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1. 发明授权

US10620127B2 Systems and methods for predicting and controlling the properties of a chemical species during a time-dependent process 有权
公开(公告)号：US10620127B2
公开(公告)日：2020-04-14
申请号：US16254532
申请日：2019-01-22
申请人： ADVANCED POLYMER MONITORING TECHNOLOGIES, INC. , THE ADMINISTRATORS OF THE TULANE EDUCATIONAL FUND
发明人： Wayne Frederick Reed , Michael Felix Drenski
IPC分类号： G01N21/75 , G01N21/27 , B01J19/00 , B01J19/18 , B01J8/22 , G01N21/84 , G01N35/00 , B01J8/00 , E21B41/00 , G01N21/19 , G01N21/21 , G01N21/23 , G01N21/33 , G01N21/35 , G01N21/47 , G01N21/64 , G01N21/65 , G01N11/08
CPC分类号： G01N21/75 , B01J8/001 , B01J8/006 , B01J8/222 , B01J8/228 , B01J19/0006 , B01J19/18 , B01J19/1881 , E21B41/00 , G01N21/272 , G01N21/84 , B01J2208/00061 , B01J2208/00212 , B01J2208/00362 , B01J2208/00539 , B01J2208/00548 , B01J2208/00575 , B01J2208/00628 , B01J2208/00637 , B01J2208/00725 , B01J2208/00973 , B01J2219/002 , B01J2219/0004 , B01J2219/0024 , B01J2219/00063 , B01J2219/00069 , B01J2219/00072 , B01J2219/00094 , B01J2219/00123 , B01J2219/00164 , B01J2219/00168 , B01J2219/00186 , B01J2219/00216 , B01J2219/00218 , B01J2219/00225 , B01J2219/00231 , B01J2219/00236 , B01J2219/00238 , B01J2219/00243 , B01J2219/00272 , G01N11/08 , G01N21/19 , G01N21/21 , G01N21/23 , G01N21/33 , G01N21/35 , G01N21/47 , G01N21/64 , G01N21/65 , G01N2021/8416 , G01N2201/12
摘要： Devices and methods for controlling the properties of chemical species during time-dependent processes. A device includes a reactor for containing one or more chemical species of a time-dependent process, an extraction pump for automatically and continuously extracting an amount of the one or more chemical species from the reactor, one or more detectors for measuring property changes of the one or more extracted chemical species and generating a continuous stream of data related to the one or more property changes to the one or more chemical species during a time interval, and a process controller configured to fit the continuous stream of data to a mathematical function to predict one or more properties of the one or more chemical species at a future time point and make one or more process decisions based on the prediction of one or more properties at the future time point.

2. 发明授权

US09050572B2 Process for the production of carbon nanotubes in a fluidized bed 有权
标题翻译：在流化床中生产碳纳米管的方法
公开(公告)号：US09050572B2
公开(公告)日：2015-06-09
申请号：US11735023
申请日：2007-04-13
申请人： Sigurd Buchholz , Maziar Kakhi , Volker Michele , Leslaw Mleczko , Christian Münnich , Reiner Rudolf , Aurel Wolf
发明人： Sigurd Buchholz , Maziar Kakhi , Volker Michele , Leslaw Mleczko , Christian Münnich , Reiner Rudolf , Aurel Wolf
IPC分类号： B01J3/06 , C01B31/06 , B01J3/08 , B01J8/18 , B01J8/24 , B82Y30/00 , B82Y40/00 , C01B31/02
CPC分类号： B01J8/18 , B01J8/24 , B01J2208/00548 , B01J2208/00575 , B01J2208/00584 , B01J2208/00672 , B01J2208/00681 , B01J2208/00725 , B82Y30/00 , B82Y40/00 , C01B32/162 , C01B2202/36
摘要： The present invention relates to a process for the production of carbon nanotubes by decomposition of hydrocarbons on a heterogeneous catalyst in a fluidized bed reactor, wherein the reactor can be operated batchwise or continuously, and in the case of continuous operation discharge can take place with sifting or without sifting.
摘要翻译：本发明涉及通过在流化床反应器中在非均相催化剂上分解碳氢化合物来生产碳纳米管的方法，其中反应器可以间歇或连续地操作，并且在连续操作的情况下，可以通过筛分或不筛选。

