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1. 发明授权

US5225084A Process for the separation of two liquid immiscible organic components using a fibre bed as a coalescence aid 失效
标题翻译：使用纤维板作为煤焦炭辅助分离两液体无机有机组分的方法
公开(公告)号：US5225084A
公开(公告)日：1993-07-06
申请号：US761959
申请日：1991-10-17
申请人： Georg Assmann , Bernhard Gutsche , Wilhelm Johannisbauer , Richard Ridinger , Jean Rigal , Rene Armengaud , Bernard Cormary
发明人： Georg Assmann , Bernhard Gutsche , Wilhelm Johannisbauer , Richard Ridinger , Jean Rigal , Rene Armengaud , Bernard Cormary
IPC分类号： B01D17/022 , B01D17/04
CPC分类号： B01D17/045
摘要： A process for the separation, by sedimentation, of at least one liquid organic component dispersed in a liquid containing mainly organic materials, this organic component and the remaining liquid exhibiting a difference in density. In order to reduce considerably the standing time, it is proposed that the liquid be passed before sedimentation through a fiber bed that the organic component and the remaining liquid have different surface tensions with respect to the fiber bed, that the temperature of the liquid and the concentration of the organic component to be separated are such that, in the equilibrium state, at least two liquid phases form, and that the rate of flow of the liquid through the fiber bed lies below a maximum value dependent on the surface tension of the organic component with respect of the fiber bed and on the difference in density and surface tension between the remaining liquid and the organic component.
摘要翻译： PCT No.PCT / EP90 / 00514 Sec。 371日期1991年10月17日 102（e）日期1991年10月17日PCT 1990年3月31日PCT公布。第WO90 / 11810号公报日本1990年10月18日。一种分散在主要是有机材料的液体中的至少一种液体有机成分的沉淀分离方法，该有机组分和剩余液体呈现密度差异。为了大大缩短停留时间，提出液体在沉降前通过纤维床，有机组分和剩余液体相对于纤维床具有不同的表面张力，液体的温度和要分离的有机组分的浓度使得在平衡状态下形成至少两个液相，并且通过纤维床的液体的流速低于取决于有机物的表面张力的最大值相对于纤维床的分量以及剩余液体和有机组分之间的密度和表面张力的差异。

2. 发明授权

US5514820A Continuous process for the production of lower alkyl esters 失效
标题翻译：用于生产低级烷基酯的连续方法
公开(公告)号：US5514820A
公开(公告)日：1996-05-07
申请号：US191746
申请日：1994-02-03
申请人： Georg Assmann , Gerhard Blasey , Bernhard Gutsche , Lutz Jeromin , Jean Rigal , Rene Armengaud , Bernard Cormary
发明人： Georg Assmann , Gerhard Blasey , Bernhard Gutsche , Lutz Jeromin , Jean Rigal , Rene Armengaud , Bernard Cormary
IPC分类号： B01J19/24 , C07C67/03 , C11C3/04
CPC分类号： B01J19/242 , C07C67/03 , B01J2219/00103 , B01J2219/00166 , B01J2219/00168 , B01J2219/00171
摘要： The invention relates to a continuous process for the production of lower alkyl esters at temperatures of up to 100.degree. C. and under pressures of up to 10 bar by reaction of fatty acid triglycerides containing less than 1% free fatty acid with a lower alcohol in two stages in the presence of a homogeneous alkaline catalyst, the glycerol formed being removed after the first stage. To enable the process to be carried out with high yields and with lower maintenance, investment and energy costs than in the prior art, the reaction mixture is passed through a reactor and a following static separator only once in each stage, tube reactors are used as the reactors and the Reynolds number of the flow of the reaction mixture is greater than 2,300.
摘要翻译：本发明涉及用于在高达100℃的温度和高达10巴的压力下生产低级烷基酯的连续方法，其通过使含有少于1％游离脂肪酸的脂肪酸甘油三酯与低级醇的反应在均相碱性催化剂存在的两个阶段，形成的甘油在第一阶段后被除去。为了使该方法能够以比现有技术高的产率和较低的维护，投资和能量成本进行，反应混合物在每个阶段仅通过反应器和静态分离器仅一次，管式反应器用作反应器和反应混合物流的雷诺数大于2,300。

