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71. 发明申请

WO01074767A1 METHOD FOR PRODUCING AROMATIC ALCOHOLS, ESPECIALLY PHENOL 审中-公开
标题翻译：工艺制备芳族醇，尤其是苯酚
公开(公告)号：WO01074767A1
公开(公告)日：2001-10-11
申请号：PCT/EP2001/003288
申请日：2001-03-22
IPC分类号： B01J31/02 , C07B61/00 , C07C27/12 , C07C37/08 , C07C39/04 , C07C45/53 , C07C49/08 , C07C49/385 , C07C49/413 , C07C409/08 , C07C409/10 , C07C409/14
CPC分类号： C07C409/14 , C07C37/08 , C07C45/53 , C07C407/00 , C07C409/08 , C07C409/10 , C07C2601/20 , Y02P20/52 , C07C49/403 , C07C49/413 , C07C49/08 , C07C39/04
摘要： The invention relates to a method for the production of phenol derivatives by performing catalytic oxidation of an aromatic hydrocarbon to obtain a hydroperoxide and subsequently cleaving the hydroperoxide into a phenol derivative and a ketone in the presence of a radical starter, wherein a compound of formula (I) is used as oxidation catalyst, wherein R , R = H, an aliphatic or aromatic alkoxy radical, a carboxyl radical, an alkoxycarbonyl radical or a hydrocarbon radical, with 1 to 20 carbon atoms, SO3H, NH2, OH, F, Cl, Br, I and/or NO2, wherein R and R represent identical or different radicals or R and R may be linked to one another by a covalent bond, wherein X, Z = C, S, CH2; Y = O, OH; k = 0, 1, 2; l = 0, 1, 2 and m = 1 to 3; wherein the molar ratio between the catalyst and the aromatic hydrocarbon is less than 10 mol %.
摘要翻译：本发明涉及一种通过芳族烃的氢过氧化物和氢过氧化物的后续切割，得到苯酚衍生物与酮的催化氧化制备苯酚衍生物，其中作为氧化催化剂，式（I）的化合物，其中R <1>，R <2> = H 脂肪族或芳香族的烷氧基，羧基基团，烷氧基羰基或烃基，各自具有1至20个碳原子，SO 3 H，NH 2，OH，氟，氯，Br，I和/或NO 2，其中R <1>和R <2>是相同的或不同表示的基团或R <1>和R <2>可以通过与X的共价键连接在一起，Z = C，S，CH 2 Y = O，OH，K = 0，1，2 L = 0，1，2 M = 1至3; 在自由基引发剂，其中所述催化剂与芳烃的摩尔比小于10摩尔％的存在下使用。

