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1. 发明申请

WO2016100700A1 METHODS FOR FORMING PEROXYFORMIC ACID AND USES THEREOF 审中-公开
标题翻译：用于形成过氧酸的方法及其用途
公开(公告)号：WO2016100700A1
公开(公告)日：2016-06-23
申请号：PCT/US2015/066438
申请日：2015-12-17
申请人： ECOLAB USA INC.
发明人： BALASUBRAMANIAN, Ramakrishnan , LI, Junzhong , STAUB, Richard , KEASLER, Victor , BENNETT, Brian , BREWSTER, Allison
IPC分类号： A01N37/00 , A01N37/16 , A61L2/18 , A23C7/02 , C02F1/72 , C07C407/00 , C07C409/24 , C07C409/26
CPC分类号： C07C409/24 , A01N37/16 , A23L3/34635 , A23L3/3508 , A23V2002/00 , C07C407/00 , C07C407/006
摘要： The present invention relates generally to methods for forming peroxyformic acid, comprising contacting formic acid with hydrogen peroxide. The methods for forming peroxyformic acid can include adding formic acid with a relatively lower concentration of hydrogen peroxide, or adding formic acid to a peroxycarboxylic acid composition or forming composition to react with hydrogen peroxide in the compositions. The present invention also relates to peroxyformic acid formed by the above methods. The present invention further relates to the uses of peroxyformic acid for treating a variety of targets, e.g ., target water, including target water used in connection with oil- and gas-field operations. The present invention further relates to methods for reducing or removing H 2 S or iron sulfide in the treated water source, improving clarity of the treated water source, or reducing the total dissolved oxygen or corrosion in the treated water source, using peroxyformic acid, including peroxyformic acid generated in situ.
摘要翻译：本发明一般涉及形成过氧甲酸的方法，包括使甲酸与过氧化氢接触。形成过氧甲酸的方法可以包括以较低浓度的过氧化氢加入甲酸，或将甲酸加入到过氧羧酸组合物中或形成组合物中以与组合物中的过氧化氢反应。本发明还涉及通过上述方法形成的过氧甲酸。本发明还涉及过氧甲酸用于处理各种靶物（例如目标水，包括与油气田操作有关的目标水）的用途。本发明还涉及使用过氧甲酸（包括过氧甲酸）来减少或除去处理水源中的硫化氢或硫化铁的方法，提高处理水源的透明度或降低处理水源中的总溶解氧或腐蚀原地生成。

2. 发明申请

WO2012090123A2 GENERATION OF PEROXYCARBOXYLIC ACIDS AT ALKALINE pH, AND THEIR USE AS TEXTILE BLEACHING AND ANTIMICROBIAL AGENTS 审中-公开
标题翻译：在碱性pH下生成过氧羧酸，并且它们用作纺织漂白剂和抗微生物剂
公开(公告)号：WO2012090123A2
公开(公告)日：2012-07-05
申请号：PCT/IB2011/055830
申请日：2011-12-20
申请人： ECOLAB USA INC. , FAST, Jonathan P. , HEI, Robert D.P. , STAUB, Richard , DURRSCHMIDT, Thomas J. , FORTH, Peter J. , LI, Junzhong , MCSHERRY, David D. , MERZ, Thomas , WINTER, Johannes
发明人： FAST, Jonathan P. , HEI, Robert D.P. , STAUB, Richard , DURRSCHMIDT, Thomas J. , FORTH, Peter J. , LI, Junzhong , MCSHERRY, David D. , MERZ, Thomas , WINTER, Johannes
IPC分类号： D06M15/327 , D06M13/196 , D06M13/10
CPC分类号： C07C407/00 , A01N37/16 , A01N59/00 , B01F5/0647 , B01F2015/0221 , B01J4/002 , B01J19/24 , B01J2219/00177 , C11D3/3945 , C07C409/24 , A01N43/08 , A01N2300/00
摘要： The present disclosure provides methods for generating percarboxylic acid compositions and/or peroxycarboxylic acid compositions formed external to a point of use in non-equilibrium reactions for use in certain bleaching and antimicrobial applications, in particular laundry applications. The compositions are generated external to a point of use, at alkaline pH levels, viz. greater than about pH 12, and optionally suitable for use with detergents and/or surfactants for synergistic bleaching efficacy. Methods of bleaching and/or disinfecting are further provided.
摘要翻译：本公开提供了用于在用于某些漂白和抗微生物应用，特别是洗衣应用的非平衡反应中形成的使用点外部的过羧酸组合物和/或过氧羧酸组合物的方法。在碱性pH水平下，在使用点外部产生组合物，即，大于约pH 12，并且任选地适合与洗涤剂和/或表面活性剂一起用于协同漂白效力。进一步提供漂白和/或消毒方法。

