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1. 发明授权

US5175259A Mono- and bis-azo compounds containing 6-hydroxy-3-heterocyclic onium-pyridone-2-groupings coupled to diazo components containing diazine or triazine rings 失效
标题翻译：含有6-羟基-3-杂环基的β-吡咯烷酮-2-基团的单 - 和双 - 异氰酸酯化合物与含有二氮杂环或三嗪环的DIAZO组分相连
公开(公告)号：US5175259A
公开(公告)日：1992-12-29
申请号：US843193
申请日：1992-02-28
申请人： Joerg L. Jessen , Manfred Ruske , Knut Kessel , Manfred Patsch
发明人： Joerg L. Jessen , Manfred Ruske , Knut Kessel , Manfred Patsch
IPC分类号： C09B62/085 , C09B62/04 , C09B62/245 , C09B62/44 , C09B62/51 , D06P1/38
CPC分类号： C09B62/245 , C09B62/04 , C09B62/4411
摘要： Reactive dyes of the formula ##STR1## where n is 1 or 2,X is a six-membered halogen-containing nitrogen heterocycle,L.sup.1, depending on n, is fluorine, chlorine, C.sub.1 -C.sub.4 -alkoxy, phenoxy, C.sub.1 -C.sub.4 -alkyl, substituted or unsubstituted phenyl or a bridge member which has one or two hydroxysulfonyl groups,D is the radical of a diazo component of the aniline or naphthalene series which has at least one hydroxysulfonyl group,L.sup.2 is hydrogen or substituted or unsubstituted C.sub.1 -C.sub.8 -alkyl,L.sup.3 is the cationic radical of an aromatic heterocycle which is linked to the pyridone ring via a nitrogen atom, andL.sup.4 is hydrogen or C.sub.1 -C.sub.4 -alkyl,with the proviso that the number of hydroxysulfonyl groups in the molecule exceeds that of the cationic groups by at least one, are useful for dyeing and printing hydroxyl- or nitrogen-containing substrates.
摘要翻译：式中，n为1或2的反应性染料，X为6元含卤素的氮杂环，L1取决于n，为氟，氯，C 1 -C 4 - 烷氧基，苯氧基，C 1 -C 4 - 烷基，取代或未取代的苯基或具有一个或两个羟基磺酰基的桥连构件，D是具有至少一个羟基磺酰基的苯胺或萘系的重氮组分的基团，L2是氢或取代或未取代的C1-C8 - 烷基，L3是通过氮原子与吡啶酮环连接的芳族杂环的阳离子基团，L4是氢或C1-C4-烷基，条件是分子中羟基磺酰基的数目超过通过至少一个的阳离子基团可用于染色和印刷含羟基或含氮底物。

2. 发明授权

US5210187A Double attachment reactive dyes having alkyl- or alkenylsulfonyl and alkyl- or alkenylsulfonylalkyl groups 失效
标题翻译：具有烷基或烯基磺酰基和烷基 - 或烯基磺酰基烷基的双连接活性染料
公开(公告)号：US5210187A
公开(公告)日：1993-05-11
申请号：US865744
申请日：1992-04-09
申请人： Manfred Patsch , Uwe Nahr , Friedrich Wirsing , Joerg L. Jessen , Klaus Pandl , Claus Marschner , Matthias Dust
发明人： Manfred Patsch , Uwe Nahr , Friedrich Wirsing , Joerg L. Jessen , Klaus Pandl , Claus Marschner , Matthias Dust
IPC分类号： C07C317/14 , C07C317/32 , C09B62/02 , C09B62/44 , C09B62/503
CPC分类号： C09B62/4403 , C07C317/14 , C07C317/32 , C09B62/02 , C09B62/503
摘要： Double attachment reactive dyes have the formula ##STR1## where U.sup.1 is C.sub.1 -C.sub.4 -alkyl, phenyl, C.sub.2 -C.sub.10 -alkenyl or the radical ##STR2## where Q.sup.1 and Q.sup.2 are each independently of the other hydrogen or C.sub.1 -C.sub.4 -alkyl and Q.sup.3 is a group which is detachable under alkaline reaction conditions,Z is the radical ##STR3## where each Q.sup.4 is independently of the other hydrogen or C.sub.1 -C.sub.4 -alkyl which may be substituted by cyano, U.sup.2 is C.sub.1 -C.sub.4 -alkyl, phenyl, C.sub.2 -C.sub.10 -alkenyl or the radical ##STR4## where Q.sup.5 and Q.sup.6 are each independently of the other hydrogen or C.sub.1 -C.sub.4 -alkyl and Q.sup.7 is a group which is detachable under alkaline reaction conditions, and w is 0, 1 or 2,t is 0, 1 or 2,v is 1 or 2 and X and L are each as defined in the description, with the proviso that at least one of the two radicals U.sup.1 and U.sup.2 is not C.sub.1 -C.sub.4 -alkyl or phenyl, and are prepared from benzyl compounds of the formula ##STR5## where A is nitro or amino and U.sup.1, Z and t are each as defined above. The reactive dyes are useful for dyeing hydroxyl-containing fibers such as cotton and wool and provide high yields and high wet fastness.
摘要翻译：双连接活性染料具有式“IMAGE”，其中U1是C1-C4-烷基，苯基，C2-C10-烯基或基团，其中Q1和Q2各自独立地是氢或C1-C4-烷基， Q3是在碱性反应条件下可分离的基团，Z是基团，其中每个Q 4独立于可被氰基取代的另一个氢或C 1 -C 4 - 烷基，U 2是C 1 -C 4 - 烷基，苯基，C 2 -C 10 - 烯基或基团，其中Q 5和Q 6各自独立地为氢或C 1 -C 4 - 烷基，Q 7为在碱性反应条件下可分离的基团，w为0,1或2 ，t为0,1或2，v为1或2，X和L各自如说明书中所定义，条件是两个基团U1和U2中的至少一个不是C 1 -C 4 - 烷基或苯基，并且由式为“IMAGE”的苄基化合物制备，其中A是硝基或氨基，并且U1，Z和t各自如上所定义。活性染料可用于染色含有羟基的纤维如棉和羊毛，并提供高产率和高耐湿牢度。

