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1. 发明授权

US5759739A Resist composition with polymeric dissolution inhibitor and alkali soluble resin 失效
标题翻译：抗溶剂组合物与聚合溶解抑制剂和碱溶性树脂
公开(公告)号：US5759739A
公开(公告)日：1998-06-02
申请号：US635856
申请日：1996-04-22
申请人： Katsuya Takemura , Toshinobu Ishihara , Kazumasa Maruyama , Yoshihumi Takeda , Minoru Shigemitsu , Ken'ichi Itoh
发明人： Katsuya Takemura , Toshinobu Ishihara , Kazumasa Maruyama , Yoshihumi Takeda , Minoru Shigemitsu , Ken'ichi Itoh
IPC分类号： G03F7/00 , G03F7/004 , G03F7/039 , G03C1/73
CPC分类号： G03F7/039 , G03F7/0045 , Y10S430/111
摘要： A resist composition comprising an alkali-soluble resin, typically a partially t-butoxycarbonylated polyhydroxystyrene, a p-butoxystyrene/t-butylacrylate copolymer or p-butoxystyrene/maleic anhydride copolymer as a dissolution inhibitor, and a iodonium or sulfonium salt as a photoacid generator is effective for forming a resist film which can be precisely and finely patterned using high energy radiation such as a KrF excimer laser.
摘要翻译：抗蚀剂组合物，其包含碱溶性树脂，通常为部分叔丁氧基羰基化的聚羟基苯乙烯，作为溶解抑制剂的对丁氧基苯乙烯/叔丁基丙烯酸酯共聚物或对丁氧基苯乙烯/马来酸酐共聚物，以及作为光酸产生剂的碘鎓盐或锍盐对于形成可以使用高能辐射如KrF准分子激光器精确和精细地图案化的抗蚀剂膜是有效的。

2. 发明授权

US5352564A Resist compositions 失效
标题翻译：抗蚀剂组合物
公开(公告)号：US5352564A
公开(公告)日：1994-10-04
申请号：US184171
申请日：1994-01-19
申请人： Yoshihumi Takeda , Toshinobu Ishihara , Ken'ichi Itoh , Kazumasa Maruyama
发明人： Yoshihumi Takeda , Toshinobu Ishihara , Ken'ichi Itoh , Kazumasa Maruyama
IPC分类号： G03F7/039 , G03F7/075 , G03C1/492
CPC分类号： G03F7/0758 , G03F7/039 , Y10S430/11
摘要： A resist composition comprising a base resin, an acid release agent, and a dissolution inhibitor is improved in sensitivity and resolution when the base resin is typically selected from poly-t-butoxystyrene/poly-hydroxystyrene, poly-t-butoxystyrene/poly-p-methoxymethoxystyrene/polyhydroxystyrene, and poly-t-butoxystyrene/poly-p-methoxystyrene/polyhydroxystyrene copolymers. The composition forms a resist useful for the manufacture of LSI.
摘要翻译：当基础树脂通常选自聚 - 丁氧基苯乙烯/聚 - 羟基苯乙烯，聚-t-丁氧基苯乙烯/多聚磷酸酯时，包含基础树脂，酸脱模剂和溶解抑制剂的抗蚀剂组合物的灵敏度和分辨率提高聚甲氧基苯乙烯/聚羟基苯乙烯和聚-t-丁氧基苯乙烯/聚对甲氧基苯乙烯/聚羟基苯乙烯共聚物。该组合物形成用于制造LSI的抗蚀剂。

3. 发明授权

US5691112A Sulfonium salt and chemically amplified positive resist composition 失效
标题翻译：锍盐和化学放大阳性抗蚀剂组成
公开(公告)号：US5691112A
公开(公告)日：1997-11-25
申请号：US762861
申请日：1996-12-10
申请人： Satoshi Watanabe , Youichi Ohsawa , Toshinobu Ishihara , Kazumasa Maruyama , Yoshihumi Takeda , Junji Shimada , Fujio Yagihashi , Katsuya Takemura
发明人： Satoshi Watanabe , Youichi Ohsawa , Toshinobu Ishihara , Kazumasa Maruyama , Yoshihumi Takeda , Junji Shimada , Fujio Yagihashi , Katsuya Takemura
IPC分类号： C07C317/22 , C07C381/12 , G03F7/004
CPC分类号： G03F7/0045 , C07C317/22 , C07C381/12
摘要： Trifluoromethanesulfonic and p-toluenesulfonic acid bis- or tris(p-tert-butoxyphenyl)sulfonium salts are novel. They are prepared from bis(p-tert-butoxyphenyl)sulfoxide which is also novel. A chemically amplified positive resist composition which contains the sulfonium salt as a photo-acid generator is highly sensitive to deep-UV rays, electron beams and X-rays, can be developed with alkaline aqueous solution to form a pattern, and is thus suitable for use in a fine patterning technique.
摘要翻译：三氟甲磺酸和对甲苯磺酸双或三（对叔丁氧基苯基）锍盐是新颖的。它们由双（对叔丁氧基苯基）亚砜制备，也是新的。含有锍盐作为光酸发生剂的化学增幅正性抗蚀剂组合物对深紫外线，电子束和X射线高度敏感，可以用碱性水溶液显影形成图案，因此适用于使用精细图案化技术。

