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1. 发明授权

US5608116A Process for the alkoxylation of fluorinated alcohols 失效
标题翻译：氟化醇的烷氧基化方法
公开(公告)号：US5608116A
公开(公告)日：1997-03-04
申请号：US405327
申请日：1995-03-16
申请人： Robert A. Halling , Hsu-Nan Huang
发明人： Robert A. Halling , Hsu-Nan Huang
IPC分类号： B01J31/14 , B01F17/00 , B01J27/08 , C07B61/00 , C07C41/03 , C07C43/11 , C07C217/28 , C07C231/12 , C07C233/18 , C07C303/40 , C07C311/04 , C07C311/09 , C08G65/26 , C08G65/28 , C11D1/00
CPC分类号： B01F17/0035 , C07C217/28 , C07C303/40 , C07C41/03 , C08G65/2639 , C11D1/004
摘要： The present invention relates to the preparation of fluoroalkylalkoxylates in which one reacts at least one fluorinated alcohol with at least one alkylene epoxide in the presence of a novel catalyst system comprising an iodine source and an alkali metal borohydride.
摘要翻译：本发明涉及氟代烷基烷氧基化物的制备，其中在包含碘源和碱金属硼氢化物的新型催化剂体系的存在下，使至少一种氟化醇与至少一种亚烷基环氧化物反应。

2. 发明授权

US5567857A Fluoroalkylethoxylate compositions having enhanced water solubility 失效
标题翻译：具有增强的水溶性的氟烷基乙氧基化物组合物
公开(公告)号：US5567857A
公开(公告)日：1996-10-22
申请号：US263091
申请日：1994-06-21
申请人： Hsu-Nan Huang , Robert A. Halling
发明人： Hsu-Nan Huang , Robert A. Halling
IPC分类号： B01J31/14 , B01F17/00 , C07B61/00 , C07C41/03 , C07C43/11 , C07C217/28 , C07C303/40 , C07C311/09 , C08G65/26 , C08G65/28 , C11D1/00
CPC分类号： C07C217/28 , B01F17/0035 , C07C303/40 , C07C41/03 , C07C43/11 , C08G65/2639 , C11D1/004
摘要： Mixture of the compounds: F(CF.sub.2).sub.m --(CH.sub.2).sub.n --(OCH.sub.2 CH.sub.2)p--OH wherein m=2 and about 20, but in at least 5 weight % of molecules m is 8 or higher or mixtures of the same, but in no more than 5 weight % of the molecules is m equal to 14 or higher or mixtures of the same; n=1 to 3; & p=1 to 40, but the mixture has an average p=8 to 17.
摘要翻译：化合物的混合物：F（CF 2）m - （CH 2）n - （OCH 2 CH 2）p -OH，其中m = 2和约20，但至少5重量％的分子m为8或更高或其混合物，但不超过5重量％的分子m等于14或更高或其混合物; n = 1〜3; ＆p = 1〜40，但混合物的平均p = 8〜17。

3. 发明授权

US5442011A Polymeric fluorocarbon siloxanes, emulsions and surface coatings thereof 失效
标题翻译：聚合碳氟硅氧烷，乳液及其表面涂层
公开(公告)号：US5442011A
公开(公告)日：1995-08-15
申请号：US205988
申请日：1994-03-04
申请人： Robert A. Halling
发明人： Robert A. Halling
IPC分类号： C08L83/08 , C04B41/49 , C04B41/64 , C08G77/22 , C08G77/24 , C08G77/26 , C08L83/04 , C09D183/04 , C09D183/08 , C08L83/06
CPC分类号： C04B41/009 , C04B41/4961 , C04B41/64 , C08G77/24 , C08G77/26 , C09D183/08 , C04B2111/00517 , C04B2111/203 , C04B2111/27 , Y10T428/31663
摘要： Novel polymeric fluorocarbon siloxane represented by the formula: ##STR1## and corresponding polymeric branched structures wherein R.sub.a is a perfluoroalkyl radical, R.sub.b is an aminoalkyl or substituted aminoalkyl radical and R.sub.c hydrocarbyl, substituted hydrocarbyl phenyl, substituted phenyl or cyanoalkyl radical are shown to form stable aqueous emulsions without the use of volatile organic solvents and by a low energy processing. These emulsion are found to be highly hydrolyzed in solution without leading to precipitation via intermolecular condensation The emulsions when applied to substrates impart both oil and water repellent properties as well as improved lubricity.
摘要翻译：由式R 1 [OSi（Ra）（OR 1）x- [OSi（R b）（OR 1）] y - [OSi（R c）（OR 1）] z-OR 1表示的新型聚合氟碳硅氧烷及其相应的聚合支链结构，其中 Ra是全氟烷基，Rb是氨基烷基或取代的氨基烷基，Rc烃基，取代的烃基苯基，取代的苯基或氰基烷基显示形成稳定的水乳液，而不使用挥发性有机溶剂和低能量处理。发现这些乳液在溶液中高度水解，不会导致通过分子间缩合而沉淀。当施加到基材上时，乳液赋予防油和防水性能以及改善的润滑性。

