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1. 发明授权

US4670309A Method for providing anti-weathering resistance to the surface of organic materials 失效
标题翻译：为有机材料表面提供耐候性的方法
公开(公告)号：US4670309A
公开(公告)日：1987-06-02
申请号：US882018
申请日：1986-07-03
申请人： Fumio Okada , Toshio Oba , Morizo Nakazato
发明人： Fumio Okada , Toshio Oba , Morizo Nakazato
IPC分类号： B05D5/00 , B05D7/08 , B05D7/12 , C08G77/04 , C08J7/04 , C09D183/04 , C09K3/00 , C09K3/18 , B05D3/02
CPC分类号： C08J7/047 , C08G77/04 , B05D2201/00 , B05D2203/24 , B05D7/12 , C08J2483/00
摘要： The invention provides a method for protecting the surface of various kinds of shaped articles made of an organic polymeric material such as rubbers, leathers, woods, plastics and the like against weathering caused by exposure to ultraviolet light, ozone, moisture, etc. The method comprises providing the surface with a coating layer of a specific organopolysiloxane composed of difunctional, tetrafunctional and nonofunctional siloxane units in a limited molar proportion of 50-85%, 10-30% and 5-20%, respectively.
摘要翻译：本发明提供一种保护由有机聚合材料如橡胶，皮革，木材，塑料等制成的各种成型制品的表面的方法，以防止由于暴露于紫外线，臭氧，水分等引起的风化。包括为表面提供由分别为50-85％，10-30％和5-20％的有限摩尔比例的由双功能，四官能和非官能的硅氧烷单元组成的特定有机聚硅氧烷的涂层。

2. 发明授权

US4617335A Method for improving mold releasability of a polymeric material 失效
标题翻译：提高聚合物材料脱模性的方法
公开(公告)号：US4617335A
公开(公告)日：1986-10-14
申请号：US758149
申请日：1985-07-23
申请人： Fumio Okada , Toshio Oba , Morizo Nakazato , Kenichi Isobe
发明人： Fumio Okada , Toshio Oba , Morizo Nakazato , Kenichi Isobe
IPC分类号： C08L101/00 , C08G18/61 , C08G18/62 , C08G77/00 , C08G77/04 , C08G77/14 , C08G77/22 , C08K5/5415 , C08L7/00 , C08L21/00 , C08K5/24
CPC分类号： C08K5/5415
摘要： The invention provides an efficient method for releasing a shaped body of a polymeric material such as a foamed polyurethane resin from a mold in which the body has been molded without the problem of adhesion to the mold. The inventive method comprises admixing the polymeric material with a specific organopolysiloxane represented by the structural formulaR.sup.1.sub.3 Si--O--SiR.sup.2.sub.2 --O).sub.m (SiR.sup.2 A--O).sub.n SiR.sup.1.sub.3,in which A is a substituent group represented by the general formula --C.sub.x H.sub.2x --O--R, R being a monovalent hydrocarbon group having 8 to 30 carbon atoms but free from terminal unsaturation and x being zero or a positive integer not exceeding 4, R.sup.1 is a monovalent hydrocarbon group or the same group as A, R.sup.2 is a hydrogen atom or the same group as R.sup.1, and m and n are each zero or a positive integer with the proviso that at least one group denoted by A is contained in a molecule of the organopolysiloxane.
摘要翻译：本发明提供了一种用于从模具中释放聚合物材料如发泡聚氨酯树脂的成形体的有效方法，其中已经模制了本体，而没有粘附到模具的问题。本发明的方法包括将聚合物材料与由结构式R 13 Si-O-SiR 22 -O）m（SiR 2 A-O）n SiR 13表示的特定有机聚硅氧烷混合，其中A是由通式-C x H 2 x -OR表示的取代基， R为碳原子数为8〜30，不含末端不饱和单价烃基，x为零或不超过4的正整数，R1为单价烃基或与A相同的基团，R2为氢原子或相同基团为R 1，m和n各自为零或正整数，条件是由A表示的至少一个基团包含在有机聚硅氧烷的分子中。

