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1. 发明授权

US4294934A Process for the production of elastic, optionally cellular, polyurethane ureas 失效
标题翻译：用于生产弹性，任选细胞的聚氨酯脲的方法
公开(公告)号：US4294934A
公开(公告)日：1981-10-13
申请号：US164752
申请日：1980-06-30
申请人： Gerhard Grogler , Jurgen Schwindt , Otto Ganster , Hans-Joachim Meiners , Hans-Dieter Ruprecht
发明人： Gerhard Grogler , Jurgen Schwindt , Otto Ganster , Hans-Joachim Meiners , Hans-Dieter Ruprecht
IPC分类号： C08G18/00 , C08G18/10 , C08G18/72 , C08G18/76 , C08G18/18 , C08G18/22
CPC分类号： C08G18/7671 , C08G18/10 , C08G2101/0008 , C08G2350/00 , C08G2380/00 , C08G2410/00 , Y10S528/906
摘要： The instant invention is directed to a process for the production of polyurethane urea elastomers having a gross density of more than 200 kg/m.sup.3 comprising: casting a reaction mixture of(A) an isocyanate prepolymer produced from(a) 1 mole of a compound containing at least 2 Zerewitinoff-active hydrogen atoms and having a molecular weight of from 400 to 10,000 and(b) 2 to 10 moles of diisocyanatodiphenylmethane,(B) an aromatic diamine, and(C) 0 to 50 mole percent, based on component (B), of a polyol containing primary hydroxyl groups and having a molecular weight of from 62 to 6000, the equivalent ratio between component (A) and components (B) + (C) amounting to between 0.9:1 and 1.3:1,into a mold, hardening the reaction mixture in the mold and subsequently removing it from the mold, the improvement wherein said isocyanate prepolymer (A) has been produced using an isomer mixture comprising:from 15 to 80 mole percent of 2,4'-diisocyanatodiphenylmethane,from 20 to 85 mole percent of 4,4'-diisocyanatodiphenylmethane, andfrom 0 to 20 mole percent of 2,2'-diisocyanatodiphenylmethane.
摘要翻译：本发明涉及生产总密度大于200kg / m 3的聚氨酯脲弹性体的方法，包括：浇铸（A）异氰酸酯预聚物的反应混合物，该异氰酸酯预聚物由（a）1摩尔含有至少2个Zerewitinoff活性氢原子，分子量为400至10,000，和（b）2至10摩尔二异氰酸二苯基甲烷，（B）芳族二胺和（C）0至50摩尔％，基于组分（ B），含有伯羟基并且分子量为62至6000的多元醇，组分（A）和组分（B）+（C）之间的当量比为0.9:1至1.3:1，转化为模具，使模具中的反应混合物硬化，随后将其从模具中除去，改进之处在于所述异氰酸酯预聚物（A）已经使用异构体混合物制备，所述异构体混合物包含：15至80摩尔％的2,4'-二异氰酸根合二苯基甲烷， 20至85摩尔％o f 4,4'-二异氰酸二苯基甲烷和0至20摩尔％的2,2'-二异氰酸二苯基甲烷。