3. 发明授权

US5245020A Reactive dyes with two or three nitrogen-containing haloheterocycles as reactive system 失效
标题翻译：具有两个或三个含氮卤素杂环的活性染料作为反应体系
公开(公告)号：US5245020A
公开(公告)日：1993-09-14
申请号：US853518
申请日：1992-03-18
申请人： Joerg L. Jessen , Klaus Pandl , Hermann Loeffler , Bernd Siegel , Manfred Patsch
发明人： Joerg L. Jessen , Klaus Pandl , Hermann Loeffler , Bernd Siegel , Manfred Patsch
IPC分类号： C09B62/04
CPC分类号： C09B62/043
摘要： Reactive dyes of the formula ##STR1## where l is 0 or 1,n is 0 or 1,E is nitrogen or C--ClA is the radical of an azo dye attached to the triazine ring via an imino or C.sub.1 -C.sub.4 -alkylimido group,B--if E is nitrogen--is the radical of an azo dye or of a formazan dye which in either case is bonded to the triazine ring via an imino of C.sub.1 -C.sub.4 -alkylimino group or else--if n is 0--is fluorine, chlorine or unsubstituted or substituted amino, or--if E is C--Cl--is fluorine, chlorine or methyl,X.sup.1 and X.sup.2 are independently of the other fluorine or chlorine,X.sup.3 is fluorine or chlorine or else--if E is C--Cl--methylsulfonyl andZ.sup.1 and Z.sup.2 are independently of the the other a radical of the formula ##STR2## where L.sup.3 and L.sup.4 are independently of the other hydrogen or unsubstituted or substituted C.sub.1 -C.sub.4 -alkyl,with the proviso that l and n are not simultaneously 0 and that, if E is C--Cl or if n is 0 and Z.sup.1 is the radical of the formula ##STR3## where L.sup.3 and L.sup.4 are each as defined above, A may also be the radical of a formazan dye which is bonded to the triazine ring via an imino or C.sub.1 -C.sub.4 -alkylimino group, are useful for dyeing or printing hydroxyl- or nitrogen-containing substrates.
摘要翻译：其中l为0或1的反应性染料，其中l为0或1，n为0或1，E为氮或C-Cl为经由亚氨基或C 1 -C 4烷基亚氨基连接到三嗪环上的偶氮染料的基团基团，B-如果E是氮，则是偶氮染料或甲an染料的基团，在任一情况下，通过C 1 -C 4 - 烷基亚氨基的亚氨基键合到三嗪环，或者 - 如果n是0- 氟，氯或未取代或取代的氨基，或 - 如果E是C-Cl-是氟，氯或甲基，则X1和X2独立于其它氟或氯，X3是氟或氯，或者 - 如果E是C- Cl-甲基磺酰基，Z 1和Z 2独立地为下式的基团：其中L 3和L 4独立于另一个氢或未取代或取代的C 1 -C 4 - 烷基，条件是 l和n不同时为0，并且如果E是C-Cl，或者如果n是0，并且Z1是式“IMAGE”的基团，其中L3和L4各自如上定义，则A也可以是通过亚氨基或C 1 -C 4烷基亚胺基与三嗪环结合的甲an染料的基团可用于染色或印刷含羟基或含氮基底。