3. 发明授权

US08846829B2 Catalyst feed control during catalyst transition periods 有权
标题翻译：催化剂过渡期催化剂进料控制
公开(公告)号：US08846829B2
公开(公告)日：2014-09-30
申请号：US13100675
申请日：2011-05-04
申请人： Gregory G. Hendrickson
发明人： Gregory G. Hendrickson
IPC分类号： C08F2/00 , C08F2/12 , C08F2/34 , C08F10/00 , B01J8/22 , B01J8/18 , B01J19/18
CPC分类号： B01J8/001 , B01J8/1809 , B01J8/224 , B01J2208/0007 , B01J2208/00265 , B01J2208/00548 , B01J2208/00725 , B01J2219/002 , B01J2219/00209 , B01J2219/00231 , C08F10/00 , C08F2400/02 , C08F2410/05 , C08F2/00 , C08F2/34
摘要： Techniques are provided for operating a reactor during a catalyst transition period. The instantaneous reaction rate during a catalyst transition period can be determined using real-time measured process variables, and material balance calculations to provide an instantaneous reaction rate in approximately real time. According to certain embodiments, a material balance can be performed on the reactor system using a continuous ideal stirred tank reactor to determine the fractions of each type of catalyst that are present in the reactor, as well as the overall weight percent of catalyst in the reactor. A controller can then calculate the overall instantaneous reaction rate based on the respective catalyst fractions and the overall weight percent of catalyst in the reactor. The catalyst feed rate can then be adjusted based on the determined instantaneous reaction rate to maintain the instantaneous reaction rate within desired limits during a catalyst transition period.
摘要翻译：提供了在催化剂过渡期间操作反应器的技术。可以使用实时测量的过程变量和材料平衡计算来确定催化剂过渡期间的瞬时反应速率，以大致实时提供瞬时反应速率。根据某些实施方案，可以使用连续理想的搅拌釜反应器在反应器系统上进行物料平衡以确定存在于反应器中的每种类型的催化剂的馏分以及反应器中催化剂的总重量百分比。然后，控制器可以基于各个催化剂组分和反应器中催化剂的总重量百分数来计算总瞬时反应速率。然后可以基于确定的瞬时反应速率来调节催化剂进料速率，以在催化剂过渡期间将瞬时反应速率保持在所需限度内。

4. 发明授权

US08814961B2 Various methods and apparatuses for a radiant-heat driven chemical reactor 有权
标题翻译：用于辐射热驱动的化学反应器的各种方法和装置
公开(公告)号：US08814961B2
公开(公告)日：2014-08-26
申请号：US13429749
申请日：2012-03-26
申请人： Christopher Perkins , Zoran Jovanovic , Timothy E. Laska
发明人： Christopher Perkins , Zoran Jovanovic , Timothy E. Laska
IPC分类号： B01J7/00
CPC分类号： C01B3/344 , B01J2208/00336 , B01J2208/00415 , B01J2208/00451 , B01J2208/00504 , B01J2208/00513 , B01J2208/00725 , B01J2208/00752 , C01B2203/0216 , C01B2203/0272 , C10J3/485 , C10J3/506 , C10J2300/0903 , C10J2300/0916 , C10J2300/092 , C10J2300/0976 , C10J2300/1223 , C10J2300/1269 , C10L9/083 , Y02P20/134 , Y02P20/145
摘要： Heat-transfer-aid particles entrained with 1) biomass particles, 2) reactant gas, or 3) both are fed into the radiant heat chemical reactor. The inner wall of a cavity and the tubes of the chemical reactor act as radiation distributors by either absorbing radiation and re-radiating it to the heat-transfer-aid particles or reflecting the incident radiation to the heat-transfer-aid particles. The radiation is absorbed by the heat-transfer-aid particles, and the heat is then transferred by conduction to the reacting gas at temperatures between 900° C. and 1600° C. The heat-transfer-aid particles mix with the reactant gas in the radiant heat chemical reactor to sustain the reaction temperature and heat transfer rate to stay within a pyrolysis regime. The heat-transfer-aid particles produce a sufficient heat surface-area to mass ratio of these particles when dispersed with the reactant gas to stay within the pyrolysis regime during the chemical reaction.
摘要翻译：带有1）生物质颗粒的热转移助剂颗粒，2）反应物气体，或3）都被送入辐射热化学反应器。空腔的内壁和化学反应器的管作为辐射分配器，通过吸收辐射并将其再辐射到热转移助剂颗粒或将入射辐射反射到热转移助剂颗粒上。放射线被热转移助剂颗粒吸收，然后在900℃至1600℃的温度下通过传导将热量转移到反应气体中。热转移助剂颗粒与反应气体在辐射热化学反应器，以维持反应温度和传热速率保持在热解状态。当在化学反应期间，当与反应物气体分散以保持在热分解状态下时，热转移助剂颗粒产生足够的热表面积与质量比的这些颗粒。

