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1. 发明授权

US5567857A Fluoroalkylethoxylate compositions having enhanced water solubility 失效
标题翻译：具有增强的水溶性的氟烷基乙氧基化物组合物
公开(公告)号：US5567857A
公开(公告)日：1996-10-22
申请号：US263091
申请日：1994-06-21
申请人： Hsu-Nan Huang , Robert A. Halling
发明人： Hsu-Nan Huang , Robert A. Halling
IPC分类号： B01J31/14 , B01F17/00 , C07B61/00 , C07C41/03 , C07C43/11 , C07C217/28 , C07C303/40 , C07C311/09 , C08G65/26 , C08G65/28 , C11D1/00
CPC分类号： C07C217/28 , B01F17/0035 , C07C303/40 , C07C41/03 , C07C43/11 , C08G65/2639 , C11D1/004
摘要： Mixture of the compounds: F(CF.sub.2).sub.m --(CH.sub.2).sub.n --(OCH.sub.2 CH.sub.2)p--OH wherein m=2 and about 20, but in at least 5 weight % of molecules m is 8 or higher or mixtures of the same, but in no more than 5 weight % of the molecules is m equal to 14 or higher or mixtures of the same; n=1 to 3; & p=1 to 40, but the mixture has an average p=8 to 17.
摘要翻译：化合物的混合物：F（CF 2）m - （CH 2）n - （OCH 2 CH 2）p -OH，其中m = 2和约20，但至少5重量％的分子m为8或更高或其混合物，但不超过5重量％的分子m等于14或更高或其混合物; n = 1〜3; ＆p = 1〜40，但混合物的平均p = 8〜17。

2. 发明授权

US5070213A Perfluoro-4,4'-bis(2,2-dimethyl-1,3-dioxolane) and its preparation and use 失效
标题翻译：全氟-4,4'-双（2,2-二甲基-1,3-二氧戊环）及其制备和用途
公开(公告)号：US5070213A
公开(公告)日：1991-12-03
申请号：US568810
申请日：1990-08-17
申请人： Hsu-Nan Huang , Ming-Hong Hung , Carl G. Krespan
发明人： Hsu-Nan Huang , Ming-Hong Hung , Carl G. Krespan
IPC分类号： A61K49/06 , C07D317/16 , C07D317/42
CPC分类号： C07D317/42 , A61K49/06 , C07D317/16 , Y10T436/24
摘要： The novel compound perfluoro-4,4'-bis(2,2-dimethyl-1,3-dioxolane) is disclosed. Its preparation by fluorination of 4,4'-bis[2,2-bis(trifluoromethyl)-1,3-dioxolane using UV radiation or by reaction of 2,2-bis(trifluoromethyl)-4-iodo-4,5,5-trifluoromethyl-1,3-dioxolane with zinc in acetic anhydride and methylene chloride is also disclosed. The infusion of perfluoro-4,4'-bis(2,2-dimethyl-1,3-dioxolane) into mammalian tissue to facilitate inspection thereof by muclear magnetic resonance imaging is also disclosed.
摘要翻译：公开了新型化合物全氟-4,4'-双（2,2-二甲基-1,3-二氧戊环）。通过使用紫外线辐射或通过2,2-二（三氟甲基）-4-碘-4,5,5-三氟苯酚的反应将4,4'-双[2,2-双（三氟甲基）-1,3-二氧戊环氟化）还公开了含有锌在乙酸酐和二氯甲烷中的5-三氟甲基-1,3-二氧戊环。还公开了将全氟-4,4'-双（2,2-二甲基-1,3-二氧戊环）输入哺乳动物组织以便于通过核磁共振成像进行检查。