4. 发明授权

US5241055A Reactive dyes with a reactive system based on alkenylsulfonyl and benzyl compounds as intermediates therefor 失效
标题翻译：具有基于烯基磺酰基和苄基化合物的反应体系的活性染料作为其中间体
公开(公告)号：US5241055A
公开(公告)日：1993-08-31
申请号：US899943
申请日：1992-06-17
申请人： Claus Marschner , Joerg L. Jessen , Klaus Pandl , Manfred Patsch
发明人： Claus Marschner , Joerg L. Jessen , Klaus Pandl , Manfred Patsch
IPC分类号： C07C317/14 , C07C317/36 , C09B62/44
CPC分类号： C09B62/4403 , C07C317/14 , C07C317/36
摘要： Reactive dyes useful for dyeing or printing hydroxyl- or nitrogen-containing substrates have the formula ##STR1## where U is vinyl, propenyl or the radical of the formula ##STR2## in which Z.sup.1 is hydrogen or methyl and Z.sup.2 is a group which is detachable under alkaline reaction conditions,X isa) the radical of a chromophore orb) the radical of a coupling component to which may be additionally attached the radical of a diazo component via an azo linkage and which may contain an additional reactive group, andL isa) a bridge member of the formula ##STR3## where Q.sup.1 is hydrogen or C.sub.1 -C.sub.4 -alkyl, Q.sup.2 and Q.sup.3 are each independently of the other hydrogen or C.sub.1 -C.sub.4 -alkyl, and Q.sup.4 is a leaving group, orb) an azo linkage,the radical X-L being bonded to the benzene ring meta or para to the CH.sub.2 -SO.sub.3 H group,and their preparation may involve novel benzyl compounds as intermediates.
摘要翻译：可用于染色或印刷含羟基或含氮底物的活性染料具有式“IMAGE”，其中U是乙烯基，丙烯基或式（IMAGE）基团，其中Z1是氢或甲基，Z2是可分离的基团在碱性反应条件下，X是a）发色团的基团或b）偶联组分的基团，其可以另外通过偶氮键连接重氮组分的基团，并且可以含有另外的反应性基团，并且L 是a）式为“IMAGE”的桥式成员，其中Q1为氢或C1-C4-烷基，Q2和Q3各自独立于另一个氢或C 1 -C 4 - 烷基，Q 4为离去基团，或b）偶氮键，基团XL键合到CH2-SO3H基团的间位或对位的苯环上，它们的制备可以包括新的苄基化合物作为中间体。

5. 发明授权

US5149789A Reactive dyes with two or three nitrogen-containing haloheterocycles as reactive system 失效
标题翻译：具有两种或三种含有硝酸的氢化物作为反应体系的反应性染料
公开(公告)号：US5149789A
公开(公告)日：1992-09-22
申请号：US490710
申请日：1990-03-08
申请人： Joerg L. Jessen , Klaus Pandl , Hermann Loeffler , Bernd Siegel , Manfred Patsch
发明人： Joerg L. Jessen , Klaus Pandl , Hermann Loeffler , Bernd Siegel , Manfred Patsch
IPC分类号： C09B50/00 , C09B62/04 , C09B62/08 , D06P3/10 , D06P3/66
CPC分类号： C09B62/043
摘要： Reactive dyes of the formula ##STR1## where 1 is 0 or 1,n is 0 or 1,E is nitrogen or C--Cl,A is the radical of an azo dye attached to the triazine ring via an imino or C.sub.1 -C.sub.4 -alkylimino group,B--if E is nitrogen--is the radical of an azo dye or of a formazan dye which in either case is bonded to the triazine ring via an imino or C.sub.1 -C.sub.4 -alkylimino group or else--if n is 0--is fluorine, chlorine or unsubstituted or substituted amino, or --if E is C--C1--is fluorine, chlorine or methyl,X.sup.1 and X.sup.2 are independently of the other fluorine or chlorine,X.sup.3 is fluorine or chlorine or else--if E is C--Cl--methylsulfonyl andZ.sup.1 and Z.sup.2 are independently of the other a radical of the formula ##STR2## where L.sup.3 and L.sup.4 are independently of the other hydrogen or unsubstituted or substituted C.sub.1 -C.sub.4 -alkyl,with the proviso that l and n are not simultaneously 0 and that, if E is C--Cl or if n is 0 and Z.sup.1 is the radical of the formula ##STR3## where L.sup.3 and L.sup.4 are each as defined above, A may also be the radical of a formazan dye which is bonded to the triazine ring via an imino or C.sub.1 -C.sub.4 -alkylimino group, are useful for dyeing or printing hydroxyl- or nitrogen-containing substrates.
摘要翻译：式1的反应性染料，其中1为0或1，n为0或1，E为氮或C-Cl，A为通过亚氨基或C 1 -C 4烷基连接到三嗪环上的偶氮染料的基团，烷基亚氨基，B-如果E是氮 - 是偶氮染料或甲an染料的基团，其在任一情况下通过亚氨基或C 1 -C 4 - 烷基亚氨基键合到三嗪环，否则 - 如果n是0- 是氟，氯或未取代或取代的氨基，或 - 如果E是C-C1 - 是氟，氯或甲基，则X1和X2独立于其他氟或氯，X3是氟或氯，或者 - 如果E是C -Cl-甲基磺酰基，Z 1和Z 2独立地为下式的基团：其中L 3和L 4独立于另一个氢或未取代或取代的C 1 -C 4 - 烷基，其中条件是l和n不同时为0，并且如果E是C-Cl或如果n是0，并且Z1是式“IMAGE”的基团，其中L3和L4各自如上所定义，A也可以是t 通过亚氨基或C 1 -C 4烷基亚胺基与三嗪环结合的甲an染料的基团可用于染色或印刷含羟基或含氮基底。

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