72. 发明申请

WO00066523A1 REMOVAL OF SALTS IN THE MANUFACTURE OF PHENOLIC COMPOUND 审中-公开
标题翻译：在酚醛化合物的制造中去除废物
公开(公告)号：WO00066523A1
公开(公告)日：2000-11-09
申请号：PCT/EP2000/004203
申请日：2000-05-02
IPC分类号： C07C37/72 , C07C37/08 , C07C37/68 , C07C37/74 , C07C39/04
CPC分类号： C07C37/685 , C07C37/08 , C07C39/04
摘要： There is provided a process for the manufacture of phenolic compounds by oxidising an alkyl-substituted aromatic compound to form the hydroperoxide derivative thereof, followed by cleavage of the hydroperoxide to form an aralkyl (aryl alkyl or alkyl aryl) hydroperoxide cleavage mass and neutralisation of the aralkyl hydroperoxide cleavage mass to form a neutralised aralkyl hydroperoxide cleavage mass stream, comprising: separating a neutralised aralkyl hydroperoxide cleavage mass stream containing salts of neutralisation into a crude ketone stream and a crude phenolic stream containing the salts of neutralisation; separating the crude phenolic stream into a concentrated phenolic-rich stream, enriched in phenolic compounds, and a crude phenolic bottoms stream enriched in tars and alpha methyl styrene dimers, each compared to the crude phenolic stream, said crude phenolic bottoms stream containing salts of neutralisation; adding water and a diluent composition to the crude phenolic bottoms stream, thereby forming a phase separable crude phenolic bottoms stream, said diluent composition comprised of hydrocarbons phase compatible with the crude phenolic bottoms stream and having a combined density lower than the density of the crude phenolic bottoms stream; separating the separable crude phenolic bottoms stream into a hydrocarbon phase and an aqueous phase containing salts of neutralisation; whereby the amount of salts of neutralisation in the hydrocarbon phase is reduced compared to the amount of salts of neutralisation present prior to separation.
摘要翻译：提供了通过氧化烷基取代的芳族化合物以形成其氢过氧化物衍生物，随后切割氢过氧化物以形成芳烷基（芳基烷基或烷基芳基）氢过氧化物切割物质并中和的方法来制备酚类化合物芳烷基氢过氧化物切割物质以形成中和的芳烷基氢过氧化物切割质量流，包括：将含有中和盐的中和芳烷基氢过氧化物切割质量流分离成粗酮流和含有中和盐的粗酚流; 将粗酚流分离成富含酚类化合物的富含浓酚的料流，以及富含焦油和α-甲基苯乙烯二聚体的粗酚底物流，与粗酚流相比，所述粗酚底物流含有中和盐 ; 向粗酚底物流中加入水和稀释剂组合物，从而形成可分离的粗酚底物流，所述稀释剂组合物由与粗酚底物流相容的烃相组成，并且具有低于粗酚苯的浓度的组合密度底部流; 将可分离的粗酚底物流分离成烃相和含有中和盐的水相; 由此与分离前存在的中和盐的量相比，烃相中的中和盐的量减少。

73. 发明申请

WO00014042A1 HIGH SELECTIVE METHOD OF PHENOL AND ACETONE PRODUCTION 审中-公开
标题翻译：苯酚和乙腈生产的高选择性方法
公开(公告)号：WO00014042A1
公开(公告)日：2000-03-16
申请号：PCT/US1999/020286
申请日：1999-09-03
IPC分类号： C07B61/00 , C07C1/20 , C07C15/44 , C07C27/00 , C07C37/08 , C07C39/04 , C07C45/53 , C07C49/08 , C07C39/12 , C07C45/00
CPC分类号： C07C1/20 , C07C37/08 , C07C45/53 , C07C2527/054 , C07C15/44 , C07C49/08 , C07C39/04
摘要： Disclosed is a process for the cleavage of technical cumene hydroperoxide (CHP) into phenol, acetone and alpha -methylstyrene. In a first stage, the CHP cleavage process is conducted in such a way to maintain the heat generation rate and the heat removal rate balanced in each of the CHP cleavage reactors. The cleavage of the CHP is conducted under substantially isothermal conditions at a temperature in the range of 47-50 DEG C. In the second stage of the process dicumylperoxide (DCP) and dimethylbenzene alcohol (DMBA) cleavage is carried out in a multi-section plug-flow reactor under non-isothermal conditions at a controlled temperature increase. The temperature is controlled with the use of thermocouples installed in each section of the reactor. The obtained temperature profile is compared with the temperature profile required by the kinetic model based on DELTA T in each section of the reactor. Based on any obtained fluctuations at least one of the amount of water additionally fed to the reactor, the temperature and the degree of sulfuric acid conversion into NH4HSO4 are adjusted.
摘要翻译：公开了将技术性氢过氧化枯烯（CHP）裂解成苯酚，丙酮和α-甲基苯乙烯的方法。在第一阶段中，CHP裂解工艺以保持每个CHP裂解反应器中的发热速率和热去除率平衡的方式进行。 CHP的裂解在基本上等温条件下在47-50℃的温度下进行。在二异辛基过氧化物（DCP）和二甲基苯醇（DMBA）的过程的第二阶段中，在多段在不受等温条件下控制温度升高的活塞式反应器。使用安装在反应堆每个部分的热电偶来控制温度。将获得的温度曲线与基于反应器每个部分中的DELTA T的动力学模型所需的温度曲线进行比较。基于任何获得的波动，至少一个额外进料到反应器的水中，调节温度和硫酸转化成NH 4 HSO 4的程度。

