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    • 1. 发明授权
    • Method and apparatus for reducing band broadening in chromatographic
detectors
    • 用于降低色谱检测器中带宽变宽的方法和装置
    • US5676830A
    • 1997-10-14
    • US632035
    • 1996-04-12
    • Gary R. JanikDouglas W. Shepard
    • Gary R. JanikDouglas W. Shepard
    • G01N30/74B01D15/08
    • G01N30/74
    • A capillary tube used to transfer a liquid sample into a detection cell following separation by a chromatographic system is modified by plugging or otherwise severely restricting its flow. Near its plugged end, said tube is drilled to provide a plurality of holes or ports perpendicular thereto and penetrating into the central flowing core of said tube so as to direct outflow from the tube perpendicularly therefrom. The outer diameter of this so-modified capillary tube is selected to be of a size comparable to, though smaller than, the detection cell diameter into which it transfers the flowing sample. In this manner, fluid transferred into a detection cell by said modified capillary tube will be split into a plurality of smaller streams flowing outwardly therefrom and striking the adjacent detector cell walls almost immediately. Because of the close proximity of the emerging split streams to the walls of the detection cell, the eddies produced thereby will be very small and the contents of the detection cell will be homogenized rapidly.
    • 用于在通过色谱系统分离后将液体样品转移到检测单元中的毛细管通过堵塞或以其他方式严格限制其流动来改变。 在其堵塞端附近,所述管被钻孔以提供与其垂直的多个孔或孔,并且穿透到所述管的中心流动的芯中,以便从管垂直地引导从管垂直流出。 该经修改的毛细管的外径被选择为与其传送流动样品的检测池直径相当的尺寸。 以这种方式,通过所述改进的毛细管转移到检测单元中的流体将被分成多个从其向外流动的较小流,并几乎立即撞击相邻的检测器单元壁。 由于新出现的分流与检测单元的壁的紧密接近,因此产生的涡流将非常小,并且检测单元的内容物将迅速均匀化。
    • 2. 发明授权
    • Extended range interferometric refractometer
    • 扩展距离干涉折射计
    • US6128080A
    • 2000-10-03
    • US870937
    • 1997-06-06
    • Gary R. JanikDouglas W. ShepardSteven P. TrainoffDavid T. Phillips
    • Gary R. JanikDouglas W. ShepardSteven P. TrainoffDavid T. Phillips
    • G01N21/45G01B9/02
    • G01N21/45
    • A method and apparatus is disclosed for measuring the refractive index difference between a reference and sample liquid based on an interferometric design. The resultant device has an almost unlimited range of operation in contrast to a conventional interferometric refractometer of the so-called polarization type whose dynamic range is restricted to a relatively narrow range of refractive indices. The measurement of the refractive index difference between a sample and reference cell is achieved by measuring the angle through which the plane of polarization of a combined beam has rotated. For the conventional device, this angle is restricted to about .pi. radians which corresponds to a half wavelength shift between the reference and sample components of said combined beam. The extended range device disclosed permits this angle to be tracked and measured accurately over many rotations. The rotation tracking is achieved by one of three embodiments, the preferred of which involves the use of a liquid crystal retarder. The other two techniques incorporate, respectively, a rotating polarizer and a doubly split beam. All three embodiments permit the measurement of both the sine and cosine of the rotation angle and, thereby, allows a four quadrant arctangent calculation to yield the rotation angle directly. The error associated with such measurements is not a function of the rotation angle of the combined beams.
    • 公开了一种用于基于干涉测量设计来测量参考和样品液体之间的折射率差的方法和装置。 与所谓的偏振型的常规干涉式折射计相反,所得到的装置具有几乎无限的操作范围,其中动态范围被限制在相对较窄的折射率范围。 通过测量组合光束的偏振平面旋转的角度来实现样品和参考单元之间的折射率差的测量。 对于常规装置,该角度限于对应于所述组合光束的参考和样本分量之间的半波长偏移的约π弧度。 所公开的扩展范围装置允许在许多旋转中精确地跟踪和测量该角度。 旋转跟踪由三个实施例中的一个实现,其中优选涉及使用液晶延迟器。 其他两种技术分别包括旋转偏振器和双分束。 所有三个实施例允许测量旋转角度的正弦和余弦两者,从而允许四象限反正切计算直接产生旋转角度。 与这种测量相关联的误差不是组合光束的旋转角度的函数。
    • 3. 发明授权
    • Apparatus to reduce inhomogeneities in optical flow cells
    • 降低光流细胞不均匀性的装置
    • US5900152A
    • 1999-05-04
    • US854442
    • 1997-05-12
    • Gary R. JanikDouglas W. ShepardSteven T. Monser
    • Gary R. JanikDouglas W. ShepardSteven T. Monser
    • G01N30/74B01D15/08
    • G01N30/74
    • A capillary tube used to transfer a liquid sample into a detection cell following separation by a chromatographic system is modified by plugging or otherwise severely restricting its flow. Near its plugged end, said tube is drilled to provide a plurality of holes or ports perpendicular thereto and penetrating to the central flowing core of said tube so as to direct outflow from the tube perpendicularly therefrom. The outer diameter of this somodified capillary tube is selected to be of a size comparable to, though smaller than, the detection cell diameter into which it transfers the flowing sample. In this manner, fluid transferred into a detection cell by said modified capillary tube will be split into a plurality of smaller streams flowing outwardly therefrom and striking the adjacent detector cell walls almost immediately. Because of the close proximity of the emerging split streams to the walls of the detection cell, the eddies produced thereby will be very small and the contents of the detection cell will be homogenized rapidly.
