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1. 发明授权

US08653183B2 Method of curing a coating composition comprising a radical curable compound and an organoborane-amine complex 有权
标题翻译：固化包含自由基固化性化合物和有机硼烷 - 胺络合物的涂料组合物的方法
公开(公告)号：US08653183B2
公开(公告)日：2014-02-18
申请号：US13380255
申请日：2010-06-22
申请人： Keith E. Gutowski , Walter H. Ohrbom , David Cranfill , Donald H. Campbell
发明人： Keith E. Gutowski , Walter H. Ohrbom , David Cranfill , Donald H. Campbell
IPC分类号： C09D7/12 , B05D7/24 , B05D3/10 , C09D4/02 , C09D133/08
CPC分类号： C09D133/08 , C08J3/24 , C08K5/55 , C09D4/00
摘要： A method of curing a coating composition and a method of forming a cured coating on an automobile component are provided. The coating composition comprises a radical polymerizable compound and an organoborane-amine complex having an organoborane initiator, an amine blocking agent, and water. The method of curing the coating composition comprises the steps of combining the organoborane-amine complex, the radical polymerizable compound, and water to form the coating composition. Carbon dioxide is introduced into the coating composition or into a composition including at least one of the organoborane-amine complex, the radical polymerizable compound, and water prior to forming the coating composition. Carbonic acid is formed in situ within the coating composition through reaction of the water and carbon dioxide. The organoborane-amine complex is decomplexed with the carbonic acid thereby separating the organoborane initiator and the amine blocking agent. The radical polymerizable compound is polymerized using the organoborane initiator in the presence of oxygen.
摘要翻译：提供固化涂料组合物的方法和在汽车部件上形成固化涂层的方法。涂料组合物包含可自由基聚合的化合物和具有有机硼烷引发剂，胺封闭剂和水的有机硼烷 - 胺络合物。固化涂料组合物的方法包括将有机硼烷 - 胺络合物，可自由基聚合的化合物和水组合以形成涂料组合物的步骤。在形成涂料组合物之前，将二氧化碳引入涂料组合物或包含至少一种有机硼烷 - 胺络合物，可自由基聚合的化合物和水的组合物。碳酸通过水和二氧化碳的反应在涂料组合物中原位形成。有机硼烷 - 胺络合物与碳酸分解，从而分离有机硼烷引发剂和胺封闭剂。使用有机硼烷引发剂在氧的存在下使自由基聚合性化合物聚合。

2. 发明申请

US20120116013A1 METHOD OF CURING A COATING COMPOSITION COMPRISING A RADICAL CURABLE COMPOUND AND AN ORGANOBORANE-AMINE COMPLEX 有权
标题翻译：固化包含耐光固化性化合物的涂料组合物和有机硼 - 胺复合物的方法
公开(公告)号：US20120116013A1
公开(公告)日：2012-05-10
申请号：US13380255
申请日：2010-06-22
申请人： Keith E. Gutowski , Walter H. Ohrbom , David Cranfill , Donald H. Campbell
发明人： Keith E. Gutowski , Walter H. Ohrbom , David Cranfill , Donald H. Campbell
IPC分类号： C09D7/12 , B05D7/24 , B05D3/10 , C09D4/02 , C09D133/08
CPC分类号： C09D133/08 , C08J3/24 , C08K5/55 , C09D4/00
摘要： A method of curing a coating composition and a method of forming a cured coating on an automobile component are provided. The coating composition comprises a radical polymerizable compound and an organoborane-amine complex having an organoborane initiator, an amine blocking agent, and water. The method of curing the coating composition comprises the steps of combining the organoborane-amine complex, the radical polymerizable compound, and water to form the coating composition. Carbon dioxide is introduced into the coating composition or into a composition including at least one of the organoborane-amine complex, the radical polymerizable compound, and water prior to forming the coating composition. Carbonic acid is formed in situ within the coating composition through reaction of the water and carbon dioxide. The organoborane-amine complex is de-complexed with the carbonic acid thereby separating the organoborane initiator and the amine blocking agent. The radical polymerizable compound is polymerized using the organoborane initiator in the presence of oxygen.
摘要翻译：提供固化涂料组合物的方法和在汽车部件上形成固化涂层的方法。涂料组合物包含可自由基聚合的化合物和具有有机硼烷引发剂，胺封闭剂和水的有机硼烷 - 胺络合物。固化涂料组合物的方法包括将有机硼烷 - 胺络合物，可自由基聚合的化合物和水组合以形成涂料组合物的步骤。在形成涂料组合物之前，将二氧化碳引入涂料组合物或包含至少一种有机硼烷 - 胺络合物，可自由基聚合的化合物和水的组合物。碳酸通过水和二氧化碳的反应在涂料组合物中原位形成。有机硼烷 - 胺络合物与碳酸脱配合，从而分离有机硼烷引发剂和胺封闭剂。使用有机硼烷引发剂在氧气存在下使自由基聚合性化合物聚合。

