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1. 发明申请

US20080092307A1 Use of tetra-azapentamethine compounds as direct dyeing agents and novel tetra-azapentamethine compounds 失效
公开(公告)号：US20080092307A1
公开(公告)日：2008-04-24
申请号：US12000223
申请日：2007-12-11
申请人： Herve Burgaud , Herve David , Rui Pereira , Beatrice Belcour-Castro
发明人： Herve Burgaud , Herve David , Rui Pereira , Beatrice Belcour-Castro
IPC分类号： A61K8/40 , A61Q5/10 , C09B50/00
CPC分类号： C07D213/77 , C07D213/87 , C07D233/88 , C07D237/20 , C07D237/22 , C07D401/14 , C09B50/10
摘要： The invention concerns the use as direct dyeing agent of at least one tetra-azapentamethine compound, a dyeing composition comprising at least such a compound, as well as a method for dyeing keratinous fibers, in particular human keratinous fibers and more particularly hair, which consists in applying at least one composition comprising such a compound. The composition also concerns tetra-azapentamethine compounds of formula (I). The invention further concerns a method for bleaching such compounds, as well as bleaching keratinous fibers previously dyed therewith.

2. 发明授权

US6086640A Formazan compounds and method of dyeing therewith 失效
标题翻译：甲an化合物及其染色方法
公开(公告)号：US6086640A
公开(公告)日：2000-07-11
申请号：US367156
申请日：1999-08-09
申请人： Toru Tabei , Eiichi Ogawa , Shin-ichi Namba
发明人： Toru Tabei , Eiichi Ogawa , Shin-ichi Namba
IPC分类号： C09B50/00 , B05D7/14 , C08B13/00 , C08L1/00 , C08L1/26 , C09B62/04 , C09B67/00 , C09B69/10 , C09D5/29 , C09D5/36 , C09D5/38 , C09D101/00 , C09D101/32 , C09K19/00 , C09K19/38 , D06P3/40 , C09B45/00
CPC分类号： C09B62/046 , C08B13/00 , C09B67/0098 , C09D5/36 , C09K19/00 , C09K19/3819 , Y10S8/918
摘要： For dyeing (printing, for example) cellulose fibers with a reactive dye, a blue compound is greatly desired, the blue compound being capable of generating a product dyed in blue at excellent dyeing reproducibility and with good light fastness and superior fastness against chlorine water, involving less staining of white area. The invention relates to a formazan compound in a free acid form as represented by the following formula I, a dyeing method of cellulose fibers using the same and a final dyed product prepared by the method, characterized in that the compound, the method and the product are suitable so as to overcome the problem.Formula I ##STR1## (wherein R represents hydrogen, sulfo group, hydroxyl group, halogen, a C1-C4 alkyl group, a C1-C4 alkoxyl group or carboxyl group; and M represents copper or nickel.)
摘要翻译： PCT No.PCT / JP98 / 00748 Sec。 371日期1999年8月9日 102（e）日期1999年8月9日PCT提交1998年2月25日PCT公布。公开号WO98 / 38252 日期1998年9月3日对于用活性染料染色（例如印刷）纤维素纤维，蓝色化合物是非常需要的，蓝色化合物能够以优异的染色重现性和良好的耐光性和优异的颜色产生蓝色染色的产品耐氯水牢度，涉及染色较少的白色区域。本发明涉及以下式I表示的游离酸形式的甲an化合物，使用其的纤维素纤维的染色方法和通过该方法制备的最终染色产物，其特征在于，化合物，方法和产物是适合的，以克服这个问题。式I（其中R表示氢，磺基，羟基，卤素，C1-C4烷基，C1-C4烷氧基或羧基; M表示铜或镍。