3. 发明授权

US4496687A Aqueous emulsion-type silicone compositions 失效
标题翻译：水性乳液型有机硅组合物
公开(公告)号：US4496687A
公开(公告)日：1985-01-29
申请号：US574669
申请日：1984-01-27
申请人： Fumio Okada , Toshio Oba , Morizo Nakazato
发明人： Fumio Okada , Toshio Oba , Morizo Nakazato
IPC分类号： C08L83/06 , C08J3/03 , C08K13/02 , C08L83/00 , C08L83/04 , C09D183/04 , D06M15/643 , C08L83/02
CPC分类号： C08J3/03 , C08K13/02 , C08K3/36 , C08K5/09 , C08K5/54 , C08G77/16 , C08J2383/04 , Y10S528/901
摘要： The invention provides a novel organopolysiloxane-containing aqueous emulsion composition which, upon removal of water by drying at room temperature, can give a cured rubbery elastomer having excellent mechanical properties and exhibiting strong adhesion to the substrate on which it has been cured. The inventive composition is prepared by blending (A) an aqueous emulsion of an organopolysiloxane having silicon-bonded hydroxy groups and emulsified in water by use of an anionic surface active agent, (B) a mixture of a reaction product of a carboxylic acid anhydride with an amino-functional organosilane and a colloidal silica in the form of an aqueous suspension and (C) a curing catalyst in limited proportions.
摘要翻译：本发明提供了一种新型的含有机聚硅氧烷的水性乳液组合物，其在室温下干燥除去水后，可得到具有优异的机械性能并对其已经固化的基材具有强粘合性的固化的橡胶弹性体。本发明的组合物通过将（A）具有硅键合的羟基的有机聚硅氧烷的水性乳液与阴离子表面活性剂共混而制备，（B）将羧酸酐的反应产物与氨基官能的有机硅烷和水性悬浮液形式的胶体二氧化硅，（C）有限比例的固化催化剂。

4. 发明授权

US4678688A Method for forming a surface film of cured organosilicon polymer on a substrate surface 失效
标题翻译：在基材表面上形成固化的有机硅聚合物的表面膜的方法
公开(公告)号：US4678688A
公开(公告)日：1987-07-07
申请号：US834906
申请日：1986-02-28
申请人： Kunio Itoh , Shohei Kozakai , Yoshinori Hida , Hiroshige Okinoshima , Fumio Okada , Toshio Oba , Hisashi Shimizu , Yuji Hinoto , Hiroshi Yoshioka
发明人： Kunio Itoh , Shohei Kozakai , Yoshinori Hida , Hiroshige Okinoshima , Fumio Okada , Toshio Oba , Hisashi Shimizu , Yuji Hinoto , Hiroshi Yoshioka
IPC分类号： C08G77/54 , C09D183/14 , B05D3/02
CPC分类号： C08J7/047 , C08G77/54 , C09D183/14 , C08J2483/00
摘要： The inventive method for forming a cured film on a substrate surface comprises coating the surface with a room temperature curable organosiloxazane polymer comprising, in a molecule, (a) at least one organosiloxane unit represented by the unit formula (a) at least one organosiloxane unit represented by the unit formulaR.sup.1.sub.a SiO.sub.(4-a)/2,and (b) at least one organosilazane unit represented by the unit formulaR.sup.2.sub.b Si(NR.sup.3).sub.(4-b)/2,in which R.sup.1, R.sup.2 and R.sup.3 are each a hydrogen atom or a substituted or unsubstituted monovalent hydrocarbon group, not all of them being simultaneously hydrogen atoms, and the subscripts a and b are each a positive integer of 1, 2 or 3 with the proviso that a and b cannot be simultaneously equal to 3, in a molecule and subjecting the coating film to exposure to a moisture-containing atmosphere. The method is useful for forming a surface-protecting film or for imparting surface releasability.
摘要翻译：用于在基材表面上形成固化膜的本发明方法包括用室温可固化的有机硅氮烷聚合物涂覆表面，所述室温可固化的有机硅氮烷聚合物在分子中包含（a）至少一个由式（a）表示的有机硅氧烷单元，至少一个有机硅氧烷单元由式R1aSiO（4-a）/ 2表示的至少一种有机硅氮烷单元，（b）由单元式R2bSi（NR3）（4-b）/ 2表示的至少一种有机硅氮烷单元，其中R1，R2和R3各自为氢原子或取代或未取代的一价烃基，并不全部同时为氢原子，下标a和b各自为正整数1,2或3，条件是a和b不能同时为3 在分子中并使涂膜暴露于含水气氛。该方法可用于形成表面保护膜或赋予表面剥离性。