3. 发明授权

US07064223B2 Method for producing technical oleic acid methyl esters 有权
标题翻译：油酸甲酯技术的生产方法
公开(公告)号：US07064223B2
公开(公告)日：2006-06-20
申请号：US10496989
申请日：2002-11-21
申请人： Stephan Heck , Volker Winterhoff , Bernhard Gutsche , Georg Fieg , Uwe Mueller , Jean Rigal , Thomas Kapala
发明人： Stephan Heck , Volker Winterhoff , Bernhard Gutsche , Georg Fieg , Uwe Mueller , Jean Rigal , Thomas Kapala
IPC分类号： C07C51/43
CPC分类号： C11C1/10 , C07C67/54 , C11B3/12 , C07C69/58
摘要： A process for making technical oleic acid methyl esters having a stearic acid methyl ester content of less than about 2% by weight, and a palmitic acid methyl ester content of less than about 5%, comprising: (a) providing a C8-18 palm kernel oil fatty acid methyl ester; (b) fractionally distilling said C8-18 palm kernel oil fatty acid methyl ester to form a C8-14 head product and a C16-18 bottom product; (c) fractionally distilling the C16-18 bottom product to form a short-chain C16 head product and a long-chain and unsaturated C18 bottom product; (d) fractionally distilling the long-chain and unsaturated C18 bottom product to form a predominantly unsaturated head product having a high palmitic acid methyl ester content and a predominantly unsaturated bottom product have a minimal palmitic acid methyl ester content; and (e) fractionally distilling the predominantly unsaturated bottom product have a minimal palmitic acid methyl ester content to form a head product rich in oleic acid methyl ester and poor in stearic acid methyl ester and a bottom product rich in both oleic acid methyl ester and stearic acid methyl ester.
摘要翻译：一种制备硬脂酸甲酯含量小于约2重量％，棕榈酸甲酯含量小于约5％的技术性油酸甲酯的方法，包括：（a）提供C 8-18棕榈仁油脂肪酸甲酯; （b）分馏蒸馏所述C 8-18 C棕榈仁油脂肪酸甲酯以形成C 8-14头孢菌素和C 16-18- / SUB>底部产品; （c）对C 16-18底部产物进行分馏，以形成短链C 16 C 16 C 16 C 16 F 16 C 16 C 14 C 14 C 14 C 14 C 14 C 14 C 14 H 16 Cl 2产物和长链和不饱和C 18 底部产品; （d）分级蒸馏长链和不饱和C 18 C 18底物以形成具有高棕榈酸甲酯含量的主要不饱和的头产物，并且主要不饱和的底部产物具有最小的棕榈酸甲酯内容; 和（e）分馏蒸馏主要不饱和的底部产物具有最小的棕榈酸甲酯含量以形成富含油酸甲酯的头部产物，并且在硬脂酸甲酯中较差，而富含油酸甲酯和硬脂酸的底部产物酸甲酯。

4. 发明申请

US20050090676A1 Method for producing technical oleic acid methyl esters 有权
标题翻译：油酸甲酯技术的生产方法
公开(公告)号：US20050090676A1
公开(公告)日：2005-04-28
申请号：US10496989
申请日：2002-11-21
申请人： Stephan Heck , Volker Winterhoff , Bernhard Gutsche , Georg Fieg , Uwe Mueller , Jean Rigal , Thomas Kapala
发明人： Stephan Heck , Volker Winterhoff , Bernhard Gutsche , Georg Fieg , Uwe Mueller , Jean Rigal , Thomas Kapala
IPC分类号： C07C67/54 , C07C69/58 , C11B3/12 , C11B11/00 , C11C1/10 , C07C51/43
CPC分类号： C11C1/10 , C07C67/54 , C11B3/12 , C07C69/58
摘要： A process for making technical oleic acid methyl esters having a stearic acid methyl ester content of less than about 2% by weight, and a palmitic acid methyl ester content of less than about 5%, comprising: (a) providing a C8-18 palm kernel oil fatty acid methyl ester; (b) fractionally distilling said C8-18 palm kernel oil fatty acid methyl ester to form a C8-14 head product and a C16-18 bottom product; (c) fractionally distilling the C16-18 bottom product to form a short-chain C16 head product and a long-chain and unsaturated C18 bottom product; (d) fractionally distilling the long-chain and unsaturated C18 bottom product to form a predominantly unsaturated head product having a high palmitic acid methyl ester content and a predominantly unsaturated bottom product have a minimal palmitic acid methyl ester content; and (e) fractionally distilling the predominantly unsaturated bottom product have a minimal palmitic acid methyl ester content to form a head product rich in oleic acid methyl ester and poor in stearic acid methyl ester and a bottom product rich in both oleic acid methyl ester and stearic acid methyl ester.
摘要翻译：一种制备硬脂酸甲酯含量小于约2重量％，棕榈酸甲酯含量小于约5％的技术性油酸甲酯的方法，包括：（a）提供C 8-18棕榈仁油脂肪酸甲酯; （b）分馏蒸馏所述C 8-18 C棕榈仁油脂肪酸甲酯以形成C 8-14头孢菌素和C 16-18- / SUB>底部产品; （c）对C 16-18底部产物进行分馏，以形成短链C 16 C 16 C 16 C 16 F 16 C 16 C 14 C 14 C 14 C 14 C 14 C 14 C 14 H 16 Cl 2产物和长链和不饱和C 18 底部产品; （d）分级蒸馏长链和不饱和C 18 C 18底物以形成具有高棕榈酸甲酯含量的主要不饱和的头产物，并且主要不饱和的底部产物具有最小的棕榈酸甲酯内容; 和（e）分馏蒸馏主要不饱和的底部产物具有最小的棕榈酸甲酯含量以形成富含油酸甲酯的头部产物，并且在硬脂酸甲酯中较差，而富含油酸甲酯和硬脂酸的底部产物酸甲酯。