3. 发明申请

WO2007031596A2 PROCESS FOR THE PREPARATION OF PEROXY ACIDS 审中-公开
标题翻译：过氧化氢的制备方法
公开(公告)号：WO2007031596A2
公开(公告)日：2007-03-22
申请号：PCT/FI2006/000303
申请日：2006-09-13
申请人： KEMIRA OYJ , AKSELA, Reijo , RENVALL, Ilkka
发明人： AKSELA, Reijo , RENVALL, Ilkka
IPC分类号： A01N37/16 , C07C20060101 , C07C409/24 , C07C409/26 , C07C409/30
CPC分类号： C07C409/24 , A01N37/02 , A01N37/16 , C07C407/00 , C07C409/26 , C07C409/30 , A01N37/04 , A01N37/06 , A01N37/10 , A01N37/36 , A01N59/00 , A01N2300/00
摘要： The present invention relates to a process for the preparation of a solution comprising a first peroxy acid comprising performic acid and a second peroxy acid, said process comprising forming a carboxylic acid solution comprising a first carboxylic acid comprising formic acid, a second carboxylic acid and hydrogen peroxide, wherein the amount of formic acid is from 0.5 to 20 % by weight of the amount of the second carboxylic acid, and allowing the components to react to form a solution comprising performic acid and said second peroxy acid, the amount of peroxy acids being at least 5 % by weight. The invention also relates to a storable solution comprising performic acid and said second peroxy acid. The solution can be used as a disinfecting agent for controlling micro-organisms.
摘要翻译：本发明涉及一种制备溶液的方法，所述溶液包含包含甲酸和第二过氧酸的第一过氧酸，所述方法包括形成羧酸溶液，所述羧酸溶液包含含有甲酸，第二羧酸和氢的第一羧酸过氧化物，其中甲酸的量为第二羧酸的量的0.5至20重量％，并且使组分反应以形成包含甲酸和所述第二过氧酸的溶液，过氧酸的量为至少5重量％。本发明还涉及包含甲酸和所述第二过氧酸的可储存溶液。该溶液可用作控制微生物的消毒剂。

4. 发明申请

WO02026459A1 METHOD FOR THE CONTINUOUS PRODUCTION OF MIXTURES OF SUBSTANCES AND REACTION MIXTURES AND A DEVICE FOR CARRYING OUT SAID METHOD 审中-公开
标题翻译：过程对于识别以及反应混合物的连续生产和实施设备将其
公开(公告)号：WO02026459A1
公开(公告)日：2002-04-04
申请号：PCT/EP2001/009454
申请日：2001-08-16
IPC分类号： B01F3/08 , B01F5/06 , C07C409/24 , C07C409/26 , G05D11/13 , B29B7/60 , B01F15/04
CPC分类号： G05D11/132 , B01F3/088 , B01F5/0602 , B01F15/00136 , B01F15/00344 , B01F15/0479 , C07C407/00 , C07C409/26 , C07C409/24
摘要： The invention relates to a method for the continuous production of a mixture of substances or a reaction mixture formed by the reaction of components contained therein. The component fluxes drawn from a storage container (1, 2 or 3) or a distribution network (12) are respectively channelled via a control path (22, 23, 24, 25), each path comprising a flowmeter device (8, 9, 10, 11) and a control organ (34, 35, 36, 37). The mass fluxes of the individual components are controlled in proportion to the mass flux of a first component. The resultant controlled mass fluxes are introduced into a reservoir either directly, or once the individual mass fluxes have been partially or fully combined. The method and the device are particularly suitable for the on-site production of non-transportable mixtures of substances, or mixtures of substances that are costly to transport, such as highly concentrated peroxycarboxylic acid solutions.
摘要翻译：本发明涉及一种用于连续生产的物质的混合物，或通过反应包含形成在其中的组分的反应混合物。由一个储存器（1，2或3）或配电网络（12）绘制成分流在每种情况下通过一个控制系统（22，23，24，25），每个具有一个流量测量装置（8，9，10，11）和控制构件（34，35，36，37），引导。各个组分的流速成比例地调节至体积参照的第一组件的电流的量。将得到的调节质量流量被引入直接或单个质量的完全或部分合并流入容器之后。该方法和装置特别适用于现场生产非/消耗输送性材料的混合物，如高浓度的Peroxycarbonsäurelösungen。