4. 发明授权

US5633409A Tristertbutoxyphenyl sulfonium tosylate compound 失效
标题翻译：三叔丁氧基苯基锍甲苯磺酸酯化合物
公开(公告)号：US5633409A
公开(公告)日：1997-05-27
申请号：US379986
申请日：1995-01-27
申请人： Satoshi Watanabe , Youichi Ohsawa , Toshinobu Ishihara , Kazumasa Maruyama , Yoshihumi Takeda , Junji Shimada , Fujio Yagihashi , Katsuya Takemura
发明人： Satoshi Watanabe , Youichi Ohsawa , Toshinobu Ishihara , Kazumasa Maruyama , Yoshihumi Takeda , Junji Shimada , Fujio Yagihashi , Katsuya Takemura
IPC分类号： C07C317/22 , C07C381/12 , G03F7/004 , C07C319/00
CPC分类号： G03F7/0045 , C07C317/22 , C07C381/12
摘要： Trifluoromethanesulfonic and p-toluenesulfonic acid bis- or tris(p-tert-butoxyphenyl)sulfonium salts are novel. They are prepared from bis(p-tert-butoxyphenyl)sulfoxide which is also novel. A chemically amplified positive resist composition which contains the sulfonium salt as a photo-acid generator is highly sensitive to deep-UV rays, electron beams and X-rays, can be developed with alkaline aqueous solution to form a pattern, and is thus suitable for use in a fine patterning technique.
摘要翻译：三氟甲磺酸和对甲苯磺酸双或三（对叔丁氧基苯基）锍盐是新颖的。它们由双（对叔丁氧基苯基）亚砜制备，也是新的。含有锍盐作为光酸发生剂的化学增幅正性抗蚀剂组合物对深紫外线，电子束和X射线高度敏感，可以用碱性水溶液显影形成图案，因此适用于使用精细图案化技术。

5. 发明授权

US5728508A Method of forming resist pattern utilizing fluorinated resin antireflective film layer 失效
标题翻译：利用氟化树脂防反射膜层形成抗蚀剂图案的方法
公开(公告)号：US5728508A
公开(公告)日：1998-03-17
申请号：US672961
申请日：1996-07-01
申请人： Katsuya Takemura , Toshinobu Ishihara , Satoshi Watanabe , Kazumasa Maruyama , Hirofumi Kishita , Kouichi Yamaguchi
发明人： Katsuya Takemura , Toshinobu Ishihara , Satoshi Watanabe , Kazumasa Maruyama , Hirofumi Kishita , Kouichi Yamaguchi
IPC分类号： G03F7/09 , G03C1/835
CPC分类号： G03F7/091
摘要： A method of forming a resist pattern comprising forming a photoresist layer on a substrate, forming a transparent anti-reflective film on said photoresist layer by applying an anti-reflective material onto said photoresist layer, said anti-reflective material comprising a fluorinated resin which is soluble in an organic hydrocarbon solvent, exposing a light to said resist layer through said transparent anti-reflective film, removing said anti-reflective film using an organic hydrocarbon solvent, and developing said photoresist layer.
摘要翻译：一种形成抗蚀剂图案的方法，包括在基材上形成光致抗蚀剂层，在所述光致抗蚀剂层上形成透明的抗反射膜，通过在所述光致抗蚀剂层上施加抗反射材料，所述抗反射材料包括氟化树脂，可溶于有机烃溶剂中，通过所述透明抗反射膜将光暴露于所述抗蚀剂层，使用有机烃溶剂除去所述抗反射膜，并显影所述光致抗蚀剂层。

6. 发明授权

US5569784A Sulfonium salt and resist composition 失效
标题翻译：锍盐和抗蚀剂组成
公开(公告)号：US5569784A
公开(公告)日：1996-10-29
申请号：US379987
申请日：1995-01-27
申请人： Satoshi Watanabe , Junji Shimada , Youichi Ohsawa , Katsuya Takemura , Toshinobu Ishihara , Kazumasa Maruyama
发明人： Satoshi Watanabe , Junji Shimada , Youichi Ohsawa , Katsuya Takemura , Toshinobu Ishihara , Kazumasa Maruyama
IPC分类号： C07C381/12 , G03F7/004 , G03F7/039 , C07C217/48
CPC分类号： C07C381/12 , G03F7/0045 , G03F7/039
摘要： A novel sulfonium salt having at least one substituted aromatic group having acid labile groups and at least one nitrogenous aromatic group is provided. A chemically amplified, positive resist composition comprising the sulfonium salt as well as an alkali soluble resin and a dissolution inhibitor in an organic solvent has solved the PED problem.
摘要翻译：提供具有至少一个具有酸不稳定基团和至少一个含氮芳族基团的取代芳族基团的新型锍盐。在有机溶剂中包含锍盐以及碱溶性树脂和溶解抑制剂的化学增幅阳性抗蚀剂组合物解决了PED问题。