2. 发明授权

US4343339A Process for the production of tires comprising vulcanized elastomers containing urethane groups 失效
标题翻译：用于生产包含含有氨基甲酸酯基团的硫化弹性体的轮胎的方法
公开(公告)号：US4343339A
公开(公告)日：1982-08-10
申请号：US189496
申请日：1980-09-22
申请人： Jurgen Schwindt , Otto Ganster , Hans-Joachim Meiners
发明人： Jurgen Schwindt , Otto Ganster , Hans-Joachim Meiners
IPC分类号： C08G18/00 , C08G18/40 , C08G18/69 , C08G18/87 , C08G18/82 , B60C1/00 , C08G18/62
CPC分类号： C08G18/87 , C08G18/69 , C08G2380/00 , Y10S152/905 , Y10T152/10495
摘要： The instant invention is directed to a process for the production of vulcanized elastomers containing urethane groups by casting, comprising:(A) mixing the following components:(1) liquid diene polymers containing isocyanate reactive functional groups,(2) compounds having molecular weights of from 400 to 10,000, and containing at least two hydroxyl groups,(3) polyisocyanates,(4) cross-linking agents having molecular weights of from 32 to 400 and containing at least two active hydrogen atoms,(5) vulcanization agents used for vulcanization and optionally(6) reinforcing fillers; and subsequently(B) pouring the mixture into a mold and allowing the mixture to react in the mold; and subsequently(C) vulcanizing the molded product at temperatures above 120.degree. C.
摘要翻译：本发明涉及通过铸造生产含有氨基甲酸酯基团的硫化弹性体的方法，包括：（A）混合以下组分：（1）含有异氰酸酯反应性官能团的液体二烯聚合物，（2）分子量为 400至10,000，并且含有至少两个羟基，（3）多异氰酸酯，（4）分子量为32-400的交联剂，并含有至少两个活性氢原子，（5）用于硫化的硫化剂和任选的（6）增强填料; 然后（B）将混合物倒入模具中并使混合物在模具中反应; 随后（C）在120℃以上的温度下硫化成型产品。

3. 发明授权

US5283364A Hydrolysis process for polyamines 失效
标题翻译：多胺的水解过程
公开(公告)号：US5283364A
公开(公告)日：1994-02-01
申请号：US4808
申请日：1993-01-15
申请人： Werner Rasshofer , Klaus Konig , Hans-Joachim Meiners , Gerhard Grogler
发明人： Werner Rasshofer , Klaus Konig , Hans-Joachim Meiners , Gerhard Grogler
IPC分类号： C08G18/10 , C08G18/46 , C08G18/50 , C07C85/00
CPC分类号： C08G18/5048 , C08G18/10 , C08G18/4623
摘要： Polyamines containing primary amino groups are made by hydrolyzing an isocyanate with water in the presence of a solvent which is a carboxylic acid amide. The solvent must be used in a quantity of at least 10% by weight solvent based on 100% by weight of isocyanate. The weight ratio of solvent to water must be from 3 to 200. A homogeneous phase is maintained during the hydrolysis which is carried out at temperatures of from 20.degree. to 210.degree. C. A not incorporable basic and/or metal catalyst particularly alkali metal hydroxides may be employed. The polyamines produced by this process are particularly useful for the production of polyurethanes.
摘要翻译：含羧基酰胺的溶剂存在下，通过用水水解异氰酸酯制备含有伯氨基的多胺。溶剂必须使用至少10重量％的溶剂，基于100重量％的异氰酸酯。溶剂与水的重量比必须为3至200.在水解期间保持均相，其在20至210℃的温度下进行。不合并的碱性和/或金属催化剂，特别是碱金属氢氧化物可以被雇用。通过该方法生产的多胺特别可用于生产聚氨酯。

4. 发明授权

US4107152A Polyurethanes produced from phosphorus containing flame retarding agents which are reactive with isocyanates 失效
标题翻译：由与含异氰酸酯反应的含磷阻燃剂生产的聚氨酯
公开(公告)号：US4107152A
公开(公告)日：1978-08-15
申请号：US829833
申请日：1977-09-01
申请人： Hans Hubner , Johannes Blahak , Hans-Joachim Meiners
发明人： Hans Hubner , Johannes Blahak , Hans-Joachim Meiners
IPC分类号： C07F9/40 , C07F9/53 , C08G18/38 , C08G18/32
CPC分类号： C07F9/4021 , C07F9/5325 , C08G18/3889
摘要： This invention relates to novel flame retarding agents and processes in which they are used in the production of polyurethanes. These compounds are represented by the general formula: ##STR1## wherein: A and L, which are identical or different, represent optionally branched C.sub.1 -C.sub.17 -alkyl groups or -OR groups wherein R represents an optionally branched C.sub.1 -C.sub.8 -alkyl group, andX represents hydrogen, halogen, an optionally branched C.sub.1 -C.sub.8 alkyl group, a C.sub.6 -C.sub.12 aryl or aralkyl group, NH.sub.2, CF.sub.3, CN, COOR', SO.sub.3 R', ##STR2## wherein: R' represents hydrogen or an optionally branched alkyl or cycloalkyl group having 1-10 C atoms andR" represents an optionally branched alkyl or cycloalkyl group having 1-10 C atoms.
摘要翻译：本发明涉及新型阻燃剂及其制备聚氨酯的方法。这些化合物由以下通式表示：其中：