5. 发明申请

WO01027078A1 PROCESS FOR PREPARING PEROXIDES USING MIXED ANHYDRIDES 审中-公开
标题翻译：使用混合无机物制备过氧化物的方法
公开(公告)号：WO01027078A1
公开(公告)日：2001-04-19
申请号：PCT/EP2000/009927
申请日：2000-10-09
IPC分类号： C07C407/00 , C07B61/00 , C07C68/02 , C07C69/96 , C07C409/24 , C07C409/34 , C07C409/38 , C08F4/32 , C08F4/34 , C08F20/00
CPC分类号： C07C69/96 , C07C409/24 , C07C409/34 , C07C409/38 , C07C2601/14
摘要： The invention relates to a process for the preparation of a peracid, perester or diacylperoxide and is characterized in that a mixed anhydride of formula: R [C(O)OC(O)OR ]n or [R C(O)OC(O)O]pR is contacted with a hydroperoxide of formula: R [OOH]m in the presence of a base, wherein R represents a mono-, di-, tri- or tetravalent C1-C19 hydrocarbon group, optionally containing one or more hetero atoms, n is 1-4, R represents a C1-C20 hydrocarbon group, optionally containing one or more hetero atoms, R represents a C1-C19 hydrocarbon group, optionally containing one or more hetero atoms, R represents a di-, tri- or tetravalent C1-C20 hydrocarbon group, optionally containing one or more hetero atoms, p is 2-4, R represents hydrogen or a mono- or divalent C3-C18 tertiary alkyl or C2-C20 acyl group, in which the tertiary alkyl or acyl group may optionally contain one or more hetero atoms, m is 1 or 2, and if R represents hydrogen, m is 1, provided that if the hydroperoxide is an alpha , alpha -dihydroperoxyperoxide, the reaction is not carried out in an inert two-phase solvent system comprising a polar solvent and an polar solvent. The invention also relates to a hydroxyperacid, hydroxyperester, and hydroxydiacylperoxide obtainable by said process and the use of said hydroxyperoxides.
摘要翻译：本发明涉及一种制备过酸，过氧化物或二酰基过氧化物的方法，其特征在于下列结构式的混合酸酐：R 1 [C（O）OC（O）OR 2] n或[ 3 C（O）OC（O）O] p R 4在碱的存在下与式R 5 [OOH] m的氢过氧化物接触，其中R 1表示单，二 - ，三价或四价的C 1 -C 19烃基，任选地含有一个或多个杂原子，n为1-4，R 2表示任选含有一个或多个杂原子的C 1 -C 20烃基，R 3，表示任选含有一个或多个杂原子的C 1 -C 19烃基，R 4表示二价，三价或四价C 1 -C 20烃基，任选地含有一个或多个杂原子，p为2-4，R 其中叔烷基或酰基可任选地含有一个或多个杂原子，m为1或2，并且如果R 1为氢或一或二价C 3 -C 18叔烷基或C 2 -C 20酰基， 5>表示氢，m为1，条件是如果水合过氧化氢是α，α-二氢过氧化氢，该反应不是在包含极性溶剂和极性溶剂的惰性两相溶剂系统中进行的。本发明还涉及通过所述方法和所述羟基过氧化物的使用可获得的羟基过酸，羟基过氧化物和羟基过氧化氢。

6. 发明申请

WO99014190A1 PROCESS FOR PREPARING EQUILIBRIUM PEROXY ACID AND PROCESS FOR PRODUCING LACTONE 审中-公开
标题翻译：制备平均过氧酸的方法和生产乳液的方法
公开(公告)号：WO99014190A1
公开(公告)日：1999-03-25
申请号：PCT/JP1998/004135
申请日：1998-09-14
IPC分类号： C07C409/24 , C07C409/26 , C07C407/00 , C07D313/04
CPC分类号： C07D315/00 , C07C407/00 , C07C407/003 , C07C409/24 , C07C409/26 , Y02P20/127
摘要： A process for preparing an equilibrium peroxy acid by the reaction of hydrogen peroxide with a carboxylic acid while removing the formed water in a reactive distillation device, the contents of the water and hydrogen peroxide in the acid being each 1.5 % by weight or less; and a process for producing a lactone by the reaction between the peroxy acid thus obtained and a cyclic ketone, which permits the selectivity of the lactone to be improved without lowering the activity of the ketone at an early stage of conversion.
摘要翻译：通过过氧化氢与羧酸的反应制备平衡过氧酸的方法，同时除去反应蒸馏装置中的形成的水，酸中的水和过氧化氢的含量为1.5重量％以下; 以及由此获得的过氧酸与环酮之间的反应生成内酯的方法，其能够在不降低酮转化的早期活性的情况下提高内酯的选择性而提高。