7. 发明授权

US5602241A Method for purifying polysaccharides 失效
标题翻译：多糖纯化方法
公开(公告)号：US5602241A
公开(公告)日：1997-02-11
申请号：US403450
申请日：1995-03-14
申请人： Kazumasa Maruyama , Kazuyuki Yamamoto , Shigehiro Nagura , Taira Homma
发明人： Kazumasa Maruyama , Kazuyuki Yamamoto , Shigehiro Nagura , Taira Homma
IPC分类号： C08B37/00 , C07G17/00 , C07H1/06
CPC分类号： C08B37/0003
摘要： A method for continuously precipitating a polysaccharide dissolved in an aqueous solution wherein a non-solvent for the polysaccharide is admixed with the aqueous solution to cause the polysaccharide to precipitate from the solution. The method includes the step of simultaneously feeding the aqueous solution containing the dissolved polysaccharide and the non-solvent through respective constant flow rate-pumps to produce non-pulsating metered first and second streams which are unaffected by pressure changes in the aqueous solution or the non-solvent fed to the respective pumps. The metered streams are simultaneously introduced from the respective pumps into a rotary turbine to mix the solution and the non-solvent and precipitate the polysaccharide. The precipitated polysaccharide is cut with an interlocking cutter which comprises a fixed cutter and a rotary cutter, and a suspension of finely cut polysaccharide particles is continuously withdrawn.
摘要翻译：将溶解在水溶液中的多糖连续沉淀的方法，其中将多糖的非溶剂与水溶液混合，使多糖从溶液中沉淀出来。该方法包括通过相应的恒定流量泵同时进料含有溶解的多糖和非溶剂的水溶液的步骤，以产生不受水溶液或非水溶液中的压力变化影响的非脉动计量的第一和第二流 - 供应到相应的泵。将计量流从各泵同时引入旋转涡轮机以混合溶液和非溶剂并沉淀多糖。沉淀的多糖用包括固定切割机和旋转切割机的互锁切割机切割，并且连续地取出细切多糖颗粒的悬浮液。

8. 发明授权

US4385078A Method for providing enteric coating on solid dosage forms and aqueous compositions therefor 失效
标题翻译：在固体剂型及其含水组合物上提供肠溶衣的方法
公开(公告)号：US4385078A
公开(公告)日：1983-05-24
申请号：US71298
申请日：1979-08-30
申请人： Yoshiro Onda , Hiroaki Muto , Hiroshi Suzuki , Kazumasa Maruyama , Atsushi Hatayama
发明人： Yoshiro Onda , Hiroaki Muto , Hiroshi Suzuki , Kazumasa Maruyama , Atsushi Hatayama
IPC分类号： A61K47/38 , A61K9/28 , C08L1/10 , C08L1/14
CPC分类号： A61K9/282 , A61K9/2866
摘要： A novel aqueous coating composition is proposed for providing enteric coating on solid dosage forms such as tablets. The aqueous coating composition of the invention comprises a fine powder of an enterosoluble cellulose derivative such as hydroxypropylmethylcellulose phthalate and hydroxypropylmethylcellulose acetate succinate, which is insoluble in water but can be plasticized and solubilized with certain plasticizing agents, as dispersed in an aqueous dispersing medium and a plasticizing agent having compatibility with the enterosoluble cellulose derivative and dissolved in the aqueous dispersing medium. The particle size of the enterosoluble cellulose derivative and the boiling point of the plasticizing agent is the key parameters and should be finer than 100 .mu.m in an average particle diameter and not lower than 100.degree. C., respectively. Upon application of the aqueous coating composition to the solid dosage forms, water as the dispersing medium is first evaporated leaving the cellulose derivative and the plasticizing agent, which latter solubilizes the former to form a continuous coating layer on the solid dosage forms imparting good and satisfactory enterosolubility thereto.
摘要翻译：提出了一种新颖的水性涂料组合物，用于在诸如片剂的固体剂型上提供肠溶衣。本发明的水性涂料组合物包括不溶于水但可以用某些增塑剂增塑和溶解的分散在水分散介质中的肠溶性纤维素衍生物如羟丙基甲基纤维素邻苯二甲酸酯和羟丙基甲基纤维素乙酸酯琥珀酸盐的细粉末，增塑剂与肠溶性纤维素衍生物具有相容性并溶于水分散介质中。肠溶性纤维素衍生物的粒径和增塑剂的沸点是关键参数，平均粒径分别小于100μm，不低于100℃。当将水性涂料组合物施用于固体剂型时，首先蒸发作为分散介质的水，留下纤维素衍生物和增塑剂，后者溶解前者，在固体剂型上形成连续涂层，赋予良好和令人满意的效果肠溶性。