5. 发明申请

US20120283395A1 CATALYST FEED CONTROL DURING CATALYST TRANSITION PERIODS 有权
标题翻译：催化转换期催化剂进料控制
公开(公告)号：US20120283395A1
公开(公告)日：2012-11-08
申请号：US13100675
申请日：2011-05-04
申请人： Gregory G. Hendrickson
发明人： Gregory G. Hendrickson
IPC分类号： C08F2/00 , B01J19/00 , C08F10/00
CPC分类号： B01J8/001 , B01J8/1809 , B01J8/224 , B01J2208/0007 , B01J2208/00265 , B01J2208/00548 , B01J2208/00725 , B01J2219/002 , B01J2219/00209 , B01J2219/00231 , C08F10/00 , C08F2400/02 , C08F2410/05 , C08F2/00 , C08F2/34
摘要： Techniques are provided for operating a reactor during a catalyst transition period. The instantaneous reaction rate during a catalyst transition period can be determined using real-time measured process variables, and material balance calculations to provide an instantaneous reaction rate in approximately real time. According to certain embodiments, a material balance can be performed on the reactor system using a continuous ideal stirred tank reactor to determine the fractions of each type of catalyst that are present in the reactor, as well as the overall weight percent of catalyst in the reactor. A controller can then calculate the overall instantaneous reaction rate based on the respective catalyst fractions and the overall weight percent of catalyst in the reactor. The catalyst feed rate can then be adjusted based on the determined instantaneous reaction rate to maintain the instantaneous reaction rate within desired limits during a catalyst transition period.
摘要翻译：提供了在催化剂过渡期间操作反应器的技术。可以使用实时测量的过程变量和材料平衡计算来确定催化剂过渡期间的瞬时反应速率，以大致实时提供瞬时反应速率。根据某些实施方案，可以使用连续理想的搅拌釜反应器在反应器系统上进行物料平衡，以确定存在于反应器中的每种类型的催化剂的馏分以及反应器中催化剂的总重量百分数。然后，控制器可以基于各个催化剂组分和反应器中催化剂的总重量百分数来计算总瞬时反应速率。然后可以基于确定的瞬时反应速率来调节催化剂进料速率，以在催化剂过渡期间将瞬时反应速率保持在所需限度内。

6. 发明申请

US20120114546A1 Hybrid TCS-siemens process equipped with 'turbo charger' FBR; method of saving electricity and equipment cost from TCS-siemens process polysilicon plants of capacity over 10,000 MT/YR 审中-公开
标题翻译：混合TCS-西门子工艺配备“涡轮增压器”FBR; TCS西门子工艺多晶硅厂的生产能力超过10000吨/年的节电方法和设备成本
公开(公告)号：US20120114546A1
公开(公告)日：2012-05-10
申请号：US13200989
申请日：2011-10-06
申请人： Yong Chee , Tetsunori Kunimune
发明人： Yong Chee , Tetsunori Kunimune
IPC分类号： C01B33/027 , B01J8/26
CPC分类号： B01J8/0055 , B01J8/1836 , B01J8/1872 , B01J8/32 , B01J8/44 , B01J2208/00168 , B01J2208/00725 , C01B33/1071 , C01B33/10731 , C01B33/10736 , C01B33/10742 , C01B33/10773
摘要： A ‘hybrid’ TCS (Trichlorosilane)-Siemens process is provided to save electricity and initial investment cost from TCS synthesizing process and silicon tetrachloride to TCS converting process in a TCS-Siemens polysilicon plant, whose size is over 10,000 MT/YR of polysilicon. The ‘hybrid’ TCS-Siemens process of the current application is equipped with one direct chlorination FBR (Fluidized Bed Reactor) and one hydro-chlorination FBR. Three different TCS-Siemens processes are compared based on mass balance calculation. The hybrid TCS-Siemens process saves at least 78,000,000Kwhr/year of electricity from TCS generation only from a 10,000 MT/YR polysilicon plant when compared with a ‘Closed Loop TCS-Siemens Process’, which is equipped with only high-pressure, high-temperature operating hydro-chlorination FBRs.
摘要翻译：提供了一种“混合”TCS（三氯硅烷）-Siemens工艺，用于将TCS合成工艺和四氯化硅的电力和初始投资成本节省到TCS西门子多晶硅工厂的TCS转换过程中，其大小超过10,000 MT / YR的多晶硅。目前应用的“混合”TCS-西门子工艺配备了一个直接氯化FBR（流化床反应器）和一个加氢氯化FBR。基于质量平衡计算，对三种不同的TCS-西门子工艺进行比较。与“闭环TCS-西门子工艺”相比，混合型TCS-西门子工艺节省了来自TCS产能的至少7800万千瓦时/年的电力，而该“闭环TCS-西门子工艺”仅配备高压高温度运行加氢氯化FBRs。