7. 发明申请

WO1992001669A1 PEROXY ACID GENERATOR 审中-公开
标题翻译：过氧酸发生器
公开(公告)号：WO1992001669A1
公开(公告)日：1992-02-06
申请号：PCT/US1990005604
申请日：1990-10-01
申请人： ECOLAB INCORPORATED
发明人： ECOLAB INCORPORATED , LOKKESMOE, Keith, D. , OAKES, Thomas, R.
IPC分类号： C07C409/24
CPC分类号： C11D3/3947 , A61L2/18 , A61L2/24 , C07C407/00 , C11D3/3945 , C07C409/24
摘要： We have found a new and useful process to generate peroxy acid sanitizing and bleaching compositions at the point-of-use, the process comprising introducing hydrogen peroxide and a carboxylic acid into a reactor at about 0.1 to 10 moles of hydrogen peroxide per mole of acid, and contacting the hydrogen peroxide and carboxylic acid in the presence of a sulfonic acid resin and in the substantial abssence of active metal ions which forms an aqueous peroxy acid composition at a concentration from about up to 20 wt %. Using this process, warewashing, laundry sanitizing and bleach, and hard surface sanitizing compositions can be produced.

8. 发明申请

WO1990014336A1 PEROXYACID MANUFACTURE 审中-公开
标题翻译：过氧化物制造
公开(公告)号：WO1990014336A1
公开(公告)日：1990-11-29
申请号：PCT/GB1990000793
申请日：1990-05-21
申请人： INTEROX CHEMICALS LIMITED , TROUGHTON, Nicholas, Arador , CARR, Graham , JAMES, Alun, Pryce , WILLSON, Andrew, John
发明人： INTEROX CHEMICALS LIMITED
IPC分类号： C07C407/00
CPC分类号： C07D209/48 , C07C407/00 , C07C407/003 , C07C409/24 , C07C409/40
摘要： In one class of processes for making poorly soluble organic peroxyacids the corresponding carboxylic acid is reacted with hydrogen peroxide in a reaction medium containing a high concentration of sulphuric acid. The presence of such constituents in the reaction mixture and the manner of the reactants and the way in which they are brought into contact, can result in the processes being hazardous. In the present invention, hazard problems are reduced or eliminated by first dissolving the carboxylic acid in concentrated sulphuric acid, secondly forming a Caro's acid solution containing a complementary amount of sulphuric acid and hydrogen peroxide within a predetermined range, and then introducing the carboxylic acid solution at a controlled rate in the Caro's acid solution, often over a period of from about 30 to 90 minutes, with agitation and temperature control. The compositions of the two reactant solutions are precalculated relative to each other such that the A value (weight ratio of sulphuric acid to the combined weight of it and water) either increases during addition of the carboxylic acid solution or if the latter is relatively less insoluble, stays the same or increases. The solutions are preferably formulated to provide an A value at the end of the reaction period selected in the range of around 0.7 to around 0.8, at a temperature of around 20 to 45 DEG C, the more soluble tending towards the lower end of each range and the less soluble towards the upper end of each range. The process is especially suitable for making poorly soluble aliphatic mono or diperoxycarboxylic acids such as peroxynonanoic acid or diperoxydodecanedioic acid, or for aromatic group substituted peroxyacids in which the peroxydation occurs in a primarily aliphatic environment, such as phthalimidoperoxyhexanoic acid.
摘要翻译：在一类制备难溶性有机过氧酸的方法中，相应的羧酸在含有高浓度硫酸的反应介质中与过氧化氢反应。反应混合物中这些组分的存在和反应物的方式以及它们接触的方式可导致该方法是危险的。在本发明中，通过首先将羧酸溶解在浓硫酸中，二次形成含有互补量的硫酸和过氧化氢的Caro酸溶液在预定范围内，然后将羧酸溶液以Caro酸溶液的控制速率，通常在约30至90分钟的时间内进行搅拌和温度控制。两种反应物溶液的组成相对于彼此预先计算，使得A值（硫酸与其与水的总重量的重量比）在加入羧酸溶液期间增加，或者如果后者相对较不溶解，保持不变或增加。优选将溶液配制成在约20至45℃的温度下在约0.7至约0.8范围内选择的反应周期结束时提供A值，对每个范围的下端的溶解度越趋向并且朝向每个范围的上端较少溶解。该方法特别适用于制备难溶的脂族单或二过氧羧酸如过氧壬酸或二过氧十二烷二酸，或芳族取代的过氧酸，其中过氧化在主要脂族环境中发生，例如邻苯二甲酰亚氨基过氧己酸。