3. 发明申请

US20120100378A1 PAINT COATING SYSTEM AND METHOD OF PRODUCING MULTILAYERED PAINT COATING 审中-公开
标题翻译：涂料涂料体系和多层涂料涂料的制造方法
公开(公告)号：US20120100378A1
公开(公告)日：2012-04-26
申请号：US13380304
申请日：2010-06-24
申请人： Walter H. Ohrbom , Gregory G. Menovcik , Patrick J. Mormile , Donald H. Campbell , David Cranfill
发明人： Walter H. Ohrbom , Gregory G. Menovcik , Patrick J. Mormile , Donald H. Campbell , David Cranfill
IPC分类号： B32B27/36 , B05D3/02 , B32B27/38
CPC分类号： B05D1/36 , B05D7/52 , C09D4/00 , Y10T428/31507 , Y10T428/31515 , Y10T428/31536
摘要： A paint coating system comprises a substrate and a first paint layer disposed on the substrate. The first paint layer is formed from a first composition comprising either a first decomplexing agent or a first organoborane complex. The paint coating system further comprises a second paint layer disposed on the first paint layer. The second paint layer is formed from a second composition comprising the other of the first decomplexing agent and the first organoborane complex. At least one of the first and second compositions further comprises a radical polymerizable compound. A method of producing a multilayered paint coating includes the steps of providing the substrate, applying a first paint layer on the substrate, applying a second paint layer on the first paint layer, and curing the at least one of the first and second paint layers.
摘要翻译：涂料系统包括基材和设置在基材上的第一涂料层。第一涂料层由包含第一解络剂或第一有机硼烷络合物的第一组合物形成。涂料系统还包括设置在第一涂料层上的第二涂料层。第二涂层由第二组合物形成，第二组合物包含第一解络剂和第一有机硼烷络合物中的另一种。第一和第二组合物中的至少一种还包含自由基聚合性化合物。制造多层涂料涂料的方法包括以下步骤：提供基材，在基材上施加第一涂料层，在第一涂料层上施加第二涂料层，并固化第一和第二涂料层中的至少一个。

4. 发明授权

US06531560B1 Carbamate-functional resins having improved adhesion, method of making the same, and method of improving intercoat adhesion 有权
公开(公告)号：US06531560B1
公开(公告)日：2003-03-11
申请号：US09677063
申请日：2000-09-29
申请人： Donald H. Campbell , Walter H. Ohrbom , Joseph Borst , Michael A. Gessner , Donald L. St. Aubin , Marvin L. Green , Bruce E. Oermann
发明人： Donald H. Campbell , Walter H. Ohrbom , Joseph Borst , Michael A. Gessner , Donald L. St. Aubin , Marvin L. Green , Bruce E. Oermann
IPC分类号： C08F12602
CPC分类号： C08G18/8116 , C08F8/00 , C08F2800/20 , C08F2810/50 , C08G18/3823 , C09D201/025 , Y10T428/31551 , Y10T428/31573 , Y10T428/31645 , C08F2220/325 , C08F220/34 , C08F220/20 , C08F212/08
摘要： The invention provides carbamate-functional resins and coating compositions incorporating said resins that have improved adhesion with respect to subsequently applied films or coatings. More particularly, the invention relates to carbamate-functional addition polymers having at least 250 grams of polymer per carbamate group which are made with less than 35 percent by weight of nonfunctional monomers, preferably with less than 20 percent by weight and most preferably from 0 to less than 10 percent by weight, based on the total weight of the polymer. The invention further provides a method of making a carbamate-functional polymer and carbamate-functional polymers made by the claimed method. Finally, the invention provides a method for improving the adhesion of a first coating composition to a subsequently applied material as well as a method of making a composite comprising a coated substrate, an adhesive composition, and a glass having at least one surface.