    • 用于在通过色谱系统分离后将液体样品转移到检测单元中的毛细管通过堵塞或以其他方式严格限制其流动来改变。 在其堵塞端附近,所述管被钻孔以提供与其垂直的多个孔或孔,并穿透到所述管的中心流动芯,以便从管垂直地引导从管垂直流出。 该变细毛细管的外径被选择为与其传送流动样品的检测池直径相当的尺寸,尽管比其小。 以这种方式,通过所述改进的毛细管转移到检测单元中的流体将被分成多个从其向外流动的较小流,并几乎立即撞击相邻的检测器单元壁。 由于新出现的分流与检测单元的壁的紧密接近,因此产生的涡流将非常小,并且检测单元的内容物将迅速均匀化。
    • 4. 发明授权
    • Electrical measurements on semiconductors using corona and microwave techniques
    • 使用电晕和微波技术对半导体进行电气测量
    • US07521946B1
    • 2009-04-21
    • US11277934
    • 2006-03-29
    • Gary R. Janik
    • Gary R. Janik
    • G01R31/302
    • G01R31/2621G01R31/311
    • A corona-microwave system can generate accurate capacitance-voltage (C-V) and resistance-voltage (R-V) curves, thereby allowing the accurate determination of gate film capacitance, sheet resistance of implanted regions, and mobility of a substrate under a gate. The corona-microwave system can combine a corona deposition system, a Kelvin probe, and a microwave probe. The corona deposition system can deposit a corona charge on a surface of the semiconductor. The Kelvin and microwave probes can be used to make first and second electrical measurements of a layer/region of the semiconductor. The steps of charge deposition and probe measurements can be repeated to generate a curve plotting the first and second electrical measurements. Because the first and second electrical measurements can be accurately made, the extracted information from the curve is also accurate.
    • 电晕微波系统可以产生精确的电容电压(C-V)和电阻电压(R-V)曲线,从而允许精确确定栅极膜电容,注入区域的薄层电阻和栅极下的衬底的迁移率。 电晕微波系统可以组合电晕沉积系统,开尔文探针和微波探头。 电晕沉积系统可以在半导体的表面上沉积电晕电荷。 开尔文和微波探头可用于对半导体层/区域进行第一次和第二次电气测量。 可以重复电荷沉积和探针测量的步骤以产生绘制第一和第二电测量的曲线。 由于可以准确地进行第一和第二电测量,所以从曲线提取的信息也是准确的。
    • 5. 发明授权
    • Scatterometry metrology using inelastic scattering
    • 散射测量使用非弹性散射
    • US07433056B1
    • 2008-10-07
    • US11182171
    • 2005-07-15
    • Gary R. Janik
    • Gary R. Janik
    • G01B11/24G01B11/30G01B11/14G01J3/44G01J3/42G01J3/427G01J3/28
    • G01B11/0616G01N21/65G01N2021/653
    • A system for characterizing material properties in miniature semiconductor structures performs a scatterometry analysis on inelastically scattered light. The system can include a narrowband probe beam generator and a detector. A single wavelength probe beam from the narrowband probe beam generator produces scattered light from a measurement pattern on a test sample. The scattered light is measured by the detector, and the measurement data (e.g., Raman spectrum) is used in a scatterometry analysis to determine material properties for the measurement pattern. The detector can measure either incoherent inelastically scattered light (e.g., using a spectrometer) or coherent inelastically scattered light (e.g., using an array detector). If the measurement pattern dimensions are substantially similar to actual device dimensions, the material property distributions determined for the measurement pattern can be applied to the actual devices on the test sample.