7. 发明授权

US07790941B2 Oxygenate-to-olefin conversions in a baffled reactor 有权
标题翻译：在挡板反应器中的氧化烯 - 烯烃转化率
公开(公告)号：US07790941B2
公开(公告)日：2010-09-07
申请号：US11435110
申请日：2006-05-16
申请人： James H. Beech, Jr. , Nicolas Coute , Jeffrey S. Smith , Michael Peter Nicoletti , Charles O. Bolthrunis , Domenic C. Ferrari , Umesh K. Jayaswal , Roy Walter Silverman
发明人： James H. Beech, Jr. , Nicolas Coute , Jeffrey S. Smith , Michael Peter Nicoletti , Charles O. Bolthrunis , Domenic C. Ferrari , Umesh K. Jayaswal , Roy Walter Silverman
IPC分类号： C07C1/00 , B01J19/00 , B01J8/18
CPC分类号： B01J8/0055 , B01J8/0292 , B01J8/1836 , B01J8/1872 , B01J8/386 , B01J8/388 , B01J29/85 , B01J29/90 , B01J2208/00132 , B01J2208/00141 , B01J2208/00548 , B01J2208/00663 , B01J2208/00725 , B01J2208/0084 , C07C1/20 , C07C2529/83 , C07C2529/85 , C10G2400/20 , Y02P20/584 , Y02P30/42 , C07C11/02
摘要： The invention concerns methods and systems for minimizing back-mixing of feedstock flow in converting oxygenates to olefins. In one embodiment, back-mixing is reduced by providing a reactor that includes baffles to reduce the hydraulic diameter of at least a portion of the reactor. Some or all of the baffles can also serve as cooling tubes for reducing temperature gradients in the reactor, and thereby maximize light olefin production.
摘要翻译：本发明涉及在将含氧化合物转化为烯烃时最小化原料流逆向混合的方法和系统。在一个实施例中，通过提供包括挡板以减少反应器的至少一部分的水力直径的反应器来减少反混合。挡板的一些或全部也可以用作冷却管，用于降低反应器中的温度梯度，从而使轻烯烃生产最大化。

8. 发明授权

US07651547B2 Fluidized bed method and plant for the heat treatment of solids containing titanium 有权
标题翻译：流化床方法和用于热处理含钛固体的设备
公开(公告)号：US07651547B2
公开(公告)日：2010-01-26
申请号：US10540376
申请日：2003-12-10
申请人： Dirk Nuber , Michael Ströder , Werner Stockhausen , Ali-Naghi Beyzavi , Lothar Formanek , Martin Hirsch
发明人： Dirk Nuber , Michael Ströder , Werner Stockhausen , Ali-Naghi Beyzavi , Lothar Formanek , Martin Hirsch
IPC分类号： B01J8/24 , C22B1/10 , C22B5/14
CPC分类号： B01J8/1818 , B01J8/1836 , B01J8/26 , B01J2208/00548 , B01J2208/00725 , C21B13/0033 , C22B1/10 , C22B5/14 , C22B34/1204 , C22B34/1209 , F27B15/02 , F27B15/10 , Y02P10/136
摘要： The present invention relates to a method and a plant for the heat treatment of solids containing titanium and possibly further metal oxides, in which fine-grained solids are heated to a temperature of 700 to 950° C. in a fluidized bed reactor (1). To improve the energy utilization, it is proposed to introduce a first gas or gas mixture from below through a gas supply tube (3) into a mixing chamber (7) of the reactor (1), the gas supply tube (3) being at least partly surrounded by a stationary annular fluidized bed (10) which is fluidized by supplying fluidizing gas. The gas velocities of the first gas or gas mixture as well as of the fluidizing gas for the annular fluidized bed (10) are adjusted such that the particle Froude numbers in the gas supply tube (3) are between 1 and 100, in the annular fluidized bed (10) between 0.02 and 2 and in the mixing chamber (7) between 0.3 and 30.
摘要翻译：本发明涉及用于热处理包含钛和可能的其它金属氧化物的固体的方法和设备，其中在流化床反应器（1）中将细粒固体加热至700-950℃，。为了提高能量利用率，建议从下方通过气体供给管（3）将第一气体或气体混合物引入反应器（1）的混合室（7），气体供给管（3）处于最少部分地被固定的环形流化床（10）包围，所述静止环形流化床通过供应流化气体而流化。调节第一气体或气体混合物以及用于环形流化床（10）的流化气体的气体速度，使得气体供应管（3）中的微粒弗劳德数在1和100之间，在环形流化床（10）在0.02和2之间，并且在混合室（7）中在0.3和30之间。