5. 发明申请

US20100183882A1 Coating System For Achieving Excellent MVSS Adhesion 有权
标题翻译：涂层体系可实现优异的MVSS粘合力
公开(公告)号：US20100183882A1
公开(公告)日：2010-07-22
申请号：US12516836
申请日：2008-02-13
申请人： Donald H. Campbell , Gregory G. Menovcik , David J. Santure , Walter H. Ohrbom , Donald St. Aubin , Paul J. Harris
发明人： Donald H. Campbell , Gregory G. Menovcik , David J. Santure , Walter H. Ohrbom , Donald St. Aubin , Paul J. Harris
IPC分类号： B32B27/08 , B32B27/40 , B05D1/36
CPC分类号： B05D7/576 , B05D2202/15 , C09D201/025 , Y10T428/31551 , C08L2666/16
摘要： A coating system includes a clear coat layer and a sealant. The clear coat layer is formed from a clear coat composition that comprises a crosslinkable carbamate-functional resin and an aminoplast. Optionally, the coating system further includes a sub-clear coat layer that is formed from a sub-clear coat composition. The sealant is bonded to the clear coat layer opposite the sub-clear coat layer. Optionally, the coating system further includes a tie coat layer that is formed from a tie coat composition and that is disposed between the sealant and the clear coat layer. An adhesion promoter is present in the clear coat composition in an amount of less than or equal to about 3% by weight based on the total weight of resin solids of the clear coat composition. Further, the adhesion promoter is present in at least one of the sub-clear coat composition and the tie coat composition in an amount sufficient to increase adhesion between the clear coat layer and the sealant.
摘要翻译：涂层系统包括透明涂层和密封剂。透明涂层由透明涂层组合物形成，该组合物包含可交联的氨基甲酸酯官能树脂和氨基塑料。任选地，涂层系统还包括由亚透明涂层组合物形成的副透明涂层。密封剂粘合到与透明涂层相对的透明涂层上。任选地，涂层系统还包括由粘结涂层组合物形成并且设置在密封剂和透明涂层之间的粘结涂层。基于透明涂料组合物的树脂固体的总重量，粘合促进剂以小于或等于约3重量％的量存在于透明涂料组合物中。此外，粘合促进剂以足以增加透明涂层和密封剂之间的粘合力的量存在于至少一种亚透明涂料组合物和粘合涂层组合物中。

6. 发明授权

US5853809A Scratch resistant clearcoats containing suface reactive microparticles and method therefore 失效
标题翻译：因此，含有表面反应性微粒的耐刮擦清漆和方法
公开(公告)号：US5853809A
公开(公告)日：1998-12-29
申请号：US723436
申请日：1996-09-30
申请人： Donald H. Campbell , Janice E. Echols , Walter H. Ohrbom
发明人： Donald H. Campbell , Janice E. Echols , Walter H. Ohrbom
IPC分类号： C09D7/12 , B05D1/36
CPC分类号： C09D7/1266 , C09D7/1216 , C09D7/1275 , C08K3/36 , C08K9/04
摘要： The present invention is a coating composition having good scratch resistance and a method for improving the scratch resistance of a coating composition. The coating composition comprises (A) a film forming binder system containing a crosslinkable resin and optionally a crosslinking agent for the crosslinkable resin; (B) substantially colorless carbide or inorganic microparticles, range in size from about 1 to 1000 nanometers prior to incorporation in the coating composition, and the microparticles are reactive with the crosslinkable portion of the film forming binder system; (C) a solvent system for the crosslinkable resin, optional crosslinking agent, and microparticles, wherein the crosslinkable resin is present in an amount from about 10 to about 80% by weight and the inorganic microparticles are present in an amount from 0.1 to 60.0% by weight based on the sum of the weights of the crosslinkable resin, the optional crosslinking agent, and the inorganic microparticles.
摘要翻译：本发明是具有良好的耐刮擦性的涂料组合物和改善涂料组合物耐擦伤性的方法。涂料组合物包含（A）含有可交联树脂和任选的可交联树脂交联剂的成膜粘合剂体系; （B）基本上无色的碳化物或无机微粒，在引入涂料组合物之前的尺寸范围为约1至1000纳米，并且微粒与成膜粘合剂体系的可交联部分反应; （C）可交联树脂的溶剂体系，任选的交联剂和微粒，其中可交联树脂的存在量为约10至约80重量％，无机微粒以0.1至60.0重量％的量存在，，基于可交联树脂，任选的交联剂和无机微粒的重量之和。