3. 发明申请

US20090017321A1 Amphoteric fluorochemicals for paper 有权
标题翻译：两性氟化合物用于纸张
公开(公告)号：US20090017321A1
公开(公告)日：2009-01-15
申请号：US11827006
申请日：2007-07-10
申请人： Hsu-Nan Huang , Martial Jean-Jacques Pabon , Romain Severac , Lamia Heuze
发明人： Hsu-Nan Huang , Martial Jean-Jacques Pabon , Romain Severac , Lamia Heuze
IPC分类号： C08F12/30 , B32B23/08 , C08F16/24 , C08F2/06
CPC分类号： C09D133/18 , C08F220/06 , C08F220/24 , C08F220/34 , D21H17/11 , D21H17/36 , D21H17/37 , D21H21/14 , D21H21/16 , Y10T428/31895 , Y10T442/2279 , Y10T442/2287
摘要： A method of imparting oil repellency to flexible, fibrous, nonwoven substrates comprising contacting the substrate with a composition prepared from polymerization of monomers in the following percentages by weight: (a) from about 60% to about 90% of a monomer of Formula 1 or a mixture thereof: Rf-Q-CO—CR═CH2 Formula 1 wherein: Rf is a straight- or branched-chain perfluoroalkyl group of 2 to about 20 carbon atoms, R is H or CH3, Q is —(CnH2n)pSO2NR1(CnH2nO)y—, wherein the —(CnH2n) is bonded to Rf, and R1 is H or C1-C20 alkyl; (b) from about 10% to about 25% of a monomer of Formula 2 or a mixture thereof: CH2═C(R)COZ(CH2)q(CHR)rNR2R3 Formula 2 wherein R2 and R3 are each independently C1-C4 alkyl, hydroxyethyl, or benzyl or R2 and R3 together with the nitrogen atom form a morpholine, pyrrolidine, or piperidine ring, and Z is —O— or —NR4— wherein R4 is H or C1-C4 alkyl; and (c) from about 1% to about 15% of a monomer of Formula 3 or a mixture thereof: CH2═CR(R5)e—COOH Formula 3 wherein R5 is CO(CH2)5, CO—O—(CH2)2, C6H4CHR, or CONRR6, and R6 is C6H4OCH2, (CH2)d, or C(CH3)2CH2.
摘要翻译：包括使柔性纤维状非织造基材赋予拒油性的方法，包括使底物与按单体聚合制备的组合物接触，重量百分比如下：（a）约60％至约90％的式1单体或其混合物：<？in-line-formula description =“In-line Formulas”end =“lead”？> Rf-Q-CO-CR-CH2 Formula 1 <？in-line-formula description =“In-line 式中：R f为2-约20个碳原子的直链或支链全氟烷基，R为H或CH 3，Q为 - （C n H 2n）p SO 2 NR 1（C n H 2n O）y - ，其中 - （C n H 2n）键合到R f，并且R 1是H或C 1 -C 20烷基; （b）约10％至约25％的式2的单体或其混合物：<？in-line-formula description =“In-line Formulas”end =“lead”？> CH2-C（R） COZ（CH2）q（CHR）rNR2R3式2 <？在线公式描述=“在线公式”end =“tail”？>其中R2和R3各自独立地为C1-C4烷基，羟乙基或苄基或 R2和R3与氮原子一起形成吗啉，吡咯烷或哌啶环，Z是-O-或-NR4-，其中R4是H或C1-C4烷基; （c）约1％至约15％的式3的单体或其混合物：<？in-line-formula description =“In-line formula”end =“lead”？> CH2-CR（R5 ）其中R5是CO（CH2）5，CO-O-（CH2）2，C6H4CHR或CONRR6，其中R5是CO- ，R6为C6H4OCH2，（CH2）d或C（CH3）2CH2。

4. 发明授权

US5608116A Process for the alkoxylation of fluorinated alcohols 失效
标题翻译：氟化醇的烷氧基化方法
公开(公告)号：US5608116A
公开(公告)日：1997-03-04
申请号：US405327
申请日：1995-03-16
申请人： Robert A. Halling , Hsu-Nan Huang
发明人： Robert A. Halling , Hsu-Nan Huang
IPC分类号： B01J31/14 , B01F17/00 , B01J27/08 , C07B61/00 , C07C41/03 , C07C43/11 , C07C217/28 , C07C231/12 , C07C233/18 , C07C303/40 , C07C311/04 , C07C311/09 , C08G65/26 , C08G65/28 , C11D1/00
CPC分类号： B01F17/0035 , C07C217/28 , C07C303/40 , C07C41/03 , C08G65/2639 , C11D1/004
摘要： The present invention relates to the preparation of fluoroalkylalkoxylates in which one reacts at least one fluorinated alcohol with at least one alkylene epoxide in the presence of a novel catalyst system comprising an iodine source and an alkali metal borohydride.
摘要翻译：本发明涉及氟代烷基烷氧基化物的制备，其中在包含碘源和碱金属硼氢化物的新型催化剂体系的存在下，使至少一种氟化醇与至少一种亚烷基环氧化物反应。

5. 发明授权

US4898991A New perfluoropolyethers 失效
标题翻译：新型全氟聚醚
公开(公告)号：US4898991A
公开(公告)日：1990-02-06
申请号：US303151
申请日：1989-01-30
申请人： Hsu-Nan Huang
发明人： Hsu-Nan Huang
IPC分类号： C07C43/12
CPC分类号： C07C43/126
摘要： New perfluoropolyethers, such as perfluoro-4,7,10-trioxa-5-methyleicosane, are useful as vapor phase soldering fluids and convection cooling liquids.
摘要翻译：新的全氟聚醚，例如全氟-4,7,10-三氧杂-5-甲基硅烷可用作气相焊接流体和对流冷却液。