74. 发明申请

WO9410106A3 ACID CATALYST AND USE THEREOF IN ALKYLATION OF OLEFINS WITH TERTIARY ALKANES 审中-公开
标题翻译：酸催化剂及其与烷基烯烃烯烃的烷基化反应
公开(公告)号：WO9410106A3
公开(公告)日：1994-06-23
申请号：PCT/US9310463
申请日：1993-10-29
申请人： CATALYTICA INC
发明人： KING DAVID L , COOPER MICHAEL D , SANDERSON WILLIAM A
IPC分类号： B01J21/08 , B01J27/08 , B01J27/16 , B01J31/02 , B01J37/02 , C07C2/62 , C07C2/66 , C07C5/27 , C07C37/08 , C07C45/45 , C07C45/46 , C07C45/49 , C07C45/53 , C07C45/74 , C07C51/353 , C07C67/04 , C07C67/08 , C07C205/06 , C07C409/24 , C07C409/26 , C07D301/14 , C10G29/20 , C07C
CPC分类号： B01J31/0259 , B01J21/08 , B01J27/08 , B01J27/16 , B01J31/0211 , B01J31/0225 , B01J31/0227 , B01J31/0231 , B01J31/0258 , B01J31/0271 , B01J37/0201 , B01J2231/323 , B01J2531/48 , C07C2/62 , C07C2/66 , C07C5/2794 , C07C37/08 , C07C45/455 , C07C45/46 , C07C45/49 , C07C45/53 , C07C45/74 , C07C51/353 , C07C67/04 , C07C67/08 , C07C201/08 , C07C409/24 , C07C2527/08 , C07C2527/10 , C07C2527/1213 , C07C2527/125 , C07C2527/126 , C07C2527/128 , C07C2527/133 , C07C2527/135 , C07C2527/14 , C07C2531/025 , C07D301/14 , C10G29/205 , Y02P20/52 , C07C15/02 , C07C9/00 , C07C39/04 , C07C205/06
摘要： The present invention provides an acid catalyst complex comprising an organosulfonic acid having at least one covalent carbon-fluorine bond or one covalent carbon-phosphorus bond provided by a phosphono radical which has been contacted with a Lewis Acid to produce a catalyst complex containing said Lewis Acid. The present invention also provides a process for the conversion of a reactant into a reaction product in the presence of said catalyst complex. In particular, the catalyst complex is useful for providing a high octane alkylate stream by converting a mixture comprising isoparaffins and olefins into said alkylate in the presence of said catalyst complex.

75. 发明申请

WO2022057003A1 一种对甲基苯酚的强化微界面制备系统及方法审中-公开
公开(公告)号：WO2022057003A1
公开(公告)日：2022-03-24
申请号：PCT/CN2020/122814
申请日：2020-10-22
申请人：南京延长反应技术研究院有限公司
发明人：张志炳 , 周政 , 张锋 , 李磊 , 孟为民 , 王宝荣 , 杨高东 , 罗华勋 , 杨国强 , 田洪舟 , 曹宇
IPC分类号： C07C37/08 , C07C37/70 , C07C37/74 , C07C39/07
摘要：本发明提供了一种对甲基苯酚的强化微界面制备系统及方法，所述强化微界面制备系统包括：氧化反应器、管道反应器，所述氧化反应器的侧壁依次设置有氧气进口，以及对甲基异丙苯与催化剂混合进口，所述氧化反应器内设置有两个微界面发生器，所述两个微界面发生器上下错位设置，所述微界面发生器的正下方设置有多排喷涌管道，每排所述喷涌管道上设置有多个喷涌口，所述喷涌口的喷射方向朝上，所述氧气进口通过管道直通靠上的所述微界面发生器的内部。本发明的强化微界面制备系统通过在氧化反应器内设置微界面发生器，使得对甲基异丙苯在进行氧化反应之前将氧气破碎为微气泡，提高氧气与对甲基异丙苯之间的相界传质面积。

