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1. 发明授权

US07064223B2 Method for producing technical oleic acid methyl esters 有权
标题翻译：油酸甲酯技术的生产方法
公开(公告)号：US07064223B2
公开(公告)日：2006-06-20
申请号：US10496989
申请日：2002-11-21
申请人： Stephan Heck , Volker Winterhoff , Bernhard Gutsche , Georg Fieg , Uwe Mueller , Jean Rigal , Thomas Kapala
发明人： Stephan Heck , Volker Winterhoff , Bernhard Gutsche , Georg Fieg , Uwe Mueller , Jean Rigal , Thomas Kapala
IPC分类号： C07C51/43
CPC分类号： C11C1/10 , C07C67/54 , C11B3/12 , C07C69/58
摘要： A process for making technical oleic acid methyl esters having a stearic acid methyl ester content of less than about 2% by weight, and a palmitic acid methyl ester content of less than about 5%, comprising: (a) providing a C8-18 palm kernel oil fatty acid methyl ester; (b) fractionally distilling said C8-18 palm kernel oil fatty acid methyl ester to form a C8-14 head product and a C16-18 bottom product; (c) fractionally distilling the C16-18 bottom product to form a short-chain C16 head product and a long-chain and unsaturated C18 bottom product; (d) fractionally distilling the long-chain and unsaturated C18 bottom product to form a predominantly unsaturated head product having a high palmitic acid methyl ester content and a predominantly unsaturated bottom product have a minimal palmitic acid methyl ester content; and (e) fractionally distilling the predominantly unsaturated bottom product have a minimal palmitic acid methyl ester content to form a head product rich in oleic acid methyl ester and poor in stearic acid methyl ester and a bottom product rich in both oleic acid methyl ester and stearic acid methyl ester.
摘要翻译：一种制备硬脂酸甲酯含量小于约2重量％，棕榈酸甲酯含量小于约5％的技术性油酸甲酯的方法，包括：（a）提供C 8-18棕榈仁油脂肪酸甲酯; （b）分馏蒸馏所述C 8-18 C棕榈仁油脂肪酸甲酯以形成C 8-14头孢菌素和C 16-18- / SUB>底部产品; （c）对C 16-18底部产物进行分馏，以形成短链C 16 C 16 C 16 C 16 F 16 C 16 C 14 C 14 C 14 C 14 C 14 C 14 C 14 H 16 Cl 2产物和长链和不饱和C 18 底部产品; （d）分级蒸馏长链和不饱和C 18 C 18底物以形成具有高棕榈酸甲酯含量的主要不饱和的头产物，并且主要不饱和的底部产物具有最小的棕榈酸甲酯内容; 和（e）分馏蒸馏主要不饱和的底部产物具有最小的棕榈酸甲酯含量以形成富含油酸甲酯的头部产物，并且在硬脂酸甲酯中较差，而富含油酸甲酯和硬脂酸的底部产物酸甲酯。