5. 发明申请

US20080033191A1 Process for producing glycerol having low aldehyde and ketone content and improved storage stability 审中-公开
标题翻译：具有低醛和酮含量的甘油的生产方法和储存稳定性得到改善
公开(公告)号：US20080033191A1
公开(公告)日：2008-02-07
申请号：US11880928
申请日：2007-07-25
申请人： Ulrich Schoerken , David Melchior , Jochen Seifert , Carolin Meyer , Valerie Eychenne , Christiane Richard-Elsner , Horst Josten , Jean Rigal , Bernhard Gutsche , Albert Strube
发明人： Ulrich Schoerken , David Melchior , Jochen Seifert , Carolin Meyer , Valerie Eychenne , Christiane Richard-Elsner , Horst Josten , Jean Rigal , Bernhard Gutsche , Albert Strube
IPC分类号： C07C51/00
CPC分类号： C07C29/88 , A61K47/10 , C07C31/225
摘要： The invention describes a process for the production of glycerol of providing a vegetable oil or fat as starting material, obtaining crude glycerol from the vegetable oil or fat, and treating the crude glycerol with a reducing agent. The present invention also describes a process for the production of a medicament or pharmaceutical composition, the medicament or composition formed by combining glycerol and at least one pharmaceutically active ingredient. The present invention also describes a pharmaceutical composition or medicament composed of glycerol obtained by way of the invention and a pharmaceutically active ingredient, which compositions forms very little glyceraldehyde and dihydroxyacetone during storage.
摘要翻译：本发明描述了一种生产以植物油或脂肪为原料的甘油的制备方法，从植物油或脂肪中获得粗甘油，并用还原剂处理粗甘油。本发明还描述了制备药物或药物组合物的方法，所述药物或组合物通过将甘油与至少一种药物活性成分组合而形成。本发明还描述了由通过本发明获得的甘油和药物活性成分组成的药物组合物或药物，该组合物在储存期间形成非常少的甘油醛和二羟基丙酮。

6. 发明授权

US06911164B2 Spherical sterol preparations, their production and their use 失效
标题翻译：球形固醇制剂，其制备及其用途
公开(公告)号：US06911164B2
公开(公告)日：2005-06-28
申请号：US10259684
申请日：2002-09-27
申请人： Gerhard Wollmann , Bernhard Gutsche , Wolfgang Albiez , Jean Rigal , Yannik Basso
发明人： Gerhard Wollmann , Bernhard Gutsche , Wolfgang Albiez , Jean Rigal , Yannik Basso
IPC分类号： A23D9/007 , A23L1/30 , B01J2/02 , B01J2/04 , C11B15/00 , B29B9/10
CPC分类号： A23D9/007 , A23L33/11 , B01J2/02 , B01J2/04 , C11B15/00
摘要： A process for making spherically-shaped sterol preparations involving: (a) providing a liquid sterol preparation; (b) forming the liquid sterol preparation into liquid sterol droplets; and (c) solidifying the liquid sterol droplets to form the spherically-shaped sterol preparations.
摘要翻译：制备球形甾醇制剂的方法，包括：（a）提供液体甾醇制剂; （b）将液体甾醇制剂形成液体甾醇液滴; 和（c）固化液体甾醇液滴以形成球形甾醇制剂。

7. 发明授权

US3946892A Double wall vessel 失效
标题翻译：双层瓦楞纸箱
公开(公告)号：US3946892A
公开(公告)日：1976-03-30
申请号：US225773
申请日：1972-02-14
申请人： Jean Rigal , Jacques Troton
发明人： Jean Rigal , Jacques Troton
IPC分类号： B01J19/00 , B65D90/02 , E04C2/36 , B32B3/12 , B65D25/00 , B65D25/18
CPC分类号： B01J19/0053 , B65D90/028 , E04C2/365 , B01J2219/00186 , B01J2219/002 , Y10S220/917 , Y10S220/918 , Y10T428/24149 , Y10T428/24182
摘要： A double-walled vessel wherein a grid is located between the walls to provide a support for the inner wall, the grid being made up of strips which are on edge and which define interconnected cells for passage of a fluid between the walls.

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