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1. 发明授权

US07342075B2 Carbamate functional addition polymers and method for their preparation 失效
标题翻译：氨基甲酸酯官能加成聚合物及其制备方法
公开(公告)号：US07342075B2
公开(公告)日：2008-03-11
申请号：US10957556
申请日：2004-10-01
申请人： Swaminathan Ramesh , Paul J. Harris , Walter H. Ohrbom , Donald H. Campbell , Donald L. St. Aubin , Ulrike Röckrath
发明人： Swaminathan Ramesh , Paul J. Harris , Walter H. Ohrbom , Donald H. Campbell , Donald L. St. Aubin , Ulrike Röckrath
IPC分类号： C08F8/28
CPC分类号： C08F220/06 , C08F8/00 , C08F8/14 , C08F220/08 , C08F222/20 , C08F222/22 , C08L2312/00 , C09D133/14 , C09D201/025 , C08F265/06
摘要： Disclosed is a method for making nongelled addition polymers, especially carbamate functional additional polymers from linear unsaturated anhydrides. The method comprises reacting an unsaturated linear anhydride with an active hydrogen compound to provide two monomers comprising polymerizable C═C bonds, at least one of said monomers comprising an acid functional group; polymerizing the polymerizable C═C bonds of the two monomers to provide an acid functional polymerization product; and reacting the acid functional polymerization product with an epoxy functional compound to provide a nongelled addition polymer, wherein the disclosed method does not include a step comprising the physical removal of any acid functional monomers or polymerization products. Also disclosed is a curable coating composition containing the resulting carbamate functional polymer, as well as a coated substrate comprising a cured film resulting from the application and curing of the disclosed curable coating composition.
摘要翻译：公开了一种用于制备非线性加成聚合物，特别是来自线性不饱和酸酐的氨基甲酸酯官能的另外的聚合物的方法。该方法包括使不饱和直链酸酐与活性氢化合物反应以提供包含可聚合C-C键的两种单体，至少一种所述单体包含酸官能团; 聚合两种单体的可聚合C-C键以提供酸官能聚合产物; 并使酸官能聚合产物与环氧官能化合物反应以提供不通电的加成聚合物，其中所公开的方法不包括物理除去任何酸官能单体或聚合产物的步骤。还公开了含有所得氨基甲酸酯官能聚合物的可固化涂料组合物，以及包含由所公开的可固化涂料组合物的施用和固化产生的固化膜的涂布基材。

2. 发明授权

US07232863B2 Functional addition polymers and a method for their preparation 有权
标题翻译：官能加成聚合物及其制备方法
公开(公告)号：US07232863B2
公开(公告)日：2007-06-19
申请号：US10957568
申请日：2004-10-01
申请人： Walter H. Ohrbom , Donald H. Campbell , Donald L. St. Aubin , Swaminathan Ramesh , Paul J. Harris , Ulrike Röckrath
发明人： Walter H. Ohrbom , Donald H. Campbell , Donald L. St. Aubin , Swaminathan Ramesh , Paul J. Harris , Ulrike Röckrath
IPC分类号： C08F8/14
CPC分类号： C08F222/20 , C08F8/14 , C08F220/06 , C08F220/08 , C08F222/22 , C08G18/00 , C09D201/025 , Y10T428/31511 , C08F265/06
摘要： Disclosed is a method for making nongelled functional addition polymers from linear unsaturated anhydrides. The method subjects a linear unsaturated anhydride compound, an active hydrogen compound, and an epoxide compound to reaction conditions such that each of the following three reactions occur: (i) polymerization of polymerizable C═C bonds, (ii) ring opening of an anhydride functional group of the linear unsaturated anhydride compound by the active hydrogen compound to create an acid functional group, and (iii) reaction of the acid functional group resulting from the anhydride ring opening with the epoxide compound. At the time of reaction (iii), the acid functional group resulting from the anhydride ring opening may be selected from an ethylenically unsaturated monomer, a polymer, or both. In one embodiment, the method does not include the physical removal of any acid functional monomers or polymerization products. Also disclosed are a curable coating composition and a coated substrate.
摘要翻译：公开了一种从线性不饱和酸酐制造非功能性加成聚合物的方法。该方法使线性不饱和酸酐化合物，活性氢化合物和环氧化合物反应，使得发生以下三个反应中的每一个：（i）可聚合的CC键的聚合，（ii）酸酐官能团的开环的线性不饱和酸酐化合物，以产生酸官能团，和（iii）由酸酐开环产生的酸官能团与环氧化合物的反应。在反应（iii）时，由酸酐开环产生的酸官能团可以选自烯属不饱和单体，聚合物或两者。在一个实施方案中，该方法不包括物理去除任何酸官能单体或聚合产物。还公开了可固化涂料组合物和涂布的基材。

