluidized by supplying fluidizing gas. The gas velocities of the first gas or gas mixture as well as of the fluidizing gas for the annular fluidized bed (10) are adjusted such that the particle Froude numbers in the gas supply tube (3) are between 1 and 100, in the annular fluidized bed (10) between 0.02 and 2 and in the mixing chamber (7) between 0.3 and 30.
摘要翻译：本发明涉及用于热处理包含钛和可能的其它金属氧化物的固体的方法和设备，其中在流化床反应器（1）中将细粒固体加热至700-950℃，。为了提高能量利用率，建议从下方通过气体供给管（3）将第一气体或气体混合物引入反应器（1）的混合室（7），气体供给管（3）处于最少部分地被固定的环形流化床（10）包围，所述静止环形流化床通过供应流化气体而流化。调节第一气体或气体混合物以及用于环形流化床（10）的流化气体的气体速度，使得气体供应管（3）中的微粒弗劳德数在1和100之间，在环形流化床（10）在0.02和2之间，并且在混合室（7）中在0.3和30之间。

68. 发明申请

US20090191101A1 CATALYST AND SYSTEMS INCORPORATING THE CATALYST 有权
标题翻译：催化剂和催化剂体系
公开(公告)号：US20090191101A1
公开(公告)日：2009-07-30
申请号：US12361377
申请日：2009-01-28
申请人： Jeffrey W. ELAM , Michael J. Pellin , Joseph A. Libera , Peter C. Stair , Gerry Zajac , Steven A. Cohen
发明人： Jeffrey W. ELAM , Michael J. Pellin , Joseph A. Libera , Peter C. Stair , Gerry Zajac , Steven A. Cohen
IPC分类号： B01J8/18 , B01J23/22 , B01J23/20 , B01J23/30 , B01J19/24
CPC分类号： B01J8/1836 , B01J23/002 , B01J23/30 , B01J35/023 , B01J35/065 , B01J35/1014 , B01J35/1019 , B01J35/1061 , B01J37/0238 , B01J37/0244 , B01J2523/00 , C23C16/405 , C23C16/45525 , B01J2523/55 , B01J2523/56 , B01J2523/69
摘要： A catalyst includes a carrier body and a catalytic portion carried by the carrier body. The catalytic portion includes a plurality of distinct layers of catalytic material, which layers may be deposited through atomic layer deposition techniques. The catalyst may have a selectivity for the conversion of alkanes to alkenes of over 50%. The catalyst may be incorporated in a reactor such as a fluidized bed reactor or a single pass reactor.
摘要翻译：催化剂包括载体和由载体承载的催化部分。催化部分包括多个不同层的催化材料，这些层可以通过原子层沉积技术沉积。催化剂可以具有选择性，使烷烃转化为烯烃超过50％。催化剂可以并入反应器如流化床反应器或单程反应器中。

69. 发明授权

US07473873B2 Apparatus and methods for synthesis of large size batches of carbon nanostructures 失效
标题翻译：用于合成大批量碳纳米结构的装置和方法
公开(公告)号：US07473873B2
公开(公告)日：2009-01-06
申请号：US11228023
申请日：2005-09-15
申请人： Alexandru Sorin Biris , Alexandru Radu Biris , Dan Lupu , Jon Gardner Wilkes , Dan Alexander Buzatu , Dwight Wayne Miller , Jerry A. Darsey
发明人： Alexandru Sorin Biris , Alexandru Radu Biris , Dan Lupu , Jon Gardner Wilkes , Dan Alexander Buzatu , Dwight Wayne Miller , Jerry A. Darsey
IPC分类号： H05B6/10
CPC分类号： B01J8/0015 , B01J8/0285 , B01J8/087 , B01J8/12 , B01J8/1836 , B01J8/1845 , B01J8/40 , B01J12/007 , B01J19/087 , B01J23/44 , B01J23/755 , B01J23/88 , B01J2208/00469 , B01J2208/00557 , B01J2208/0084 , B01J2219/0875 , B01J2219/0892 , B82Y30/00 , B82Y40/00 , C01B32/162 , C23C16/46 , D01F9/127 , H05B6/108 , H05B2214/04 , Y10S977/70 , Y10S977/844
摘要： An apparatus and method for synthesizing nanostructures. In one embodiment, the apparatus includes a reactor having a reaction zone and a conductive susceptor positioned in the reaction zone. The method includes the steps of transporting a gas mixture having an aerosolized catalyst, a feedstock and a carrier gas into the reaction zone of the reactor, inductively heating the reaction zone, and regulating a flow rate of the gas mixture to allow the catalyst to spend a sufficient amount of time in the reaction zone for the growth of nanostructures.
摘要翻译：纳米结构合成的装置和方法。在一个实施方案中，该装置包括具有位于反应区中的反应区和导电基座的反应器。该方法包括以下步骤：将具有雾化催化剂，原料和载气的气体混合物输送到反应器的反应区中，感应加热反应区，并调节气体混合物的流速以使催化剂消耗在反应区中足够的时间用于生长纳米结构。

70. 发明申请

US20080312076A1 Process for sulfurization or presulfurization of solid particles of a catalyst or an adsorbent 有权
标题翻译：催化剂或吸附剂的固体颗粒的硫化或预硫化方法
公开(公告)号：US20080312076A1
公开(公告)日：2008-12-18
申请号：US12117805
申请日：2008-05-09
申请人： Pierre DUFRESNE , Franck Labruyere , Maxime Meens , Loredana Romano
发明人： Pierre DUFRESNE , Franck Labruyere , Maxime Meens , Loredana Romano
IPC分类号： B01J27/051 , B01J27/02 , B01J27/043 , B05C3/00 , B01J20/00 , B01J27/047
CPC分类号： B01J8/16 , B01J8/1809 , B01J8/1818 , B01J8/1836 , B01J8/40 , B01J23/72 , B01J23/882 , B01J27/043 , B01J27/047 , B01J27/0515 , B01J37/20 , B01J2208/00017 , B01J2208/00061 , B01J2208/00212 , B01J2208/00371 , B01J2208/00407 , B01J2208/00415 , B01J2208/0053 , B01J2219/1944 , C10G45/04 , C10G2300/207 , Y10S502/514
摘要： The invention relates to a process for incorporating sulfur in the porosity of the solid particles of a catalyst for the conversion of hydrocarbons or an adsorbent. This process is carried out off-site in the presence of hydrogen sulfide that is pure or diluted in hydrogen or nitrogen, a process in which said particles are made to rise or fall in a sulfur incorporation zone that comprises at least one vibratory helical coil that is essentially tubular in shape and that comprises at least two turns, whereby said particles are subjected to a temperature profile over the majority of their path in said coil and whereby said particles are brought into contact with at least one fluid on at least one portion of their path.
摘要翻译：本发明涉及在用于转化烃或吸附剂的催化剂的固体颗粒的孔隙中掺入硫的方法。这种方法是在氢气或氮气中纯化或稀释的硫化氢存在下进行的，所述硫化氢在硫掺入区中上升或下降，其中包含至少一个振动螺旋线圈，基本上是管状的并且包括至少两匝，由此所述颗粒在所述线圈中的大部分路径上经受温度分布，并且由此使所述颗粒在至少一个部分上与至少一个流体接触他们的路径

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