76. 发明申请

WO2018097690A1 메탄올 및 아세톤의 제거 유닛 및 이를 포함하는 페놀 및 비스페놀 A의 제조 시스템 审中-公开
公开(公告)号：WO2018097690A1
公开(公告)日：2018-05-31
申请号：PCT/KR2017/013650
申请日：2017-11-28
申请人： 주식회사 엘지화학
发明人： 이상범 , 이성규 , 신준호 , 이성호 , 박사은 , 정인용
IPC分类号： C07C37/68 , C07C37/08 , C07C37/86 , C07C37/88 , C07C37/70 , C07C39/04 , C07C37/20 , C07C39/16 , B01D3/32
摘要： 본 발명은 메탄올 및 아세톤 제거 유닛에 관한 것으로, 분해반응유닛 및 정제유닛을 포함하는 페놀의 제조 시스템과, 반응유닛 및 농축유닛을 포함하는 비스페놀A의 제조 시스템을 포함하는 시스템에 구비된다. 상기 제거 유닛은 제거 컬럼; 상기 제거 컬럼의 중단에 구비된 공급부; 메탄올 및 아세톤이 제거되는 탑정 퍼지부; 및 정제유닛으로 재순환되는 탑저 재순환부;를 포함하고, 상기 공급부는, 메탄올, 아세톤 및 물이 포함된 정제유닛 배출부와, 페놀, 아세톤 및 물이 포함된 농축유닛 배출부를 포함하는 것이다. 상기 제거 유닛은 페놀 및 비스페놀 A의 제조 시스템 내 포함될 수 있고, 이 경우 비스페놀 A의 생산성이 향상될 수 있고, 반응기 내 촉매의 수명이 향상될 수 있다.

77. 发明申请

WO2016083256A1 PROCESS FOR THE MANUFACTURE OF ALCOHOL AND/OR KETONE 审中-公开
标题翻译：制造酒精和/或酮的方法
公开(公告)号：WO2016083256A1
公开(公告)日：2016-06-02
申请号：PCT/EP2015/077203
申请日：2015-11-20
申请人： RHODIA OPERATIONS
发明人： CHOUZIER, Sandra , RASCON CRUZ, Luis Fernando , WECKHUYSEN, Bert , MASTROIANNI, Sergio
IPC分类号： C07C29/132 , C07C35/08 , C07C45/53 , C07C49/403 , C07C37/08 , C07C39/04 , C07C49/08 , C07C31/12 , B01J37/03 , B01J37/08 , B01J23/26 , B01J27/24 , B01J35/10
CPC分类号： B01J37/086 , B01J23/26 , B01J23/75 , B01J27/24 , B01J29/0308 , B01J29/84 , B01J35/1009 , B01J35/1014 , B01J37/0018 , B01J37/06 , B01J37/08 , C07C29/132 , C07C37/08 , C07C45/53 , C07C2523/24 , C07C2523/26 , C07C2601/14 , Y02P20/52 , C07C49/403 , C07C49/08 , C07C39/04 , C07C35/08 , C07C31/12
摘要： Process for the manufacture of at least one alcohol and/or at least one ketone, which comprises a step during which at least one organic peroxide compound is put into contact with at least one catalyst responding to formula (I) CrN x O y Formula (I) in which x is a number varying from 0.10 to 1.00 and y is a number varying from 0.00 to 1.50, in order to produce the at least one alcohol and/or at least one ketone.
摘要翻译：制备至少一种醇和/或至少一种酮的方法，其包括至少一种有机过氧化物化合物与至少一种响应式（I）的催化剂接触的步骤。其中x为0.10至1.00的数，y为0.00至1.50的数，以产生至少一种醇和/或至少一种酮。