3. 发明申请

US20100183882A1 Coating System For Achieving Excellent MVSS Adhesion 有权
标题翻译：涂层体系可实现优异的MVSS粘合力
公开(公告)号：US20100183882A1
公开(公告)日：2010-07-22
申请号：US12516836
申请日：2008-02-13
申请人： Donald H. Campbell , Gregory G. Menovcik , David J. Santure , Walter H. Ohrbom , Donald St. Aubin , Paul J. Harris
发明人： Donald H. Campbell , Gregory G. Menovcik , David J. Santure , Walter H. Ohrbom , Donald St. Aubin , Paul J. Harris
IPC分类号： B32B27/08 , B32B27/40 , B05D1/36
CPC分类号： B05D7/576 , B05D2202/15 , C09D201/025 , Y10T428/31551 , C08L2666/16
摘要： A coating system includes a clear coat layer and a sealant. The clear coat layer is formed from a clear coat composition that comprises a crosslinkable carbamate-functional resin and an aminoplast. Optionally, the coating system further includes a sub-clear coat layer that is formed from a sub-clear coat composition. The sealant is bonded to the clear coat layer opposite the sub-clear coat layer. Optionally, the coating system further includes a tie coat layer that is formed from a tie coat composition and that is disposed between the sealant and the clear coat layer. An adhesion promoter is present in the clear coat composition in an amount of less than or equal to about 3% by weight based on the total weight of resin solids of the clear coat composition. Further, the adhesion promoter is present in at least one of the sub-clear coat composition and the tie coat composition in an amount sufficient to increase adhesion between the clear coat layer and the sealant.
摘要翻译：涂层系统包括透明涂层和密封剂。透明涂层由透明涂层组合物形成，该组合物包含可交联的氨基甲酸酯官能树脂和氨基塑料。任选地，涂层系统还包括由亚透明涂层组合物形成的副透明涂层。密封剂粘合到与透明涂层相对的透明涂层上。任选地，涂层系统还包括由粘结涂层组合物形成并且设置在密封剂和透明涂层之间的粘结涂层。基于透明涂料组合物的树脂固体的总重量，粘合促进剂以小于或等于约3重量％的量存在于透明涂料组合物中。此外，粘合促进剂以足以增加透明涂层和密封剂之间的粘合力的量存在于至少一种亚透明涂料组合物和粘合涂层组合物中。