5. 发明授权

US4814376A Process for preparing organopolysiloxane emulsion 失效
标题翻译：制备有机聚硅氧烷乳液的方法
公开(公告)号：US4814376A
公开(公告)日：1989-03-21
申请号：US119568
申请日：1987-11-12
申请人： Masaki Tanaka , Fumio Okada , Toshio Oba , Hiroshi Oohashi , Tatuo Tanaka
发明人： Masaki Tanaka , Fumio Okada , Toshio Oba , Hiroshi Oohashi , Tatuo Tanaka
IPC分类号： C08L83/04 , B01F3/08 , B01F7/00 , B01F7/16 , C08J3/03 , C08L83/07 , C08L75/00
CPC分类号： C08J3/03 , B01F3/0807 , B01F3/0853 , B01F7/1665 , B01F7/00 , C08J2383/04 , Y10S516/922 , Y10S516/93
摘要： A process for preparing organopolysiloxane emulsion comprised of dispersed particles having an average particle size of 0.5.mu. or less, comprising emulsifying a liquid organopolysiloxane with use of an emulsifying agent by means of a composite emulsifying apparatus equipped with(A) a stirring means having a stirring blade capable of stirring contents of a container at a low speed over the whole of the container, and at least one stirring means selected from(B) a disc type stirring means capable of rotating at a high speed and having tooth-like projections on its peripheral edge, and(C) a stirring means having a stator and a turbine blade disposed in the inside of the stator and capable of rotating at a high speed. According to this process, an organopolysiloxane having a high viscosity up to 500,000 cP can be emulsified to prepare an emulsion of high stability.
摘要翻译：一种制备有机聚硅氧烷乳液的方法，该乳液由平均粒度为0.5μm以下的分散颗粒组成，包括使用乳化剂乳化液体有机聚硅氧烷，该复合乳化装置配备有（A）搅拌装置，刀片能够在整个容器内以低速搅拌容器的内容物，以及至少一个搅拌装置，其选自（B）能够高速旋转并且在其上具有齿状突起的盘式搅拌装置周边，（C）具有定子和设置在定子内部并能够高速旋转的涡轮叶片的搅拌装置。根据该方法，可以将具有高达500,000cP的高粘度的有机聚硅氧烷乳化以制备高稳定性的乳液。

6. 发明授权

US4690986A Impact-resistant thermoplastic polyorganosiloxane-based graft copolymer and process for producing same 失效
标题翻译：耐冲击热塑性聚有机硅氧烷基接枝共聚物及其制备方法
公开(公告)号：US4690986A
公开(公告)日：1987-09-01
申请号：US904463
申请日：1986-09-08
申请人： Isao Sasaki , Akira Yanagase , Yasunori Kawachi , Tetsuya Mayuzumi , Toshio Oba , Fumio Okada
发明人： Isao Sasaki , Akira Yanagase , Yasunori Kawachi , Tetsuya Mayuzumi , Toshio Oba , Fumio Okada
IPC分类号： C08F30/00 , C08F30/08 , C08F283/00 , C08F283/12 , C08F290/00 , C08F299/08 , C09D151/08
CPC分类号： C08F283/124 , C09D151/085
摘要： A polyorganosiloxane-based high-impact thermoplastic graft copolymer superior in impact resistance, light resistance, surface gloss and color fastness produced by the emulsion graft polymerization of at least one vinyl monomer on an emulsion-polymerized polyorganosiloxane which consists of90 to 99.8 mole % of an organosiloxane unit represented by the formulaR'.sub.2 SiO.sub.2/2 (I) wherein R' is the same or different and denotes methyl, ethyl, propyl, or phenyl,0.1 to 10 mole % of a unit derived from a graft-linking agent, said unit being represented by the formula ##STR1## wherein; R.sup.2 denotes methyl, ethyl, propyl, or phenyl; n denotes a number of 0, 1, and 2; and p denotes a number of 1 to 6, and0.1 to 10 mole % of a unit derived from a tetrafunctional silane crosslinking agent, said unit being represented by the formulaSiO.sub.4/2 (III),said polyorganosiloxane showing a degree of swelling of 5 to 15 in toluene, andsaid graft copolymer containing said polyorganosiloxane in an amount of 10 to 70% by weight; and a process for producing the said graft copolymer.
摘要翻译：通过在乳液聚合的聚有机硅氧烷上由至少一种乙烯基单体的乳液接枝聚合产生的抗冲击性，耐光性，表面光泽和色牢度优异的基于聚有机硅氧烷的高冲击热塑性接枝共聚物，其由90-99.8摩尔％由式R'2SiO2 / 2（I）表示的有机硅氧烷单元，其中R'相同或不同，表示甲基，乙基，丙基或苯基，0.1-10摩尔％衍生自接枝交联剂的单元，所述单元由式（II）表示，其中： R2表示甲基，乙基，丙基或苯基; n表示0，1和2的数; p表示1〜6的数，0.1〜10摩尔％的来自四官能性硅烷交联剂的单元，所述单元由式SiO 4/2（III）表示，所述聚有机硅氧烷的膨胀度为5 至15，并且所述含有所述聚有机硅氧烷的接枝共聚物的量为10-70重量％; 以及所述接枝共聚物的制造方法。