4. 发明授权

US5552476A Hydrolyzed silane emulsions and their use as surface coatings 失效
标题翻译：水解硅烷乳液及其用作表面涂料
公开(公告)号：US5552476A
公开(公告)日：1996-09-03
申请号：US248613
申请日：1994-05-12
申请人： Robert A. Halling
发明人： Robert A. Halling
IPC分类号： C08J7/04 , C03C17/30 , C04B41/49 , C04B41/64 , C04B41/80 , C07F7/18 , C09D4/00 , D06M13/02 , D06M13/513 , C08J3/03 , C08J3/07 , B05D1/00 , B01F17/54
CPC分类号： D06M13/513 , C03C17/30 , C04B41/4922 , C04B41/4933 , C07F7/1836 , C09D4/00
摘要： Novel and highly reactive hydrolyzed silane emulsions are achieved by emulsifying a hydrolyzable alkoxysilane (e.g., or the like) in water in the presence of an effective amount of an emulsifier of sufficiently high HLB value (preferably 14 or greater) to simultaneously retain said hydrolyzable alkoxysilane compound in a substantially totally hydrolyzed state and inhibit said resulting hydrolyzed alkoxysilane compound from self-condensation. Such reactive emulsions containing hydrocarbon silanes are useful to produce durable coatings that impart water repellency and lubricity to substrates having siliceous, cellulosic or proteinaceous surfaces.
摘要翻译：通过在有效量的HLB值（优选为14或更高）的HLB值的乳化剂的存在下，在水中乳化水解性烷氧基硅烷（例如等）来实现新型和高反应性水解硅烷乳液，以同时保留所述可水解的烷氧基硅烷化合物基本上完全水解的状态，并且抑制所得到的水解烷氧基硅烷化合物自缩合。含有烃硅烷的这种反应性乳液可用于生产耐久性涂料，其赋予具有硅质，纤维素或蛋白质表面的底物的疏水性和润滑性。

5. 发明授权

US5550184A Hydrolyzed silane emulsions and their use as surface coatings 失效
标题翻译：水解硅烷乳液及其用作表面涂料
公开(公告)号：US5550184A
公开(公告)日：1996-08-27
申请号：US206779
申请日：1994-03-04
申请人： Robert A. Halling
发明人： Robert A. Halling
IPC分类号： C08J7/04 , C03C17/30 , C04B41/49 , C04B41/64 , C04B41/80 , C07F7/18 , C09D4/00 , D06M13/02 , D06M13/513 , C08J3/03 , C08J3/07 , C09D183/06
CPC分类号： D06M13/513 , C03C17/30 , C04B41/4922 , C04B41/4933 , C07F7/1836 , C09D4/00
摘要： Novel and highly reactive hydrolyzed silane emulsions are achieved by emulsifying a hydrolyzable alkoxysilane (e.g., perfluoroalkylethyltris(2-(2-methoxyethoxy)ethoxy)silane, 2-perfluoroalkylethyltris(2-(2-(2-methoxyethoxy)ethoxy)ethoxy) silane, 2-Perfluoroalkylethyltris(polyoxyethyleneglycolmonomethylether)silane or the like) in water in the presence of an effective amount of an emulsifier of sufficiently high HLB value (preferably 14 or greater) to simultaneously retain said hydrolyzable alkoxysilane compound in a substantially totally hydrolyzed state and inhibit said resulting hydrolyzed alkoxysilane compound from self-condensation. Such reactive emulsions containing fluorocarbon silanes are useful to produce durable coatings that impart oil and water repellency to substrates having siliceous, cellulosic or proteinaceous surfaces.
摘要翻译：新颖的和高反应性的硅烷水解乳剂由乳化水解烷氧基硅烷（例如实现，perfluoroalkylethyltris（2-（2-甲氧基乙氧基）乙氧基）硅烷，2- perfluoroalkylethyltris（2-（2-（2-甲氧基乙氧基）乙氧基）乙氧基）硅烷， 2- Perfluoroalkylethyltris在有效量足够高HLB值的乳化剂的存在下，在水（polyoxyethyleneglycolmonomethylether）硅烷等）（优选为14或更大）同时保持所述以基本上完全水解的状态和可水解烷氧基硅烷化合物禁止所述从自缩合得到水解的烷氧基硅烷化合物。含有氟碳硅烷的这种反应性乳液可用于生产耐油和防水性的耐油涂层，该基材具有硅质，纤维素或蛋白质表面。

6. 发明授权

US5239019A Modified hydrophilic polyesters 失效
标题翻译：改性水解聚酯
公开(公告)号：US5239019A
公开(公告)日：1993-08-24
申请号：US571571
申请日：1990-09-07
申请人： Robert A. Halling , Davis E. Lee , Charles F. Palmer, Jr.
发明人： Robert A. Halling , Davis E. Lee , Charles F. Palmer, Jr.
IPC分类号： D06M11/00 , D04H1/02 , D04H1/42 , D04H1/435 , D04H1/542 , D04H1/74 , D06M13/02 , D06M13/192 , D06M13/322 , D06M13/368 , D06M13/372 , D06M13/402 , D06M13/432 , D06M15/507 , D06M15/53 , D06M101/00 , D06M101/16 , D06M101/30 , D06M101/32
CPC分类号： D04H1/435 , D04H1/4382 , D04H1/4391 , D04H1/542 , D04H1/74 , D06M15/507
摘要： A hydrophilic copolyester containing both polyoxyethylene diester and alkylene diester segments, and optionally containing other components, which copolyester has been modified after being formed by reaction with one or more polyols containing three or more hydroxy groups or one or more polyoxyethylene glycols or a mixture of one or more of such polyols and one or more of such glycols. The copolyester can be used in treating fibers and films.

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