7. 发明授权

US07232863B2 Functional addition polymers and a method for their preparation 有权
标题翻译：官能加成聚合物及其制备方法
公开(公告)号：US07232863B2
公开(公告)日：2007-06-19
申请号：US10957568
申请日：2004-10-01
申请人： Walter H. Ohrbom , Donald H. Campbell , Donald L. St. Aubin , Swaminathan Ramesh , Paul J. Harris , Ulrike Röckrath
发明人： Walter H. Ohrbom , Donald H. Campbell , Donald L. St. Aubin , Swaminathan Ramesh , Paul J. Harris , Ulrike Röckrath
IPC分类号： C08F8/14
CPC分类号： C08F222/20 , C08F8/14 , C08F220/06 , C08F220/08 , C08F222/22 , C08G18/00 , C09D201/025 , Y10T428/31511 , C08F265/06
摘要： Disclosed is a method for making nongelled functional addition polymers from linear unsaturated anhydrides. The method subjects a linear unsaturated anhydride compound, an active hydrogen compound, and an epoxide compound to reaction conditions such that each of the following three reactions occur: (i) polymerization of polymerizable C═C bonds, (ii) ring opening of an anhydride functional group of the linear unsaturated anhydride compound by the active hydrogen compound to create an acid functional group, and (iii) reaction of the acid functional group resulting from the anhydride ring opening with the epoxide compound. At the time of reaction (iii), the acid functional group resulting from the anhydride ring opening may be selected from an ethylenically unsaturated monomer, a polymer, or both. In one embodiment, the method does not include the physical removal of any acid functional monomers or polymerization products. Also disclosed are a curable coating composition and a coated substrate.
摘要翻译：公开了一种从线性不饱和酸酐制造非功能性加成聚合物的方法。该方法使线性不饱和酸酐化合物，活性氢化合物和环氧化合物反应，使得发生以下三个反应中的每一个：（i）可聚合的CC键的聚合，（ii）酸酐官能团的开环的线性不饱和酸酐化合物，以产生酸官能团，和（iii）由酸酐开环产生的酸官能团与环氧化合物的反应。在反应（iii）时，由酸酐开环产生的酸官能团可以选自烯属不饱和单体，聚合物或两者。在一个实施方案中，该方法不包括物理去除任何酸官能单体或聚合产物。还公开了可固化涂料组合物和涂布的基材。

8. 发明授权

US06696535B2 Carbamate-functional resins having improved adhesion, method of making the same, and method of improving intercoat adhesion 有权
标题翻译：具有改进粘合性的氨基甲酸酯官能树脂，其制备方法以及改进层间粘附性的方法
公开(公告)号：US06696535B2
公开(公告)日：2004-02-24
申请号：US10348492
申请日：2003-01-21
申请人： Donald H. Campbell , Walter H. Ohrbom , Joseph Borst , Michael A. Gessner , Donald L. St. Aubin , Marvin L. Green , Bruce E. Oermann
发明人： Donald H. Campbell , Walter H. Ohrbom , Joseph Borst , Michael A. Gessner , Donald L. St. Aubin , Marvin L. Green , Bruce E. Oermann
IPC分类号： C08F12602
CPC分类号： C08G18/8116 , C08F8/00 , C08F2800/20 , C08F2810/50 , C08G18/3823 , C09D201/025 , Y10T428/31551 , Y10T428/31573 , Y10T428/31645 , C08F2220/325 , C08F220/34 , C08F220/20 , C08F212/08
摘要： The invention provides carbamate-functional resins and coating compositions incorporating said resins that have improved adhesion with respect to subsequently applied films or coatings. More particularly, the invention relates to carbamate-functional addition polymers having at least 250 grams of polymer per carbamate group which are made with less than 35 percent by weight of nonfunctional monomers, preferably with less than 20 percent by weight and most preferably from 0 to less than 10 percent by weight, based on the total weight of the polymer. The invention further provides a method of making a carbamate-functional polymer and carbamate-functional polymers made by the claimed method. Finally, the invention provides a method for improving the adhesion of a first coating composition to a subsequently applied material as well as a method of making a composite comprising a coated substrate, an adhesive composition, and a glass having at least one surface.
摘要翻译：本发明提供氨基甲酸酯官能树脂和包含所述树脂的涂料组合物，其相对于随后施加的膜或涂层具有改善的粘合性。更具体地说，本发明涉及具有每个氨基甲酸酯基团至少250克聚合物的氨基甲酸酯官能加成聚合物，它们以小于35重量％的非官能单体，优选小于20重量％，最优选0至小于10重量％，基于聚合物的总重量。本发明还提供一种制备通过所要求保护的方法制备的氨基甲酸酯官能聚合物和氨基甲酸酯官能聚合物的方法。最后，本发明提供了一种用于改善第一涂料组合物与随后施加的材料的粘附性的方法，以及制备包含涂覆的基材，粘合剂组合物和具有至少一个表面的玻璃的复合材料的方法。