5. 发明授权

US4107103A Polyurethanes produced from phosphorus containing flame retarding agents which are reactive with isocyanates 失效
标题翻译：由与含异氰酸酯反应的含磷阻燃剂生产的聚氨酯
公开(公告)号：US4107103A
公开(公告)日：1978-08-15
申请号：US836189
申请日：1977-09-26
申请人： Hans Hubner , Johannes Blahak , Hans-Joachim Meiners
发明人： Hans Hubner , Johannes Blahak , Hans-Joachim Meiners
IPC分类号： C07F9/6521 , C08G18/38 , C08G18/32
CPC分类号： C07F9/65216 , C08G18/3889
摘要： This invention relates to novel halogen-free flame retarding agents and a process in which they are used in the production of polyurethanes. These compounds are represented by the general formula: ##STR1## wherein: R.sub.1 represents C.sub.1 -C.sub.5 alkylene groups which may be branched,R.sub.2 represents C.sub.1 -C.sub.3 alkyl groups which may be branched or R.sub.1 OH andR.sub.3 represents C.sub.1 -C.sub.8 -alkyl, C.sub.1 -C.sub.8 -dialkylamino, C.sub.1 -C.sub.4 -oxyalkyl, C.sub.1 -C.sub.4 -thioslkyl, C.sub.6 -C.sub.14 -aryl or C.sub.7 -C.sub.15 -aralkyl groups or ##STR2## and A and L may be identical or different and represent C.sub.1 -C.sub.10 -alkyl groups, which may be branched, benzyl groups or OR groups, whereinR represents an alkyl group, with 1-8 C atoms which may be branched, or a benzyl group.
摘要翻译：本发明涉及新型无卤素阻燃剂及其制备聚氨酯的方法。这些化合物由以下通式表示：其中：

6. 发明授权

US4101468A Process for cold-hardening polyurethane foams using sulfonamide emulsifiers 失效
标题翻译：使用磺酰胺乳化剂的冷硬化聚氨酯泡沫的方法
公开(公告)号：US4101468A
公开(公告)日：1978-07-18
申请号：US767608
申请日：1977-02-10
申请人： Hermann Perrey , Hans-Joachim Meiners , Jurgen Ick
发明人： Hermann Perrey , Hans-Joachim Meiners , Jurgen Ick
IPC分类号： B01F17/26 , C08J9/00 , C08G18/14 , C07C143/72
CPC分类号： C08J9/0061 , C08J9/0033 , C08J2375/08 , C08J2471/00 , Y10S521/904
摘要： The invention relates to a process for preparing cold-hardening foams containing urethane groups using as an emulsifier, sulphonamide compounds of the formula: ##STR1## wherein R represents an alkyl, chloroalkyl, cycloalkyl radical having from 8 to 30 carbon atoms, or an alkaryl radical having from 10 to 30 carbon atoms,R.sup.1 and R.sup.2, which may be the same or different, each represent a hydrogen atom, a chloromethyl, methyl, ethyl or phenyl radical,m is an integer of from 0 to 50,R.sup.3 represents a hydrogen atom, an alkyl, aralkyl, alkaryl, aryl radical or a --(CHR.sup.1 -CHR.sup.2 -O-).sub.m R.sup.4 - group andR.sup.4 represents a hydrogen atom, an alkyl, aralkyl, acyl, carbamoyl or cyanalkyl radical having from 1 to 20 carbon atoms.The use of these additions results in an increase in compression hardness without detrimental effects on other foam properties.
摘要翻译：本发明涉及一种使用乳化剂制备含有氨基甲酸酯基团的冷硬化泡沫的方法，下式的磺酰胺化合物：其中R表示烷基，氯代烷基，具有8至30个碳原子的环烷基或烷芳基具有10至30个碳原子的基团，R 1和R 2可以相同或不同，各自表示氢原子，氯甲基，甲基，乙基或苯基，M为0至50的整数，R 3表示氢原子，烷基，芳烷基，烷芳基，芳基或 - （CHR 1 -CHR 2 -O-）m R 4 - 基，R 4表示氢原子，具有1至20个碳的烷基，芳烷基，酰基，氨基甲酰基或氰基烷基原子