4. 发明授权

US08906507B2 Coating system for achieving excellent MVSS adhesion 有权
标题翻译：涂层系统可实现优异的MVSS粘附力
公开(公告)号：US08906507B2
公开(公告)日：2014-12-09
申请号：US12516836
申请日：2008-02-13
申请人： Donald H. Campbell , Gregory G. Menovcik , David J. Santure , Walter H. Ohrbom , Donald St. Aubin , Paul J. Harris
发明人： Donald H. Campbell , Gregory G. Menovcik , David J. Santure , Walter H. Ohrbom , Donald St. Aubin , Paul J. Harris
IPC分类号： B32B27/08 , B32B27/40 , C08G18/00 , B05D7/00 , C09D201/02
CPC分类号： B05D7/576 , B05D2202/15 , C09D201/025 , Y10T428/31551 , C08L2666/16
摘要： A coating system includes a clear coat layer and a sealant. The clear coat layer is formed from a clear coat composition that comprises a crosslinkable carbamate-functional resin and an aminoplast. Optionally, the coating system further includes a sub-clear coat layer. The sealant is bonded to the clear coat layer opposite the sub-clear coat layer. Optionally, the coating system further includes a tie coat layer and that is disposed between the sealant and the clear coat layer. An adhesion promoter is present in the clear coat composition in an amount of less than or equal to about 3% by weight based on the total weight of resin solids of the clear coat composition. Further, the adhesion promoter is present in at least one of the sub-clear coat composition and the tie coat composition in an amount sufficient to increase adhesion between the clear coat layer and the sealant.
摘要翻译：涂层系统包括透明涂层和密封剂。透明涂层由透明涂层组合物形成，该组合物包含可交联的氨基甲酸酯官能树脂和氨基塑料。任选地，涂层系统还包括副透明涂层。密封剂粘合到与透明涂层相对的透明涂层。任选地，涂层系统还包括粘结涂层，并且设置在密封剂和透明涂层之间。基于透明涂料组合物的树脂固体的总重量，粘合促进剂以小于或等于约3重量％的量存在于透明涂料组合物中。此外，粘合促进剂以足以增加透明涂层和密封剂之间的粘合力的量存在于至少一种亚透明涂料组合物和粘合涂层组合物中。

5. 发明授权

US6162546A Unsaturated copolymer reacted with substituted p-hydroxybenzoic acid and crosslinker 失效
标题翻译：不饱和共聚物与取代的对羟基苯甲酸和交联剂反应
公开(公告)号：US6162546A
公开(公告)日：2000-12-19
申请号：US904279
申请日：1997-07-31
申请人： Paul J. Harris , John W. Rehfuss , Gregory G. Menovcik , Robert J. Taylor, Jr. , Donald L. St. Aubin
发明人： Paul J. Harris , John W. Rehfuss , Gregory G. Menovcik , Robert J. Taylor, Jr. , Donald L. St. Aubin
IPC分类号： C08F8/00 , C08F8/30 , B32B15/08 , B32B27/08 , B32B27/30 , C08L33/14
CPC分类号： C08F8/00 , C08F2800/20 , C08F2810/20 , Y10T428/31511 , Y10T428/31515 , Y10T428/31522 , Y10T428/31529 , Y10T428/31576 , Y10T428/31692 , Y10T428/31699 , Y10T428/31862 , Y10T428/31928 , Y10T428/31935 , C08F8/10 , C08F2220/325
摘要： The present invention relates to a modified crosslinkable resin and a composite coating composition or system employing the resin. More particularly, the resin comprises an ethylenically unsaturated monomer or copolymer and para-hydroxybenzoic acid or substituted para-hydroxybenzoic acid, the reaction product thereof subsequently being reacted with a crosslinking agent gives rise to a composition including an ether linkage with a carbon-carbon site ortho to the phenolic hydroxy group.
摘要翻译：本发明涉及改性交联性树脂和使用该树脂的复合涂料组合物或体系。更具体地说，树脂包含烯属不饱和单体或共聚物和对羟基苯甲酸或取代的对羟基苯甲酸，其随后与交联剂反应产生包含与碳 - 碳位点的醚键的组合物邻苯酚羟基。

6. 发明授权

US07030263B2 Method of preparing a carbamate- or urea-functional compound 有权
公开(公告)号：US07030263B2
公开(公告)日：2006-04-18
申请号：US10280619
申请日：2002-10-25
申请人： Brian D. Bammel , John D. McGee , Walter H. Ohrbom , Todd A. Seaver , Gregory G. Menovcik , Paul J. Harris , John W. Rehfuss
发明人： Brian D. Bammel , John D. McGee , Walter H. Ohrbom , Todd A. Seaver , Gregory G. Menovcik , Paul J. Harris , John W. Rehfuss
IPC分类号： C08G63/64
CPC分类号： C09D175/02 , C07C269/04 , C07C269/06 , C07C273/1809 , C07C273/1854 , C08G18/4615 , C09D175/06 , Y10T428/31551 , C08L2666/16
摘要： A method of preparing a carbamate or urea-functional compound is described comprising the step of reacting a lactone or hydroxy carboxylic acid with a compound (A) comprising a carbamate or urea group or a group that can be converted to a carbamate or urea group, and an active hydrogen group capable of reacting with the hydroxy carboxylic acid or in a ring-opening reaction with a lactone. The compound thus prepared is useful in curable compositions.