9. 发明授权

US4226981A Ether-ester derivatives of cellulose and their applications 失效
标题翻译：纤维素的醚酯衍生物及其应用
公开(公告)号：US4226981A
公开(公告)日：1980-10-07
申请号：US944177
申请日：1978-09-20
申请人： Yoshiro Onda , Hiroaki Muto , Kazumasa Maruyama
发明人： Yoshiro Onda , Hiroaki Muto , Kazumasa Maruyama
IPC分类号： A61K9/28 , A61K9/36 , C08B13/00 , G03C1/835 , B44D1/50 , G03C1/92
CPC分类号： A61K9/2866 , C08B13/00 , G03C1/835
摘要： A novel cellulose derivative provided in this invention is a mixed ester of an alkoxy or hydroxyalkoxy substituted cellulose ether, prepared by the esterification reaction of the ether with succinic anhydride and an anhydride of an aliphatic monocarboxylic acid. The cellulose derivatives are advantageous because of their capability of producing enteric coatings having sufficient flexibility without the use of a plasticizer as well as by their chemical and physical stability against moisture, and also by easy purification after completion of the esterification reaction. The coatings produced from the derivatives have a similar chemical and physical stability. The cellulose derivatives are useful for the enteric coating of pharmaceutical dosage forms and also for providing halation-preventing layers on photographic films.
摘要翻译：本发明提供的新型纤维素衍生物是通过醚与琥珀酸酐的酯化反应和脂族一元羧酸的酸酐制备的烷氧基或羟基烷氧基取代的纤维素醚的混合酯。纤维素衍生物是有利的，因为它们具有在不使用增塑剂的情况下具有足够柔韧性的肠溶衣的能力，以及它们对水分的化学和物理稳定性以及酯化反应完成后容易的纯化。由衍生物生产的涂料具有相似的化学和物理稳定性。纤维素衍生物可用于药物剂型的肠溶包衣以及用于在照相胶片上提供防晕层。

10. 发明授权

US5416206A Modified xanthan gum and method for modifying xanthan gum 失效
标题翻译：改性黄原胶和改性黄原胶的方法
公开(公告)号：US5416206A
公开(公告)日：1995-05-16
申请号：US984215
申请日：1992-11-30
申请人： Shigehiro Nagura , Kanji Murofushi , Kazumasa Maruyama
发明人： Shigehiro Nagura , Kanji Murofushi , Kazumasa Maruyama
IPC分类号： A23L29/20 , C08B37/00 , C07H1/00 , C07H3/06
CPC分类号： C08B37/0033
摘要： A modified xanthan gum has a viscosity of not less than 800 cP as determined on a 0.5% by weight solution thereof in a 12% by weight aqueous sodium chloride solution at 20.degree. C. and a ratio of this viscosity to that determined on a 0.5% by weight solution thereof in distilled water of not less than 1.5. The modified xanthan gum can be prepared by a method comprising the steps of mixing an organic solvent which does not dissolve xanthan gum and is hydrophilic with an aqueous solution of xanthan gum in a mixer, cutting, into fine fibrous materials, deposites formed in the mixed solution together with the mixed solution with a cutter, separating and recovering the suspended fine fibrous materials from the mixed solution and then drying the materials at a temperature of not more than 80.degree. C. The modified xanthan gum can directly be dissolved in aqueous solutions of salts such as common salt even at room temperature and can thus easily show a desired effect of thickening the aqueous salt solutions.
摘要翻译：改性黄原胶具有不低于800cP的粘度，其在20重量％的12重量％氯化钠水溶液中的0.5重量％溶液测得，并且该粘度与在0.5 其重量百分比在蒸馏水中的溶液不低于1.5。改性黄原胶可以通过以下方法制备，该方法包括以下步骤：在混合器中混合不溶于黄原胶并且与黄原胶水溶液亲水的有机溶剂，将其切割成细纤维材料，混合形成的沉积物溶液与混合溶液与切割器一起分离并从混合溶液中回收悬浮的细纤维材料，然后在不高于80℃的温度下干燥材料。改性的黄原胶可以直接溶于即使在室温下也可以使用盐，例如盐，因此可容易地显示出使盐水溶液变稠的期望效果。

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