6. 发明授权

US08071489B2 Amphoteric fluorochemicals for paper 有权
标题翻译：两性氟化合物用于纸张
公开(公告)号：US08071489B2
公开(公告)日：2011-12-06
申请号：US11827006
申请日：2007-07-10
申请人： Hsu-Nan Huang , Martial Jean-Jacques Pabon , Romain Severac , Lamia Heuze
发明人： Hsu-Nan Huang , Martial Jean-Jacques Pabon , Romain Severac , Lamia Heuze
IPC分类号： B32B27/04
CPC分类号： C09D133/18 , C08F220/06 , C08F220/24 , C08F220/34 , D21H17/11 , D21H17/36 , D21H17/37 , D21H21/14 , D21H21/16 , Y10T428/31895 , Y10T442/2279 , Y10T442/2287
摘要： A method of imparting oil repellency to flexible, fibrous, nonwoven substrates comprising contacting the substrate with an amphoteric fluorochemical copolymer composition prepared from polymerization of monomers in the following percentages by weight: (a) from about 60% to about 90% of a fluorinated (meth)acrylate monomer of Formula 1 which is Rf-Q-CO—CR═CH2, (b) from about 10% to about 25% of an amine substituted (meth)acrylate or (meth)acylamide monomer of Formula 2 which is CH2═C(R)COZ(CH2)q(CHR)rNR2R3, and (c) from about 1% to about 15% of a substituted (meth)acrylic acid monomer of Formula 3 which is CH2=CR(R5)e—COOH.
摘要翻译：将柔性纤维状非织造基材赋予斥油性的方法，包括使基材与由单体聚合制备的两性含氟共聚物组合物接触，所述两性含氟共聚物组合物的重量百分比如下：（a）约60％至约90％的氟化（甲基）丙烯酸酯单体，其为Rf-Q-CO-CR = CH 2，（b）约10％至约25％的胺取代的（甲基）丙烯酸酯或式（2）的（甲基）（C）COZ（CH2）q（CHR）rNR2R3和（c）约1％至约15％的CH 2 = CR（R 5）e -COOH的式3的取代的（甲基）丙烯酸单体。

7. 发明授权

US06353051B1 Top coating for synthetic leathers 失效
公开(公告)号：US06353051B1
公开(公告)日：2002-03-05
申请号：US09495132
申请日：2000-01-31
申请人： Hsu-Nan Huang
发明人： Hsu-Nan Huang
IPC分类号： C08L2712
CPC分类号： D06N3/144 , D06N3/042
摘要： The present invention comprises a composition for coating synthetic grain leather having both dynamic water repellency and oil repellency comprising a copolymer or blend of copolymers and a polyurethane resin in solvent.

8. 发明授权

US5259938A Process for omega-halo-perfluoro acid chlorides 失效
标题翻译： ω-卤代全氟酰氯的方法
公开(公告)号：US5259938A
公开(公告)日：1993-11-09
申请号：US944673
申请日：1992-09-15
申请人： Hsu-Nan Huang
发明人： Hsu-Nan Huang
IPC分类号： C07C51/58 , C07C51/00
CPC分类号： C07C51/58
摘要： A liquid phase process for preparing .omega.-haloperfluoroacid chlorides by the photo oxidation of polyfluoroalkyl mono- and di-chloromethanes in the presence of chlorine using light wavelengths greater than 280 nm.
摘要翻译：在使用大于280nm的光波长的氯存在下，通过多氟烷基单氯代甲烷和二氯甲烷的光氧化制备ω-氟全氟酰氯的液相方法。

9. 发明授权

US5084146A Method for preparing perfluoropolyethers 失效
标题翻译：制备全氟聚醚的方法
公开(公告)号：US5084146A
公开(公告)日：1992-01-28
申请号：US509416
申请日：1990-04-09
申请人： Hsu-Nan Huang
发明人： Hsu-Nan Huang
IPC分类号： C08G61/00 , C08G65/00 , C08G65/32 , C25B3/10
CPC分类号： C08G65/007 , C25B3/10
摘要： A method for preparing perfluoropolyether oligomers comprising electrochemical coupling of perfluorocarboxylic acid salts or mixtures thereof in aqueous methanol under controlled conditions to produce perfluoropolyether oligomers.
摘要翻译：一种制备全氟聚醚低聚物的方法，包括在受控条件下在含水甲醇中全氟羧酸盐或其混合物的电化学偶联以产生全氟聚醚低聚物。

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