3. 发明授权

US6005085A Condensed azo compounds and process for preparing the same 失效
标题翻译：缩合偶氮化合物及其制备方法
公开(公告)号：US6005085A
公开(公告)日：1999-12-21
申请号：US194500
申请日：1998-11-18
申请人： Ryuzo Ueno , Masaya Kitayama , Kenji Minami , Hiroyuki Wakamori , Katsunori Tanikawa
发明人： Ryuzo Ueno , Masaya Kitayama , Kenji Minami , Hiroyuki Wakamori , Katsunori Tanikawa
IPC分类号： C09B50/00 , C07C245/10 , C07D209/88 , C07D235/26 , C07D249/14 , C07D249/20 , C07D271/10 , C07D271/107 , C07D307/52 , C09B33/147 , C09B62/04 , D06P3/40 , G03G5/06 , C08J3/20 , C09B67/20 , C09D7/12 , C09D11/00
CPC分类号： C07D271/107 , C07C245/10 , C07D209/88 , C07D235/26 , C07D249/14 , C07D249/20 , C07D307/52 , C09B33/147 , C09B62/046 , G03G5/0679 , G03G5/0681 , Y10S8/918
摘要： The present invention provides novel condensed azo compounds using bisamide compounds of 2-hydroxynaphthalene-3,6-dicarboxylic acid, amide, or ester as the couplers, which have excellent properties such as excellent water resistance, chemical resistance, solvent resistance, and heat resistance.
摘要翻译： PCT No.PCT / JP98 / 01166 Sec。 371日期：1998年11月18日 102（e）1998年11月18日日期PCT提交1998年3月19日PCT公布。公开号WO98 / 41580 日期1998年9月24日本发明提供使用2-羟基萘-3,6-二羧酸，酰胺或酯的双酰胺化合物作为成色剂的新颖的缩合偶氮化合物，其具有优异的耐水性，耐化学性，溶剂性电阻和耐热性。

4. 发明授权

US3013868A Liquid hydrocarbon compositions 失效
标题翻译：液体烃组合物
公开(公告)号：US3013868A
公开(公告)日：1961-12-19
申请号：US81603959
申请日：1959-05-27
申请人： SHELL OIL CO
发明人： THURSTON SKEI , DOUGLAS JAMES E
IPC分类号： C07C51/41 , C07C65/05 , C08F20/62 , C08F22/00 , C09B50/00 , C09K3/16 , C10L1/14 , C10L1/18 , C10L1/22 , C10L1/24 , D06L1/04
CPC分类号： D06L1/04 , C07C51/412 , C07C65/05 , C08F20/62 , C08F22/00 , C09B50/00 , C09K3/16 , C10L1/14 , C10L1/143 , C10L1/189 , C10L1/1963 , C10L1/1973 , C10L1/2283 , C10L1/2364 , C10L1/2366 , C10L1/2368 , C10L1/2437

5. 发明授权

US5858026A Dicyclic metal complex formazan derivatives, process for producing the same, composition containing the same and dyeing process employing the same 失效
标题翻译：二环金属络合甲an衍生物，其制造方法，含有它们的组合物和使用其的染色方法
公开(公告)号：US5858026A
公开(公告)日：1999-01-12
申请号：US750405
申请日：1996-12-05
申请人： Dong Gil Kim , Sung Yong Cho
发明人： Dong Gil Kim , Sung Yong Cho
IPC分类号： C07D491/044 , C09B50/00 , C09B62/018 , C09B62/44 , C09B62/503 , D06P1/38
CPC分类号： C09B62/4407 , C09B50/00
摘要： The invention relates to dicyclic metal complex formazan dye derivatives and processes for producing compositions and for using them in dyeing processes.
摘要翻译： PCT No.PCT / KR96 / 00049 Sec。 371日期：1996年12月5日 102（e）日期1996年12月5日PCT PCT 1996年4月8日PCT公布。出版物WO96 / 33240 日期：1996年10月24日本发明涉及双环金属络合物甲an染料衍生物及其制备方法及其在染色工艺中的应用。

6. 发明授权

US5563248A Fiber reactive formazan dyes containing a vinyl sulfonyl reactive group 失效
标题翻译：含有乙烯基磺酰基反应性基团的纤维反应型甲an染料
公开(公告)号：US5563248A
公开(公告)日：1996-10-08
申请号：US448277
申请日：1995-05-23
申请人： Walter Helmling , Philomen DeCroos
发明人： Walter Helmling , Philomen DeCroos
IPC分类号： C07F1/08 , C09B29/30 , C09B50/00 , C09B62/503 , C09B67/22 , D06P3/24
CPC分类号： D06P3/248 , C09B62/5036 , C09B67/0033 , C09B67/0041 , C09B67/0042 , C09B67/0052 , Y10S8/924
摘要： The invention is a dye composition containing two or more dyes of the vinyl sulfone type which can be used in combination to dye polyamide substrates. Preferably the dye compositions of the invention contain at least three dyes of different primary colors.
摘要翻译：本发明是含有两种或更多种乙烯基砜型染料的染料组合物，其可以组合用于染色聚酰胺底物。优选地，本发明的染料组合物含有至少三种不同原色的染料。