78. 发明申请

WO2016059569A1 INTEGRATED POLYCARBONATE PRODUCTION PROCESS 审中-公开
标题翻译：一体化聚碳酸酯生产工艺
公开(公告)号：WO2016059569A1
公开(公告)日：2016-04-21
申请号：PCT/IB2015/057868
申请日：2015-10-14
申请人： SABIC GLOBAL TECHNOLOGIES B.V.
发明人： WANG, Henry
IPC分类号： C08G64/20 , C08G64/30 , C07C68/00 , C07C68/06 , C07C37/08 , C07C37/20 , C07C45/53 , C07C407/00 , C07C2/66 , C10G29/20 , C10G50/00 , C10G57/00 , C10G57/02 , C10G9/36 , C10G11/18
CPC分类号： C08G64/307 , C07C2/66 , C07C37/08 , C07C37/20 , C07C45/53 , C07C68/005 , C07C68/06 , C07C407/00 , C08G64/205 , C10G9/36 , C10G11/18 , C10G29/205 , C10G50/00 , C10G51/06 , C10G57/005 , C07C409/10 , C07C39/04 , C07C49/08 , C07C39/16 , C07C69/96 , C07C15/085
摘要： The disclosure concerns refining crude oil to produce a first plurality of streams comprising one or more of offgas, naphtha, liquefied petroleum, C3 and C4 olefins, processing at least a portion of the first plurality of streams to produce one or more streams comprising one or more of propylene, ethylene, butadiene, and offgas; reacting the ethylene and the offgas to produce streams comprising one or more of hydrogen, syngas, and polyethylene; processing one or more of the vacuum gas oil and the naphtha with a fluid catalytic cracker to produce a stream comprising propylene; reacting benzene with the propylene to produce cumene, reacting the cumene to produce phenol and acetone; reacting phenol and acetone to produce bisphenol A; contacting carbon monoxide, oxygen and methanol to produce dimethyl carbonate; reacting dimethyl carbonate and phenol to produce diphenyl carbonate; and reacting diphenyl carbonate with bisphenol A to produce polycarbonate.
摘要翻译：本公开涉及精炼原油以产生包含废气，石脑油，液化石油，C3和C4烯烃中的一种或多种的第一多种物流，处理第一多个物流的至少一部分以产生一种或多种物流，其包含一种或多种更多的是丙烯，乙烯，丁二烯和废气; 使乙烯和废气反应以产生包含氢，合成气和聚乙烯中的一种或多种的流; 用流化催化裂化器处理一种或多种减压瓦斯油和石脑油，以产生包含丙烯的料流; 使苯与丙烯反应生成异丙苯，使异丙苯反应生成苯酚和丙酮; 使苯酚和丙酮反应生成双酚A; 接触一氧化碳，氧气和甲醇，生产碳酸二甲酯; 使碳酸二甲酯和苯酚反应生成碳酸二苯酯; 并使碳酸二苯酯与双酚A反应生成聚碳酸酯。