7. 发明授权

US4022720A Process for the production of polyurethane foams 失效
标题翻译：生产聚氨酯泡沫的方法
公开(公告)号：US4022720A
公开(公告)日：1977-05-10
申请号：US579522
申请日：1975-05-21
申请人： Johannes Blahak , Hans-Joachim Meiners
发明人： Johannes Blahak , Hans-Joachim Meiners
IPC分类号： C07C271/20 , C08G18/18 , C07C97/02
CPC分类号： C08G18/1841 , C07C271/20
摘要： The present invention relates to a process for the production of polyurethane foams by reacting1. organic compounds with at least two hydrogen atoms capable of reacting with isocyanates and having molecular weights in the range from 400 to 10,000,2. polyisocyanates,3. water and/or organic blowing agents in the presence of catalysts containing tertiary nitrogen and, optionally, other additives, the improvement wherein the catalysts used are polyacyl compounds corresponding to the general formula: ##STR1## wherein A represents a C.sub.1 -C.sub.6 alkylene group, preferably a C.sub.2 or C.sub.3 alkylene group;R represents a C.sub.1 -C.sub.5 alkyl group, preferably methyl or ethyl;X represents an acyl group, preferably ##STR2##
摘要翻译：本发明涉及一种生产聚氨酯泡沫的方法，该方法是通过使有机化合物与至少两个可与异氰酸酯反应并具有400至10,000的范围内的分子量的氢原子反应而生成的。2.聚异氰酸酯，3.水和 /或有机发泡剂在含有苛性氮的催化剂存在下，以及任选的其它添加剂，所使用的催化剂的改进是与通用公式相关的聚酰胺化合物：其中A表示C1-C6亚烷基，优选为 C2或C3亚烷基; R表示C1-C5烷基，优选甲基或乙基; X表示酰基，优选

8. 发明授权

US5262448A Process for the preparation of polyurea elastomers containing urethane groups 失效
标题翻译：制备含氨基甲酸酯基团的聚脲弹性体的方法
公开(公告)号：US5262448A
公开(公告)日：1993-11-16
申请号：US515885
申请日：1990-04-27
申请人： Andreas Ruckes , Hans-Joachim Meiners , Heinrich Boden , Manfred Schmidt
发明人： Andreas Ruckes , Hans-Joachim Meiners , Heinrich Boden , Manfred Schmidt
IPC分类号： C08G18/66 , C08G18/10 , C08G18/50 , C08G18/65 , C08G18/76
CPC分类号： C08G18/5048 , C08G18/10 , C08G18/5024 , C08G2101/0008 , C08G2101/0033 , C08G2101/0066 , C08G2120/00
摘要： The present invention relates to a process for the production of an optionally cellular elastomeric molded article having a compact surface and based on a polyurea elastomer containing urethane groups which is the reaction product ofa) a polyisocyanate component based on a polyisocyanate of the diphenylmethane series,b) a polyol component based on a polyether polyol, a polyester polyol or mixtures thereof andc) a polyamine component containing1) 50 to 95% by weight, based on the weight of component c), of at least one sterically hindered aromatic diamine and2) 5 to 50% by weight, based on the weight of component c), of at least one compound which has a molecular weight of about 1,000 to 12,000,by reacting component a) with at least 90% by weight of component b) at an NCO/OH equivalent ratio of at least 4:1 to form an NCO semi-prepolymer and subsequently reacting the NCO semi-prepolymer with component c) and the remainder of component b) by the reaction injection molding process to form the polyurea elastomer containing urethane groups, component c) being present in an amount sufficient to provide an isocyanate index, based on the reactive groups of components a), b) and c), of 70 to 130.
摘要翻译：本发明涉及一种制备具有紧凑表面并且基于含有氨基甲酸酯基团的聚脲弹性体的任选多孔弹性体模塑制品的方法，该聚脲弹性体是a）基于二苯基甲烷系列的多异氰酸酯的多异氰酸酯组分的反应产物， b）基于聚醚多元醇，聚酯多元醇或其混合物的多元醇组分和c）多胺组分，其含有1）基于组分c）的重量计50至95重量％的至少一种空间位阻芳族二胺和2）基于组分c）重量的5-50重量％的至少一种分子量为约1,000至12,000的化合物，通过使组分a）与至少90重量％的组分b ），以至少4:1的NCO / OH当量比形成NCO半预聚物，随后通过反应注射成型工艺t将NCO半预聚物与组分c）和组分b）的剩余部分反应 o形成含有氨基甲酸酯基团的聚脲弹性体，组分c）以足以提供异氰酸酯指数的量存在，基于组分a），b）和c）的反应性基团为70至130。