9. 发明授权

US06462144B1 Carbamate-functional resins and their use in high solids coating compositions 有权
标题翻译：氨基甲酸酯官能树脂及其在高固含量涂料组合物中的应用
公开(公告)号：US06462144B1
公开(公告)日：2002-10-08
申请号：US09793289
申请日：2001-02-26
申请人： Swaminathan Ramesh , Marvin L. Green , Donald H. Campbell , Walter H. Ohrbom
发明人： Swaminathan Ramesh , Marvin L. Green , Donald H. Campbell , Walter H. Ohrbom
IPC分类号： C08G1832
CPC分类号： C09D201/025 , C09D201/005 , Y10T428/31511 , Y10T428/31551
摘要： The present invention provides a coating composition containing 1) a carbamate-functional resin having in its structure a hyperbranched or star polyol core, a first chain extension based on a polycarboxylic acid or anbydride, a second chain extension based on an epoxy containing compound, and having carbamate functional groups on the core, the second chain extension, or both; and 2) a second resin containing functional groups reactive with the carbamate groups on the carbamate-functional resin. In one embodiment, the coating compositions are used as a cloarcoat to be applied over a basecoat to form a composite coating. The compositions exhibit a combination of desirable properties, such as scratch and mar resistance, resistance to environmental etch, good intercoat adhesion, and high solids.
摘要翻译：本发明提供了一种涂料组合物，其含有1）氨基甲酸酯官能树脂，其结构是其超结构或星型多元醇芯，基于多元羧酸或二硼化物的第一链延伸，基于含环氧化合物的第二链延伸，以及在芯上具有氨基甲酸酯官能团，第二链延伸部分或两者; 和2）含有与氨基甲酸酯官能树脂上的氨基甲酸酯基反应的官能团的第二树脂。在一个实施方案中，涂料组合物用作蜡涂层以涂覆在底涂层上以形成复合涂层。组合物显示出所需性能的组合，例如耐刮擦和耐擦伤性，耐环境腐蚀性，良好的涂层间粘合性和高固含量。

10. 发明授权

US5777048A Method for modified aminoplast compounds, aminoplasts obtained thereby and coatings containing the same 失效
标题翻译：修饰氨基塑料化合物的方法，由此获得的氨基塑料和含有它们的涂层
公开(公告)号：US5777048A
公开(公告)日：1998-07-07
申请号：US667261
申请日：1996-06-20
申请人： Walter H. Ohrbom , Donald H. Campbell , Donald L. St. Aubin
发明人： Walter H. Ohrbom , Donald H. Campbell , Donald L. St. Aubin
IPC分类号： C08G12/40 , C08G18/80 , C09D161/20 , C09D201/00 , C09D201/02 , C08F8/30
CPC分类号： C09D201/025 , C08G12/40 , C08G18/8077 , C09D161/20 , C09D201/02
摘要： A method for reducing the molecular weight of aminoplast compounds, the aminoplast compounds obtained thereby, and coating compositions containing said aminoplast compounds are provided. The reduced molecular weight aminoplasts are obtained by reacting (a) an aminoplast compound, having a total number (y) of reactive substituents on the amino nitrogens of the aminoplast, where y=(E.times.M) and E=equivalents per mole of aminoplast and M=total number of moles of aminoplast, wherein the reactive substituents are selected from the group consisting of --NH, alkylol, alkoxy, alkoxyalkyl, and mixtures thereof and(b) at least one carbamate compound selected from the group consisting of unsubstituted and substituted primary carbamate compounds, unsubstituted and substituted secondary carbamate compounds and mixtures thereof, in the presence of primary or secondary alcohols, at temperatures under 150.degree. C., and at pressures ranging between atmospheric pressure and 20 atm pressure, to form a functionalized aminoplast compound, wherein at least one and up to (y-1) of the amino substituents on the aminoplast are substituted with the carbamate functionality.
摘要翻译：提供了降低氨基塑料化合物的分子量，由此获得的氨基塑料化合物和含有所述氨基塑料化合物的涂料组合物的方法。通过使（a）在氨基塑料的氨基氮上具有总数（y）的反应性取代基的氨基塑料化合物，其中y =（ExM）和E =每摩尔氨基塑料的当量和M =氨基塑料的总摩尔数，其中反应性取代基选自-NH，羟烷基，烷氧基，烷氧基烷基及其混合物，和（b）至少一种选自未取代和取代的伯氨基甲酸酯化合物，未取代和取代的仲氨基甲酸酯化合物及其混合物，在初级醇或仲醇的存在下，在150℃的温度和在大气压和20atm压力之间的压力下形成官能化的氨基塑料化合物，其中氨基塑料上氨基取代基的至少一个和至多（y-1）被氨基甲酸酯官能团取代。

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