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1. 发明申请

US20050051917A1 Devices and methods for the production of particles 失效
标题翻译：用于生产颗粒的装置和方法
公开(公告)号：US20050051917A1
公开(公告)日：2005-03-10
申请号：US10483194
申请日：2002-07-10
申请人： Willy Grothe , Daniel Jarmer , Corinne Lengsfeld , Theodore Randolph
发明人： Willy Grothe , Daniel Jarmer , Corinne Lengsfeld , Theodore Randolph
IPC分类号： B01D11/04 , B01F5/00 , B01J2/04 , B29B9/00
CPC分类号： B01J2/04 , B01D11/0403 , B01D11/0407 , B01D11/0473 , B01F5/0057 , B01F2003/0064
摘要： The present invention provides methods and devices for producing particles with an average diameter less than about 15 μm using the precipitation with compressed fluid-antisolvent (PCA) process and the carbon-dioxide assisted nebulization with a bubble dryer (CAN-BD) process. In the methods and nozzles of the invention, at least one jet of supercritical or near-supercritical fluid and at least one jet of solution interact to mix the supercritical or near-supercritical fluid and the solution within a chamber. The solution contains at least one solvent and at least one solute. At least one of the jets is a swirling jet. To form particles, the solvent and supercritical or near-supercritical fluid are then injected into a PCA or a CAN-BD process chamber. The degree of mixing depends in part on the power input into the mixing chamber. Power inputs of about 6.5×109 W/m3 enhance the degree of mixing and allow production of nanoscale particles with the PCA process. The nanoscale particles have a size distribution so that polydispersity is less than about 1.75.
摘要翻译：本发明提供了使用压缩流体 - 反溶剂（PCA）沉淀法和用气泡干燥器（CAN-BD）方法进行二氧化碳辅助雾化来生产平均直径小于约15μm的颗粒的方法和装置。在本发明的方法和喷嘴中，至少一个超临界或近超临界流体射流和至少一个溶液射流相互作用以将超临界或近超临界流体和溶液在腔室内混合。该溶液含有至少一种溶剂和至少一种溶质。至少有一架喷气式飞机是旋流式飞机。为了形成颗粒，然后将溶剂和超临界或近临界流体注入PCA或CAN-BD处理室中。混合程度部分取决于输入混合室的功率。大约6.5×10 9 W / m 3的功率输入提高了混合的程度，并允许用PCA工艺生产纳米级颗粒。纳米级颗粒具有尺寸分布，使得多分散性小于约1.75。

2. 发明授权

US07332111B2 Devices and methods for the production of particles 失效
标题翻译：用于生产颗粒的装置和方法
公开(公告)号：US07332111B2
公开(公告)日：2008-02-19
申请号：US10483194
申请日：2002-07-10
申请人： Willy Grothe , Daniel Jarmer , Corinne Lengsfeld , Theodore Randolph
发明人： Willy Grothe , Daniel Jarmer , Corinne Lengsfeld , Theodore Randolph
IPC分类号： B29B9/00
CPC分类号： B01J2/04 , B01D11/0403 , B01D11/0407 , B01D11/0473 , B01F5/0057 , B01F2003/0064
摘要： The present invention provides methods and devices for producing particles with an average diameter less than about 15 μm using the precipitation with compressed fluid-antisolvent (PCA) process and the carbon-dioxide assisted nebulization with a bubble dryer (CAN-BD) process. In the methods and nozzles of the invention, at least one jet of supercritical or near-supercritical fluid and at least one jet of solution interact to mix the supercritical or near-supercritical fluid and the solution within a chamber. The solution contains at least one solvent and at least one solute. At least one of the jets is a swirling jet. To form particles, the solvent and supercritical or near-supercritical fluid are then injected into a PCA or a CAN-BD process chamber. The degree of mixing depends in part on the power input into the mixing chamber. Power inputs of about 6.5×109 W/m3 enhance the degree of mixing and allow production of nanoscale particles with the PCA process. The nanoscale particles have a size distribution so that polydispersity is less than about 1.75.
摘要翻译：本发明提供了使用压缩流体 - 反溶剂（PCA）沉淀法和用气泡干燥器（CAN-BD）方法进行二氧化碳辅助雾化来生产平均直径小于约15μm的颗粒的方法和装置。在本发明的方法和喷嘴中，至少一个超临界或近超临界流体射流和至少一个溶液射流相互作用以将超临界或近超临界流体和溶液在腔室内混合。该溶液含有至少一种溶剂和至少一种溶质。至少有一架喷气式飞机是旋流式飞机。为了形成颗粒，然后将溶剂和超临界或近临界流体注入PCA或CAN-BD处理室中。混合程度部分取决于输入混合室的功率。大约6.5×10 9 W / m 3的功率输入提高了混合的程度并允许用PCA工艺生产纳米尺寸的颗粒。纳米级颗粒具有尺寸分布，使得多分散性小于约1.75。