9. 发明申请

WO1990007480A1 ACID CATALYZED PROCESS 审中-公开
标题翻译：酸催化工艺
公开(公告)号：WO1990007480A1
公开(公告)日：1990-07-12
申请号：PCT/US1990000054
申请日：1990-01-03
申请人： CATALYTICA, INC.
发明人： CATALYTICA, INC. , KING, David, L. , COOPER, Michael, D. , USHIBA, Ken, K. , SANDERSON, William, A.
IPC分类号： C07C05/22
CPC分类号： C07H3/02 , C07C2/26 , C07C2/58 , C07C37/08 , C07C37/14 , C07C37/20 , C07C41/09 , C07C45/455 , C07C45/46 , C07C45/49 , C07C45/53 , C07C45/72 , C07C45/74 , C07C51/14 , C07C201/08 , C07C407/00 , C07C409/24 , C07C409/26 , C07C2531/025 , C07C2531/10 , C07C2531/26 , C07C2531/38 , C07F9/3808 , Y02P20/52 , C07C205/06 , C07C39/04 , C07C43/043 , C07C43/06 , C07C39/06 , C07C39/16
摘要： The present invention provides a process for the conversion of a reactant into a reaction product in the presence of a solid acid catalyst comprising one or more fluorine atoms, sulfo radicals and phosphono radicals, each such radical being bonded to the same or different carbon atom, with the proviso that at least one sulfo radical and at least one phosphono radical are bonded to such carbon atoms through the sulfur atom and the phosphorus atom, respectively. These compounds are preferably non-polymeric, i.e. they have a molecular weight of about 5000 or less. The above acid catalysts may be reacted with a tetravalent metal, e.g. Zr, to provide a solid acid catalyst.
摘要翻译：本发明提供了在包含一个或多个氟原子，磺基和膦酰基的固体酸催化剂存在下将反应物转化成反应产物的方法，每个这样的基团键合到相同或不同的碳原子上，条件是至少一个磺基和至少一个膦酰基分别通过硫原子和磷原子键合到这些碳原子上。这些化合物优选是非聚合的，即其分子量为约5000或更小。上述酸催化剂可以与四价金属反应，例如 Zr，以提供固体酸催化剂。

10. 发明申请

WO2014200178A1 저산소증 검출 또는 이와 관련된 질환의 진단 방법 审中-公开
标题翻译：检测HYPOXIA或诊断与HYPOXIA相关的疾病的方法
公开(公告)号：WO2014200178A1
公开(公告)日：2014-12-18
申请号：PCT/KR2014/003770
申请日：2014-04-29
申请人： 서울대학교산학협력단
发明人： 박종완 , 신현우 , 조주연 , 이재서 , 홍일희
IPC分类号： G01N33/53 , G01N21/76 , G01N30/72
CPC分类号： G01N33/92 , C07C57/03 , C07C59/42 , C07C59/76 , C07C409/24 , G01N33/6893 , G01N2030/8813 , G01N2800/52 , G01N2800/54 , G01N2800/7038
摘要： 본원은 아라키돈산 및 그 유도체 검출용 물질을 포함하는 저산소증 검출 또는 저산소증 관련 질환 진단용 조성물, 키트 및 방법을 제공한다. 본원에 따른 조성물, 키트 및 방법은 생물학적 시료에서 생체 표지자의 검출을 통해 간편하고 신속하게 저산소증의 유무 검출 및 이를 이용하여, 저산소증에 의해 유발되는 질환의 예방 또는 조기 진단, 질환의 중증도, 치료 효과 판정 또는 경과추적 등에 유용하게 사용될 수 있다.
摘要翻译：本发明提供了用于检测缺氧或诊断缺氧相关疾病的组合物，试剂盒和方法，所述组合物含有用于检测花生四烯酸的材料及其衍生物。根据本发明的组合物，试剂盒和方法可以通过检测生物样品中的生物标志物来方便地及时地检测缺氧，因此可用于预防或早期诊断由缺氧引起的疾病，疾病的严重程度和治疗效果，疾病的追踪等。

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