7. 发明授权

US06391969B1 Powder slurry compositions with solid particulate carbamate resin component dispersed in liquid aminoplast resin carrier 失效
标题翻译：具有固体颗粒状氨基甲酸酯树脂组分的粉末浆料组合物分散在液体氨基塑料树脂载体中
公开(公告)号：US06391969B1
公开(公告)日：2002-05-21
申请号：US09633513
申请日：2000-08-07
申请人： Paul J. Harris , Walter H. Ohrbom , John W. Rehfuss
发明人： Paul J. Harris , Walter H. Ohrbom , John W. Rehfuss
IPC分类号： C08K507
CPC分类号： C09D201/06 , C08L2666/14
摘要： The invention provides a powder slurry composition comprising a first solid particulate component (a) dispersed in a crosslinking component (b) having at least one crosslinking resin which is liquid at 20° C. First component (a) is in solid particulate form having an average particle size of from 3 to 30 microns. Component (a) has a compound (i) having a Tg>40° C. and at least one carbamate or urea functional group, or a group convertible to a carbamate or urea group appended thereto. Crosslinking component (b) has at least one crosslinking resin (i) which is liquid at 20° C. Most preferably, crosslinking component (b) will further include a self-crosslinking aminoplast resin (ii) having at least two aminoplast groups and at least two groups which are nonreactive with solid particulate first component (a) but which are reactive with said aminoplast groups. The powder slurry composition of the invention has a VOC of less than 1.0 lbs./gal and provides performance and application improvements over the prior art.
摘要翻译：本发明提供一种粉末浆料组合物，其包含分散在具有至少一种在20℃下为液体的交联树脂的交联组分（b）中的第一固体颗粒组分（a）。第一组分（a）为固体颗粒形式，其具有平均粒径为3至30微米。组分（a）具有Tg> 40℃的化合物（i）和至少一个氨基甲酸酯或脲官能团，或可转化成氨基甲酸酯或脲基团的基团。交联组分（b）具有至少一种在20℃下为液体的交联树脂（i）。最优选地，交联组分（b）还包括具有至少两个氨基塑料基团的自交联氨基塑料树脂（ⅱ）至少两个与固体颗粒第一组分（a）反应但与所述氨基塑料基团反应的基团。本发明的粉末浆料组合物具有小于1.0lbs./gal的VOC，并且相对于现有技术提供了性能和应用改进。

8. 发明授权

US5760127A Curable coating composition 失效
标题翻译：可固化涂料组合物
公开(公告)号：US5760127A
公开(公告)日：1998-06-02
申请号：US698526
申请日：1996-08-15
申请人： Brian D. Bammel , John D. McGee , Walter H. Ohrbom , Todd A. Seaver , Gregory G. Menovcik , Paul J. Harris , John W. Rehfuss
发明人： Brian D. Bammel , John D. McGee , Walter H. Ohrbom , Todd A. Seaver , Gregory G. Menovcik , Paul J. Harris , John W. Rehfuss
IPC分类号： C08G71/00 , C09D167/04 , C09D201/02 , C08J3/00 , B32B27/00 , C08K3/20 , C08L75/00
CPC分类号： C09D201/02 , C08G71/00 , C09D167/04 , C09D201/025 , Y10T428/31551
摘要： A curable coating composition is described comprising (A) a carbamate- or urea-functional compound that is the reaction product of a mixture comprising (1) a compound comprising a carbamate or urea group or a group that can be converted to carbamate or urea, and a hydroxyl functional group that is the reaction product of (a) a compound comprising a carbamate or urea group or a group that can be converted to a carbamate or urea group, and an active hydrogen group that is reactive with a lactone ring or a hydroxy carboxylic acid, and (b) a lactone or a hydroxy carboxylic acid, and (2) a compound that is reactive with hydroxyl groups on a plurality of molecules of compound (A)(1), but that is not reactive with the carbamate or urea groups on compound (A)(1), (B) a compound comprising a plurality of groups that are reactive with carbamate or urea.
摘要翻译：描述了可固化涂料组合物，其包含（A）氨基甲酸酯或脲官能化合物，其为包含（1）包含氨基甲酸酯或脲基团的化合物或可转化为氨基甲酸酯或脲的基团的混合物的反应产物，和作为（a）包含氨基甲酸酯或脲基的化合物或可以转化为氨基甲酸酯或脲基的基团的反应产物的羟基官能团以及与内酯环或羟基羧酸和（b）内酯或羟基羧酸，和（2）与多个化合物（A）（1）分子上的羟基反应但不与氨基甲酸酯反应的化合物或化合物（A）（1）上的脲基，（B）包含与氨基甲酸酯或脲反应的多个基团的化合物。