7. 发明授权

US4772323A Ink comprising at least one water soluble-formazan dye, free from cellulose-reactive groups 失效
标题翻译：油墨包含至少一种不含纤维素反应性基团的水溶性甲az染料
公开(公告)号：US4772323A
公开(公告)日：1988-09-20
申请号：US67262
申请日：1987-06-29
申请人： Anthony G. W. Baxter , Stephen B. Bostock , David Greenwood
发明人： Anthony G. W. Baxter , Stephen B. Bostock , David Greenwood
IPC分类号： C09B45/02 , C09B50/00 , C09B56/10 , C09D11/00 , C09D11/16 , D06P5/00 , C09D11/02 , C09D11/18
CPC分类号： C09D11/328 , C09B50/00 , C09B56/10
摘要： An ink comprising at least one water-soluble dye, free from cellulose-reactive groups, of the formula: ##STR1## wherein, R.sup.1 is --(C.sub.a H.sub.2a O).sub.m (C.sub.b H.sub.2b O).sub.n H,R.sup.2 is H or --(C.sub.a H.sub.2a O).sub.m (C.sub.b H.sub.2b O).sub.n H, orR.sup.1 and R.sup.2 together with the nitrogen atom form a morpholine ring;a and b are different and from 2 to 8m is from 1 to 10; n is from 0 to 9;M is H, ammonium or sodium, potassium or lithium;X is (i) NR.sup.1 R.sup.2, (ii) NR.sup.3 R.sup.4, in which R.sup.3 and R.sup.4 are each independently selected from H, alkyl and aryl, or (iii) a mono- or dis-azo chromophore consisting of benzene, naphthalene or mono- or bi-cyclic heteroaryl diazo and coupling components linked to the triazine nucleus through an amino linking group, NR.sup.9, in which R.sup.9 is H, C.sub.1-4 -alkyl or phenyl;R.sup.5 and R.sup.6 are selected from SO.sub.3 M and H provided at least one is SO.sub.3 M;R.sup.7 is H, halogen, C.sub.1-4 alkyl, C.sub.1-4 alkoxy, SO.sub.3 M or COOM; and R.sup.8 is H or SO.sub.3 M.The ink is particularly suited for ink jet printing having improved solution stability, excellent recording properties, ejection stability, ejection responsiveness and continuous recording workability.

8. 发明授权

US4758658A Water-soluble formazan dye 失效
标题翻译：水溶性甲an染料
公开(公告)号：US4758658A
公开(公告)日：1988-07-19
申请号：US909848
申请日：1986-09-22
申请人： Anthony G. W. Baxter , Stephen B. Bostock , David Greenwood
发明人： Anthony G. W. Baxter , Stephen B. Bostock , David Greenwood
IPC分类号： C09B45/02 , C09B50/00 , C09B56/10 , C09D11/00 , C09D11/16 , D06P5/00 , C09D11/02
CPC分类号： C09D11/328 , C09B50/00 , C09B56/10
摘要： A water-soluble dye, free from cellulose-reactive groups, of the formula: ##STR1## wherein R.sup.1 is --(C.sub.a H.sub.2a O).sub.m (C.sub.b H.sub.2b O).sub.n H,R.sup.2 is H or --(C.sub.a H.sub.2a O).sub.m (C.sub.b H.sub.2b O).sub.n H, orR.sup.1 & R.sup.2 together with the nitrogen atom form a morpholine ring;a & b are different and from 1 to 8m is from 1 to 10; n is from 0 to 9;M is H, ammonium or a monovalent metal;X is (i) NR.sup.1 R.sup.2, (ii) NR.sup.3 R.sup.4, in which R.sup.3 and R.sup.4 are each independently selected from H, alkyl and aryl, or (ii) a mono- or dis-azo chromophore comprising benzene, naphthalene or mono - or bi-cyclic heteroaryl diazo and coupling components linked to the triazine nucleus through an amino linking group;R.sup.5 & R.sup.6 are selected from SO.sub.3 M and H provided at least one is SO.sub.3 M;R.sup.7 is H, halogen, C.sub.1-4 alkyl, C.sub.1-4 alkoxy, SO.sub.3 M or COOM;and R.sup.8 is H or SO.sub.3 M,a printing ink containing the dye and a method of printing.
摘要翻译：没有纤维素反应性基团的水溶性染料，其具有下式：其中R 1是 - （CaH 2 H）m（C b H b B）n H，R 2是H或 - （CaH 2 H）m（C b H b B）n H或R 1 ＆R2与氮原子一起形成吗啉环; a＆b是不同的，1到8 m是1到10; n为0〜9; M是H，铵或一价金属; X是（i）NR 1 R 2，（ii）NR 3 R 4，其中R 3和R 4各自独立地选自H，烷基和芳基，或（ⅱ）单或二偶氮发色团，包括苯，萘或单 - 或双 - 环状杂芳基重氮和通过氨基连接基团与三嗪核连接的偶联组分; R5和R6选自SO3M和H，至少一个是SO 3 M; R 7为H，卤素，C 1-4烷基，C 1-4烷氧基，SO 3 M或COOM; R8是H或SO3M，含有染料的印刷油墨和印刷方法。