    • 用于表征微型半导体结构中的材料性质的系统对非弹性散射光进行散射分析。 该系统可以包括窄带探测光束发生器和检测器。 来自窄带探测光束发生器的单个波长探测光束从测试样品上的测量图形产生散射光。 通过检测器测量散射光,并且在散射分析中使用测量数据(例如,拉曼光谱)来确定测量图案的材料特性。 检测器可以测量非相干非弹性散射光(例如,使用光谱仪)或相干非弹性散射光(例如,使用阵列检测器)。 如果测量图形尺寸基本上类似于实际的装置尺寸,则可以将测量图案确定的材料特性分布应用于测试样品上的实际装置。
    • 6. 发明授权
    • X-ray imaging for patterned film measurement
    • 用于图案膜测量的X射线成像
    • US07166838B1
    • 2007-01-23
    • US11135974
    • 2005-05-23
    • Gary R. Janik
    • Gary R. Janik
    • G01N23/201
    • G01N23/04
    • An x-ray metrology system includes an e-beam generator to cause a test sample to emit x-rays, x-ray optics for focusing the x-rays, and an x-ray imager to generate an image of the test sample from the focused x-rays. Because the x-ray imager provides a direct representation of the x-ray emission characteristics of the test sample, the resolution of a measurement taken using such a sensor is limited only by the resolution of the sensor (and any focusing optics), rather than by the amount of e-beam spread in the thin film. The x-ray imaging can be performed for object planes at the test sample that are not parallel to the test sample, thereby allowing vertical dimension data to be accurately generated by the x-ray imaging system.
    • x射线测量系统包括电子束发生器,以使测试样品发射x射线,用于聚焦x射线的x射线光学元件和x射线成像仪,以从 聚焦x射线。 由于x射线成像仪提供了测试样品的x射线发射特性的直接表示,所以使用这种传感器进行测量的分辨率仅受传感器(和任何聚焦光学器件)的分辨率的限制,而不是 通过电子束在薄膜中的传播量。 可以对与测试样品不平行的测试样品的物体平面执行x射线成像,从而允许由x射线成像系统精确地产生垂直尺寸数据。
    • 8. 发明授权
    • Method and system for measuring deep trenches in silicon
    • 测量硅深沟的方法和系统
    • US07369235B1
    • 2008-05-06
    • US11165711
    • 2005-06-24
    • Gary R. JanikJohn Fielden
    • Gary R. JanikJohn Fielden
    • G01J4/00
    • G01J4/04G01B11/0641G01N21/211
    • A spectroscopic ellipsometry system directs a near infra-red (NIR) probe beam at a test sample to allow metrology to be performed on vertical structures within the test sample. Because silicon is relatively transparent to NIR light, structural information can be determined from the polarization effects produced by the test sample, in a manner similar to that used with IR spectroscopic ellipsometry systems. However, unlike IR light, which requires delicate and costly optical and measurement components (e.g., vibration-sensitive Fourier transform sensors), NIR light can be directed and detected using more robust and inexpensive components (e.g., array-based detectors), thereby making a NIR spectroscopic ellipsometry system much more affordable and usable than conventional IR spectroscopic ellipsometry systems.
    • 光谱椭圆测量系统在测试样品上引导近红外(NIR)探针光束,以便在测试样品内的垂直结构上进行测量。 因为硅对于NIR光是相对透明的,所以结构信息可以由与测试样品产生的极化效应以与用于IR光谱椭偏仪系统的方式类似的方式来确定。 然而,与需要精密和昂贵的光学和测量部件(例如,振动傅里叶变换传感器)的IR光不同,可以使用更稳健和便宜的部件(例如,基于阵列的检测器)来引导和检测NIR光,从而使 近红外光谱椭偏仪系统比常规IR光谱椭偏仪系统更加实惠和可用。
    • 10. 发明授权
    • Film measurement with interleaved laser cleaning
    • 电影测量与交错激光清洗
    • US07110113B1
    • 2006-09-19
    • US10616064
    • 2003-07-08
    • Gary R. JanikDan G. Georgesco
    • Gary R. JanikDan G. Georgesco
    • G01J4/00B08B7/00
    • G01N21/8422B08B7/0042G01N21/211G01N21/55G01N2021/213G01N2021/8438
    • A system for analyzing a thin film simultaneously applies a pulsed cleaning beam and a measurement beam to an analysis location on a test sample to enhance measurement accuracy. The pulsed cleaning beam prevents contaminant regrowth on the analysis location during the actual measurement. To minimize the effects of thermal transients from the pulsed cleaning beam on measurement data, cleaning pulses can be timed to fall between data samples. Alternatively, data sampling can be blocked during each cleaning operation (i.e., each cleaning pulse and subsequent cooldown period) or data levels can be clamped at measurement levels from just before the start of the cleaning operation for the duration of the cleaning operation. Alternatively, data samples taken during each cleaning operation can be discarded or replaced with data samples from just before the cleaning operation using post-processing techniques.
    • 用于分析薄膜的系统同时将脉冲清洁光束和测量光束施加到测试样品上的分析位置,以提高测量精度。 脉冲清洁光束可防止在实际测量过程中分析位置的污染物再生长。 为了最小化来自脉冲清洁光束的热瞬变对测量数据的影响,清洁脉冲可以定时地落在数据样本之间。 或者,在清洁操作期间,可以在每次清洁操作期间(即,每个清洁脉冲和随后的冷却期间)阻止数据采样,或者可以在清洁操作开始之前的测量水平将数据水平钳位。 或者,可以在使用后处理技术的清洁操作之前的数据样本中丢弃或替换在每个清洁操作期间采集的数据样本。