9. 发明授权

US06498266B1 Method of preparing a carbamate- or urea-functional compound 失效
标题翻译：制备氨基甲酸酯或脲官能化合物的方法
公开(公告)号：US06498266B1
公开(公告)日：2002-12-24
申请号：US08698525
申请日：1996-08-15
申请人： Brian D. Bammel , John D. McGee , Walter H. Ohrbom , Todd A. Seaver , Gregory G. Menovcik , Paul J. Harris , John W. Rehfuss
发明人： Brian D. Bammel , John D. McGee , Walter H. Ohrbom , Todd A. Seaver , Gregory G. Menovcik , Paul J. Harris , John W. Rehfuss
IPC分类号： C08G6364
CPC分类号： C09D167/04 , C08G71/00 , C09D201/02
摘要： A method of preparing a carbamate or urea-functional compound is described comprising the step of reacting a lactone or hydroxy carboxylic acid with a compound (A) comprising a carbamate or urea group or a group that can be converted to a carbamate or urea group, and an active hydrogen group capable of reacting with the hydroxy carboxylic acid or in a ring-opening reaction with a lactone. The compound thus prepared is useful in curable compositions.
摘要翻译：描述了制备氨基甲酸酯或脲官能化合物的方法，其包括使内酯或羟基羧酸与包含氨基甲酸酯或脲基团的化合物（A）或可转化为氨基甲酸酯或脲基团的基团反应的步骤，和能够与羟基羧酸反应或与内酯开环反应的活性氢基团。由此制备的化合物可用于可固化组合物中。

10. 发明授权

US5945499A High solids thermosetting compositions with dual cure mechanism 失效
标题翻译：具有双固化机理的高固含量热固性组合物
公开(公告)号：US5945499A
公开(公告)日：1999-08-31
申请号：US968395
申请日：1997-11-12
申请人： Walter H. Ohrbom , Paul J. Harris
发明人： Walter H. Ohrbom , Paul J. Harris
IPC分类号： C08G18/62 , C08G18/80 , C09D175/04 , C09D201/02 , C09D201/06 , C08G18/63
CPC分类号： C09D175/04 , C08G18/6225 , C08G18/807 , C08G18/8093 , C09D201/025 , C09D201/06 , Y10S525/903 , Y10T428/31551
摘要： Disclosed is a curable coating composition that includes a compound having carbamate functionality of the structure ##STR1## wherein R is H or alkyl, a compound having hydroxyl functionality, a polyisocyanate crosslinking agent, and an aminoplast crosslinking agent. The effective equivalents of the aminoplast crosslinking agent is equal to or less than the equivalents of carbamate functionality and the effective equivalents of polyisocyanate crosslinker is equal to or less than the equivalents of hydroxyl functionality. The carbamate-functional resin and the aminoplast crosslinking agent provide rheology control during the early part of the bake to cure an applied coating of the coating composition.
摘要翻译：公开了一种可固化涂料组合物，其包含具有其中R为H或烷基的结构的氨基甲酸酯官能团，具有羟基官能团的化合物，多异氰酸酯交联剂和氨基塑料交联剂的化合物。氨基塑料交联剂的有效当量等于或小于氨基甲酸酯官能度的当量，多异氰酸酯交联剂的有效当量等于或小于羟基官能度的当量。氨基甲酸酯官能树脂和氨基塑料交联剂在烘烤的早期阶段提供流变控制，以固化涂料组合物的涂覆涂层。

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