2. 发明申请

US20050090676A1 Method for producing technical oleic acid methyl esters 有权
标题翻译：油酸甲酯技术的生产方法
公开(公告)号：US20050090676A1
公开(公告)日：2005-04-28
申请号：US10496989
申请日：2002-11-21
申请人： Stephan Heck , Volker Winterhoff , Bernhard Gutsche , Georg Fieg , Uwe Mueller , Jean Rigal , Thomas Kapala
发明人： Stephan Heck , Volker Winterhoff , Bernhard Gutsche , Georg Fieg , Uwe Mueller , Jean Rigal , Thomas Kapala
IPC分类号： C07C67/54 , C07C69/58 , C11B3/12 , C11B11/00 , C11C1/10 , C07C51/43
CPC分类号： C11C1/10 , C07C67/54 , C11B3/12 , C07C69/58
摘要： A process for making technical oleic acid methyl esters having a stearic acid methyl ester content of less than about 2% by weight, and a palmitic acid methyl ester content of less than about 5%, comprising: (a) providing a C8-18 palm kernel oil fatty acid methyl ester; (b) fractionally distilling said C8-18 palm kernel oil fatty acid methyl ester to form a C8-14 head product and a C16-18 bottom product; (c) fractionally distilling the C16-18 bottom product to form a short-chain C16 head product and a long-chain and unsaturated C18 bottom product; (d) fractionally distilling the long-chain and unsaturated C18 bottom product to form a predominantly unsaturated head product having a high palmitic acid methyl ester content and a predominantly unsaturated bottom product have a minimal palmitic acid methyl ester content; and (e) fractionally distilling the predominantly unsaturated bottom product have a minimal palmitic acid methyl ester content to form a head product rich in oleic acid methyl ester and poor in stearic acid methyl ester and a bottom product rich in both oleic acid methyl ester and stearic acid methyl ester.
摘要翻译：一种制备硬脂酸甲酯含量小于约2重量％，棕榈酸甲酯含量小于约5％的技术性油酸甲酯的方法，包括：（a）提供C 8-18棕榈仁油脂肪酸甲酯; （b）分馏蒸馏所述C 8-18 C棕榈仁油脂肪酸甲酯以形成C 8-14头孢菌素和C 16-18- / SUB>底部产品; （c）对C 16-18底部产物进行分馏，以形成短链C 16 C 16 C 16 C 16 F 16 C 16 C 14 C 14 C 14 C 14 C 14 C 14 C 14 H 16 Cl 2产物和长链和不饱和C 18 底部产品; （d）分级蒸馏长链和不饱和C 18 C 18底物以形成具有高棕榈酸甲酯含量的主要不饱和的头产物，并且主要不饱和的底部产物具有最小的棕榈酸甲酯内容; 和（e）分馏蒸馏主要不饱和的底部产物具有最小的棕榈酸甲酯含量以形成富含油酸甲酯的头部产物，并且在硬脂酸甲酯中较差，而富含油酸甲酯和硬脂酸的底部产物酸甲酯。

3. 发明授权

US07449088B2 Process for obtaining fatty acids with improved odor, color and heat stability 有权
标题翻译：获得具有改善气味，颜色和热稳定性的脂肪酸的方法
公开(公告)号：US07449088B2
公开(公告)日：2008-11-11
申请号：US11095364
申请日：2005-03-31
申请人： Nataly Lausberg , Horst Josten , Georg Fieg , Thomas Kapala , Ralf Christoph , Andreas Suessenbach , Andreas Heidbreder , Ingomar Mrozek , Albrecht Schwerin
发明人： Nataly Lausberg , Horst Josten , Georg Fieg , Thomas Kapala , Ralf Christoph , Andreas Suessenbach , Andreas Heidbreder , Ingomar Mrozek , Albrecht Schwerin
IPC分类号： B01D3/14 , B01D3/38 , C11B3/12 , C11B3/14 , B01D3/42
CPC分类号： C11C1/10 , C11C1/106 , Y10S203/20
摘要： The present invention relates to a new process for obtaining fatty acids with improved color, odor and heat stability which is characterized in that: (a) in a first step the crude acids are fed to a rectification (“precut”) column in order to remove low boiling by-products being present in the starting material as a top fraction, and (b) in a second step the bottom fraction of the precut column is fed to a sidestream column in order to obtain the pure fatty acids as the side fraction, to remove low boiling by-products which have been formed in the course of the first distillation as a top fraction and to remove high boiling by-products, either being present from the starting material or formed during the first distillation, with the residue.
摘要翻译：本发明涉及一种获得具有改善的颜色，气味和热稳定性的脂肪酸的新方法，其特征在于：（a）在第一步中，将粗酸加入到精馏（“预制”）柱中，以便除去起始原料中存在的低沸点副产物作为顶馏分，和（b）在第二步中，将预切塔的塔底部分进料到侧流塔中，以获得作为副馏分的纯脂肪酸以除去在第一蒸馏过程中形成的低沸点副产物作为顶级馏分，并除去原料存在或在第一蒸馏期间形成的高沸点副产物与残余物。