79. 发明申请

WO2016031491A1 固体酸触媒、及び酸化物の製造方法审中-公开
标题翻译：固体酸催化剂和生产氧化物的方法
公开(公告)号：WO2016031491A1
公开(公告)日：2016-03-03
申请号：PCT/JP2015/071827
申请日：2015-07-31
申请人：株式会社ダイセル
发明人：鈴木崇将 , 高瀬一郎
IPC分类号： B01J31/32 , B01J31/28 , C07C27/16 , C07C29/48 , C07C31/125 , C07C33/14 , C07C33/22 , C07C35/08 , C07C35/18 , C07C37/08 , C07C39/04 , C07C45/33 , C07C47/02 , C07C47/54 , C07C49/403 , C07C49/603 , C07C51/215 , C07C53/126 , C07C63/06 , C07B61/00
CPC分类号： C07D311/76 , B01J23/8892 , B01J31/10 , B01J31/28 , B01J31/32 , B01J35/0006 , B01J35/02 , B01J35/026 , B01J37/009 , B01J37/0219 , B01J37/0221 , B01J37/0236 , B01J37/04 , B01J37/30 , B01J2231/70 , B01J2531/005 , B01J2531/008 , C07B61/00 , C07C27/16 , C07C29/48 , C07C31/125 , C07C33/14 , C07C33/22 , C07C35/08 , C07C35/18 , C07C37/08 , C07C39/04 , C07C45/33 , C07C45/40 , C07C47/02 , C07C47/54 , C07C49/403 , C07C49/603 , C07C51/215 , C07C51/34 , C07C53/126 , C07C63/06 , C07C2601/14 , C07C2601/16 , Y02P20/52
摘要：　基質を酸素とオゾンの共存下で酸化する際に用いる酸素－オゾン共存下酸化反応用の固体酸触媒であって、該基質を高い転化率で酸化できる固体酸触媒を提供する。　本発明の酸素－オゾン共存下酸化用固体酸触媒は、基質（Ａ）を酸素とオゾンの共存下で酸化する際に用いる酸化反応用の固体酸触媒であって、ハメットの酸度関数（Ｈ 0 ）が－９以下である強酸若しくは超強酸を少なくとも表面に有する担体に、遷移金属が、単体、化合物又はイオンの形態で担持されていることを特徴とする。前記担体は、フッ素化スルホン酸系樹脂からなるペレット若しくは粉粒体、又は固体表面にフッ素化スルホン酸系樹脂の被膜が形成された担体であるのが好ましい。
摘要翻译：本发明提供一种在氧气和臭氧存在的情况下进行氧化反应的固体酸催化剂，其在氧气和臭氧两者都被氧化时使用，其中基板可以以高转化率氧化。当在氧气和臭氧存在下氧化基质（A）时，使用这种在氧气和臭氧存在下进行氧化反应的固体酸催化剂，其特征在于过渡金属以至少在其表面上具有哈米特酸度函数（H0）为-9以下的强酸或超级酸的载体上的元素，化合物或离子。载体优选是由氟化磺酸树脂或在其固体表面上形成有氟化磺酸树脂的涂层的载体形成的颗粒或粉末或颗粒状材料。

80. 发明申请

WO2016020895A1 COATING TO INHIBIT FOULING OF REACTORS FOR CUMENE HYDROPEROXIDE CLEAVAGE 审中-公开
标题翻译：用于抑制氯化氢氧化酶清除剂反应器的涂料
公开(公告)号：WO2016020895A1
公开(公告)日：2016-02-11
申请号：PCT/IB2015/056023
申请日：2015-08-07
申请人： SABIC GLOBAL TECHNOLOGIES B.V.
发明人： NELSON, Mark Erik , DYKMAN, Arkady Samuilovich , ZINENKOV, Andrey Vladimirovich
IPC分类号： C07C37/08 , C07C45/53 , C07C407/00 , B01J19/02 , B01J31/06 , C07C39/04 , C07C49/08
CPC分类号： C07C37/08 , B01J19/0093 , B01J31/06 , B01J2219/00783 , B01J2219/00795 , B01J2219/00819 , B01J2219/00822 , B01J2219/00835 , B01J2219/00837 , B01J2219/00842 , B01J2219/00862 , B01J2219/00885 , B01J2219/0099 , C07C1/20 , C07C45/53 , C07C407/00 , Y02P20/52 , C07C39/04 , C07C49/08 , C07C409/16 , C07C15/44
摘要： The disclosure concerns methods comprising forming a phenol and acetone mixture from decomposition of a cumene hydroperoxide or a phenol, acetone, and AMS from the decomposition of a mixture containing dicumyl peroxide in a system comprising one or more reactors where at least a portion of an inner surface of the one or more reactors has a polymer coating and wherein the coating inhibits build-up of a fouling precipitate on the coated inner surface of the one or more reactors as compared to such build-up in the absence of the coating.
摘要翻译：本公开涉及包括在包含一种或多种反应器的系统中从含二枯基过氧化物的混合物的分解中形成苯酚和丙酮混合物从氢过氧化枯烯或苯酚，丙酮和AMS分解的方法，其中至少一部分内部一个或多个反应器的表面具有聚合物涂层，并且其中与在不存在涂层的情况下的这种积聚相比，涂层抑制了在一个或多个反应器的涂覆内表面上的结垢沉淀物的积聚。

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