9. 发明授权

US4757135A Bicyclic formazan compounds containing a beta-sulfatoethyl-sulfonyl or vinyl sulfonyl group, suitable as fiber reactive dyestuffs 失效
标题翻译：含有β-硫酸乙基磺酰基或乙烯基磺酰基的双环甲an化合物，适合作为纤维活性染料
公开(公告)号：US4757135A
公开(公告)日：1988-07-12
申请号：US915941
申请日：1986-10-02
申请人： Gunther Schwaiger
发明人： Gunther Schwaiger
IPC分类号： C09B62/503 , C09B50/00 , D06P1/384 , D06P3/66
CPC分类号： C09B62/5036
摘要： Water-soluble copper formazan compounds of the general formula ##STR1## in which: Y is vinyl or ethyl which is substituted by a substituent eliminatable under alkaline conditions; the benzene nucleus A can be substituted by further substituents;M is hydrogen or a metal;B is substituted or unsubstituted phenylene or naphthylene;Z.sup.1 is hydrogen or a water-solubilizing group, or --B--Z.sup.1 together denote hydrogen, carboxy, cyano or nitro;D is a substituted or unsubstituted benzene or naphthalene radical; andR is hydrogen or a group of the formula ##STR2## in which R* is hydrogen or a substituted or unsubstituted lower alkyl, n denotes the number zero or 1, and Y.sup.2 is defined in the same manner as Y.These copper formazan compounds possess fiber-reactive dye properties and dye particular cellulose fiber materials in deep reddish blue to greenish blue fast shades.
摘要翻译：通式（1）的水溶性铜甲an化合物，其中：Y为乙烯基或被可在碱性条件下消除的取代基取代的乙基; 苯核A可以被其它取代基取代; M是氢或金属; B是取代或未取代的亚苯基或亚萘基; Z1是氢或水溶性基团，或-B-Z1一起表示氢，羧基，氰基或硝基; D是取代或未取代的苯或萘基; 并且R是氢或其中R *是氢或取代或未取代的低级烷基的式“IMAGE”的基团，n表示数字0或1，Y2以与Y相同的方式定义。这些铜甲an化合物具有纤维反应性染料性能，并将特定的纤维素纤维材料染成深红蓝色至绿蓝色的快速色调。

10. 发明授权

US4336190A Copper complex formazan compounds, process for their manufacture and their use as dyestuffs 失效
标题翻译：铜复合甲烷化合物，其制造方法及其作为染料的使用
公开(公告)号：US4336190A
公开(公告)日：1982-06-22
申请号：US204915
申请日：1980-11-07
申请人： Gunther Schwaiger , Ernst Hoyer
发明人： Gunther Schwaiger , Ernst Hoyer
IPC分类号： C09B62/503 , D06P1/384 , C09B50/00
CPC分类号： C09B62/5036 , Y10S8/918
摘要： This invention relates to novel copper complex formazan compounds of the formula ##STR1## in which M is hydrogen or the equivalent of a metal and R is hydrogen or chlorine. The invention also relates to a process for their manufacture. The compounds can be used as dyestuffs, in particular fiber reactive dyestuffs for dyeing cellulose fiber materials, wool, or synthetic polyamide fiber materials for example, on which they exhibit intense blue dyeings having good fastness properties.
摘要翻译：本发明涉及式为“IMAGE”的新型铜络合物甲an化合物，其中M为氢或相当于金属，R为氢或氯。本发明还涉及其制造方法。这些化合物可以用作染料，特别是用于染色纤维素纤维材料，羊毛或合成聚酰胺纤维材料的纤维活性染料，例如，它们表现出具有良好牢度性质的强烈蓝色染色。

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