4. 发明申请

US20070060763A1 PROCESS FOR WORKING UP FATTY COMPOUNDS 审中-公开
标题翻译：加工脂肪化合物的方法
公开(公告)号：US20070060763A1
公开(公告)日：2007-03-15
申请号：US11463396
申请日：2006-08-09
申请人： Stefan Franzen , Thomas Kapala , Eike Ulf Mahnke , Yiwen Dong
发明人： Stefan Franzen , Thomas Kapala , Eike Ulf Mahnke , Yiwen Dong
IPC分类号： C07C51/43
CPC分类号： C11C3/00 , C11B3/06 , C11B3/10 , C11C1/08
摘要： The invention relates to a process for working up fatty compounds from esterification and transesterification reactions, wherein, the fatty compounds are contacted with ion exchangers to remove unwanted constituents.
摘要翻译：本发明涉及一种通过酯化和酯交换反应处理脂肪化合物的方法，其中脂肪化合物与离子交换剂接触以除去不需要的成分。

5. 发明申请

US20060090995A1 System and method for carrying out a discontinuous rectification or reaction 审中-公开
标题翻译：进行不连续整流或反应的系统和方法
公开(公告)号：US20060090995A1
公开(公告)日：2006-05-04
申请号：US10526956
申请日：2003-08-29
申请人： Georg Fieg , Thomas Kapala
发明人： Georg Fieg , Thomas Kapala
IPC分类号： B01D3/34
CPC分类号： B01D3/322 , B01D3/008 , B01D3/009 , B01D3/14 , B01D3/4205 , B01D3/4238 , B01J19/0006 , B01J2219/00101
摘要： The invention is an apparatus and process for batch rectification or reaction with batch distillation. The apparatus is a rectifying column alone or mounted on a batch reactor. The rectifying column having a collector for the downflowing column liquid arranged to collect liquid flowing down the column and a valve arrangement to direct the flow selectively away from the column or to the column at a time when downflowing product is being removed from the column. The column is operated at total reflux until the product reaches a required purity then the liquid flow from the collector is directed away from the column and the product recovered.
摘要翻译：本发明是用于间歇式精馏或与分批蒸馏反应的装置和方法。该装置是单独的精馏塔或安装在间歇式反应器上。精馏塔具有用于向下流动的柱状液体的收集器，用于收集沿柱流动的液体，以及阀装置，用于在从塔中取出下流产品时，选择性地将流量从塔或塔排出。该柱在完全回流下运行，直到产物达到所需的纯度，然后将来自收集器的液体流引导离开塔并回收产物。

6. 发明申请

US20060006056A1 Process for obtaining fatty acids with improved odor, color and heat stability 有权
标题翻译：获得具有改善气味，颜色和热稳定性的脂肪酸的方法
公开(公告)号：US20060006056A1
公开(公告)日：2006-01-12
申请号：US11095364
申请日：2005-03-31
申请人： Nataly Lausberg , Horst Josten , Georg Fieg , Thomas Kapala , Ralf Christoph , Andreas Suessenbach , Andreas Heidbreder , Ingomar Mrozek , Albrecht Schwerin
发明人： Nataly Lausberg , Horst Josten , Georg Fieg , Thomas Kapala , Ralf Christoph , Andreas Suessenbach , Andreas Heidbreder , Ingomar Mrozek , Albrecht Schwerin
IPC分类号： B01D3/10
CPC分类号： C11C1/10 , C11C1/106 , Y10S203/20
摘要： Disclosed is a new process for obtaining fatty acids with improved color, odor and heat stability which is characterized in that (a) in a first step the crude acids are fed to a rectification (“precut”) column in order to remove low boiling by-products being present in the starting material as a top fraction, and (b) in a second step the bottom fraction of the precut column is fed to a sidestream column in order to obtain the pure fatty acids as the side fraction, to remove low boiling by-products which have been formed in the course of the first distillation as a top fraction and to remove high boiling by-products, either being present from the starting material or formed during the first distillation, with the residue.
摘要翻译：公开了一种获得具有改善的颜色，气味和热稳定性的脂肪酸的新方法，其特征在于：（a）在第一步中，将粗酸加入到精馏（“预制”）柱中，以通过 - 作为顶级馏分存在于起始原料中的产物，和（b）在第二步中，将预切塔的塔底部分进料到侧流塔中以获得作为副馏分的纯脂肪酸，以除去低在第一蒸馏过程中形成的沸腾副产物作为顶级馏分，并且从原料中存在或在第一次蒸馏期间形成的高沸点副产物与残余物一起除去。

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