9. 发明授权

US5504179A Process for the manufacture of flexible molded parts 失效
标题翻译：柔性模制件制造工艺
公开(公告)号：US5504179A
公开(公告)日：1996-04-02
申请号：US521204
申请日：1995-08-30
申请人： Hans-Joachim Meiners , Peter Haas , Eduard Mayer , Karl-Heinz Dorner
发明人： Hans-Joachim Meiners , Peter Haas , Eduard Mayer , Karl-Heinz Dorner
IPC分类号： C08G18/08 , C08G18/10 , C08G18/34
CPC分类号： C08G18/089 , C08G18/10 , C08G2120/00
摘要： The present invention is directed to a RIM process wherein an isocyanate-terminated prepolymer is reacted with one or more isocyanate-reactive components which contian inorganic fillers. The improvement resides in including an acidc group containing compound with the isocyanate reactive components.
摘要翻译：本发明涉及一种RIM方法，其中异氰酸酯封端的预聚物与一种或多种与无机填料相关的异氰酸酯反应性组分反应。改进在于包括含酸基团的化合物与异氰酸酯反应性组分。

10. 发明授权

US4206289A Process for the production of cold-curing foam resins which contain urethane groups 失效
标题翻译：用于生产含有氨基甲酸酯基团的冷固化泡沫树脂的方法
公开(公告)号：US4206289A
公开(公告)日：1980-06-03
申请号：US6988
申请日：1979-01-29
申请人： Hans-Joachim Meiners , Klaus Seyfried , Armand de Montigny , Rolf Baumhakel
发明人： Hans-Joachim Meiners , Klaus Seyfried , Armand de Montigny , Rolf Baumhakel
IPC分类号： C08G18/40 , C08G18/65 , C08J9/00 , C08G18/14 , C07F7/08 , C08G18/38
CPC分类号： C08J9/0061 , C08G18/4072 , C08G18/6564 , C08J9/0042 , C08G2101/0008 , C08G2101/005 , C08G2101/0083 , C08J2375/04 , C08J2483/00 , Y10S521/904
摘要： A process for making cold-setting, non-shrinkable polyurethane foam resins using a mixture of silicon compounds of the formula:A.sub.x B.sub.x+2whereinx=2-25, preferably 2-5A is the group R' Si O.sub.3/2B is the group (R).sub.3 Si O.sub.1/2R represents an alkyl group having from 1 to 3 carbon atomsR' represents an aryl group having from 6 to 14 carbon atoms, with the proviso that the mixture contains at least one compound wherein x is greater than 3.
摘要翻译：使用下式的硅化合物（其中x = 2-25，优选2-5A）的硅化合物的混合物制备冷凝，不可收缩的聚氨酯泡沫树脂的方法是R'Si O 3/2 B组（R）3 SiO1 / 2R表示具有1至3个碳原子的烷基，R'表示具有6至14个碳原子的芳基，条件是该混合物含有至少一种其中x为大于3。

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