9. 发明申请

US20090214395A1 Raw Material Efficiency Method and Process 审中-公开
标题翻译：原料效率法和工艺
公开(公告)号：US20090214395A1
公开(公告)日：2009-08-27
申请号：US12038163
申请日：2008-02-27
申请人： John R. Parrish , Jeffrey B. Drabish , Oscar M. Longoria, JR. , James L. Swecker, II
发明人： John R. Parrish , Jeffrey B. Drabish , Oscar M. Longoria, JR. , James L. Swecker, II
IPC分类号： B01J19/00 , B01J8/24 , F27B15/08 , C08F2/12
CPC分类号： F27B15/18 , B01J8/003 , B01J8/0035 , B01J8/1872 , B01J2208/0061 , B01J2208/00725 , B01J2208/00761 , B01J2208/00769 , C08F10/00 , C08F2400/02 , C08F2/34
摘要： A method and apparatus are disclosed for controlling product discharge from a fluidized bed reactor and for minimizing the loss of the unreacted monomer in the fluidizing gas upon removing the solid polymer product from the reactor. The method and apparatus utilize at least one detector in the product tank or its vent line and a control system in communication with the detector and the product tank fill valve, along with certain algorithms, to adjust by an iterative process, the product discharge time, thereby maximizing resin fill in the product tank and minimizing the lost reactor gas volume.
摘要翻译：公开了一种用于控制来自流化床反应器的产物排放并且在从反应器中除去固体聚合物产物时使流化气体中的未反应单体的损失最小化的方法和装置。该方法和装置利用产品罐或其排气管线中的至少一个检测器和与检测器和产品罐填充阀连通的控制系统以及某些算法，通过迭代过程来调整产品排放时间，从而使产品罐中的树脂填充最大化并使反应堆的气体体积减少到最小。

10. 发明申请

US20060270884A1 Oxygenate-to-olefin conversions in a baffled reactor 有权
标题翻译：在挡板反应器中的氧化烯 - 烯烃转化率
公开(公告)号：US20060270884A1
公开(公告)日：2006-11-30
申请号：US11435110
申请日：2006-05-16
申请人： James Beech , Nicolas Coute , Jeffrey Smith , Michael Nicoletti , Charles Bolthrunis , Domenic Ferrari , Umesh Jayaswal , Roy Silverman
发明人： James Beech , Nicolas Coute , Jeffrey Smith , Michael Nicoletti , Charles Bolthrunis , Domenic Ferrari , Umesh Jayaswal , Roy Silverman
IPC分类号： C07C1/00 , B01J19/00 , B01J8/18
CPC分类号： B01J8/0055 , B01J8/0292 , B01J8/1836 , B01J8/1872 , B01J8/386 , B01J8/388 , B01J29/85 , B01J29/90 , B01J2208/00132 , B01J2208/00141 , B01J2208/00548 , B01J2208/00663 , B01J2208/00725 , B01J2208/0084 , C07C1/20 , C07C2529/83 , C07C2529/85 , C10G2400/20 , Y02P20/584 , Y02P30/42 , C07C11/02
摘要： The invention concerns methods and systems for minimizing back-mixing of feedstock flow in converting oxygenates to olefins. In one embodiment, back-mixing is reduced by providing a reactor that includes baffles to reduce the hydraulic diameter of at least a portion of the reactor. Some or all of the baffles can also serve as cooling tubes for reducing temperature gradients in the reactor, and thereby maximize light olefin production.
摘要翻译：本发明涉及在将含氧化合物转化为烯烃时最小化原料流逆向混合的方法和系统。在一个实施例中，通过提供包括挡板以减少反应器的至少一部分的水力直径的反应器来减少反混合。挡板的一些或全部也可以用作冷却管，用于降低反应器中的温度梯度，从而使轻烯烃生产最大化。

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