3. 发明申请

US20060140848A1 Solar-thermal fluid-wall reaction processing 审中-公开
公开(公告)号：US20060140848A1
公开(公告)日：2006-06-29
申请号：US11354544
申请日：2006-02-14
申请人： Alan Weimer , Jaimee Dahl , Allan Lewandowski , Carl Bingham , Karen J. Buechler , Willy Grothe
发明人： Alan Weimer , Jaimee Dahl , Allan Lewandowski , Carl Bingham , Karen J. Buechler , Willy Grothe
IPC分类号： C09C1/48
CPC分类号： B01J8/0045 , B01J8/025 , B01J8/087 , B01J10/002 , B01J19/127 , B01J2208/00212 , B01J2208/0038 , B01J2208/00451 , B01J2208/00513 , B01J2208/00522 , B01J2208/00752 , B01J2219/00006 , B01J2219/0272 , B01J2219/0883 , C01B3/04 , C01B3/24 , C01B3/34 , C01B3/344 , C01B17/0495 , C01B2203/0216 , C01B2203/0222 , C01B2203/0272 , C01B2203/04 , C01B2203/049 , C01B2203/0805 , C01B2203/0833 , C01B2203/085 , C01B2203/0866 , C01P2006/80 , C09C1/48 , F24S20/20 , F28C3/12 , Y02E10/41 , Y02E60/364 , Y02P20/134
摘要： The present invention provides a method for carrying out high temperature thermal dissociation reactions requiring rapid-heating and short residence times using solar energy. In particular, the present invention provides a method for carrying out high temperature thermal reactions such as dissociation of hydrocarbon containing gases and hydrogen sulfide to produce hydrogen and dry reforming of hydrocarbon containing gases with carbon dioxide. In the methods of the invention where hydrocarbon containing gases are dissociated, fine carbon black particles are also produced. The present invention also provides solar-thermal reactors and solar-thermal reactor systems.

4. 发明授权

US08673035B2 Solar-thermal reaction processing 失效
标题翻译：太阳热反应加工
公开(公告)号：US08673035B2
公开(公告)日：2014-03-18
申请号：US13088185
申请日：2011-04-15
申请人： Alan W Weimer , Jaimee K Dahl , Allan A Lewandowski , Carl Bingham , Karen J Raska Buechler , Willy Grothe
发明人： Alan W Weimer , Jaimee K Dahl , Allan A Lewandowski , Carl Bingham , Karen J Raska Buechler , Willy Grothe
IPC分类号： B01J7/00 , C10J3/00 , C01B3/24
CPC分类号： B01J8/0045 , B01J8/025 , B01J8/087 , B01J10/002 , B01J19/127 , B01J2208/00212 , B01J2208/0038 , B01J2208/00451 , B01J2208/00513 , B01J2208/00522 , B01J2208/00752 , B01J2219/00006 , B01J2219/0272 , B01J2219/0883 , C01B3/04 , C01B3/24 , C01B3/34 , C01B3/344 , C01B17/0495 , C01B2203/0216 , C01B2203/0222 , C01B2203/0272 , C01B2203/04 , C01B2203/049 , C01B2203/0805 , C01B2203/0833 , C01B2203/085 , C01B2203/0866 , C01P2006/80 , C09C1/48 , F24S20/20 , F28C3/12 , Y02E10/41 , Y02E60/364 , Y02P20/134
摘要： In an embodiment, a method of conducting a high temperature chemical reaction that produces hydrogen or synthesis gas is described. The high temperature chemical reaction is conducted in a reactor having at least two reactor shells, including an inner shell and an outer shell. Heat absorbing particles are included in a gas stream flowing in the inner shell. The reactor is heated at least in part by a source of concentrated sunlight. The inner shell is heated by the concentrated sunlight. The inner shell re-radiates from the inner wall and heats the heat absorbing particles in the gas stream flowing through the inner shell, and heat transfers from the heat absorbing particles to the first gas stream, thereby heating the reactants in the gas stream to a sufficiently high temperature so that the first gas stream undergoes the desired reaction(s), thereby producing hydrogen or synthesis gas in the gas stream.
摘要翻译：在一个实施方案中，描述了进行产生氢气或合成气体的高温化学反应的方法。高温化学反应在具有至少两个反应器壳的反应器中进行，所述反应器壳包括内壳和外壳。在内壳中流动的气流中包含吸热颗粒。反应器至少部分由浓度太阳光源加热。内壳由集中的阳光加热。内壳从内壁再辐射并加热流过内壳的气流中的吸热颗粒，并将热量从吸热颗粒转移到第一气流，从而将气流中的反应物加热至足够高的温度使得第一气流经历所需的反应，从而在气流中产生氢气或合成气。

5. 发明授权

US07033570B2 Solar-thermal fluid-wall reaction processing 失效
公开(公告)号：US07033570B2
公开(公告)日：2006-04-25
申请号：US10383875
申请日：2003-03-07
申请人： Alan W. Weimer , Jaimee K. Dahl , Allan A. Lewandowski , Carl Bingham , Karen J. Raska Buechler , Willy Grothe
发明人： Alan W. Weimer , Jaimee K. Dahl , Allan A. Lewandowski , Carl Bingham , Karen J. Raska Buechler , Willy Grothe
IPC分类号： C01B3/26
CPC分类号： B01J8/0045 , B01J8/025 , B01J8/087 , B01J10/002 , B01J19/127 , B01J2208/00212 , B01J2208/0038 , B01J2208/00451 , B01J2208/00513 , B01J2208/00522 , B01J2208/00752 , B01J2219/00006 , B01J2219/0272 , B01J2219/0883 , C01B3/04 , C01B3/24 , C01B3/34 , C01B3/344 , C01B17/0495 , C01B2203/0216 , C01B2203/0222 , C01B2203/0272 , C01B2203/04 , C01B2203/049 , C01B2203/0805 , C01B2203/0833 , C01B2203/085 , C01B2203/0866 , C01P2006/80 , C09C1/48 , F24S20/20 , F28C3/12 , Y02E10/41 , Y02E60/364 , Y02P20/134
摘要： The present invention provides a method for carrying out high temperature thermal dissociation reactions requiring rapid-heating and short residence times using solar energy. In particular, the present invention provides a method for carrying out high temperature thermal reactions such as dissociation of hydrocarbon containing gases and hydrogen sulfide to produce hydrogen and dry reforming of hydrocarbon containing gases with carbon dioxide. In the methods of the invention where hydrocarbon containing gases are dissociated, fine carbon black particles are also produced. The present invention also provides solar-thermal reactors and solar-thermal reactor systems.

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