7. 发明申请

US20100040885A1 HIGHLY DISPERSIBLE FINE POWDER OF ALKALINE EARTH METAL CARBONATE 有权
标题翻译：碱性金属碳酸盐的高度分散的精细粉末
公开(公告)号：US20100040885A1
公开(公告)日：2010-02-18
申请号：US12530919
申请日：2008-03-12
申请人： Yojiro Ichimura , Takashi Watanabe , Fumio Okada
发明人： Yojiro Ichimura , Takashi Watanabe , Fumio Okada
IPC分类号： C01F11/18
CPC分类号： C01F11/18 , B82Y30/00 , C01F11/186 , C01P2004/54 , C01P2004/62 , C01P2004/64 , C01P2006/12 , C01P2006/14 , C01P2006/16 , C01P2006/22 , Y10T428/2982 , Y10T428/2998
摘要： A fine powder of an alkaline earth metal carbonate selected from the group consisting of barium carbonate, strontium carbonate and calcium carbonate, in which a primary particle of the powder has a mean diameter of 30 to 90 nm, in which the mean diameter is measured on a circle obtained from a projected area of the primary particle, and in which an accumulated volume of micropores having a pore size in the range of 10 to 20 nm is not less than 5×10−2 cm3/g can be easily dispersed in an aqueous medium in the form of essentially primary particles by an industrially employable dispersing method.
摘要翻译：选自碳酸钡，碳酸锶和碳酸钙的碱土金属碳酸盐的细粉末，其中粉末的初级颗粒的平均直径为30至90nm，其中平均直径在从一次粒子的投影面积获得的圆，其中孔径在10〜20nm范围内的微细孔的累积体积不小于5×10 -2 cm 3 / g可以容易地分散在水性介质，其基本上是初级粒子的形式，通过工业上可用的分散方法。

8. 发明授权

US06187939B1 Method for preparing fatty acid esters and fuel comprising fatty acid esters 有权
标题翻译：制备脂肪酸酯和包含脂肪酸酯的燃料的方法
公开(公告)号：US06187939B1
公开(公告)日：2001-02-13
申请号：US09392478
申请日：1999-09-09
申请人： Toshio Sasaki , Tomoyuki Suzuki , Fumio Okada
发明人： Toshio Sasaki , Tomoyuki Suzuki , Fumio Okada
IPC分类号： C11C100
CPC分类号： C11C3/003 , C07C67/03 , C10L1/026 , C10L1/19 , C10M101/04 , Y02E50/13 , Y02P20/544 , Y02P30/20 , C07C69/52
摘要： Fatty acid esters, which are prepared by reacting fats and oils with an alcohol in the absence of a catalyst under a condition under which at least one of the fats and oils and the alcohol is in a supercritical state, are useful as fuels such as diesel fuels, lubrication base oils or fuel additives.
摘要翻译：在脂肪和油和醇中的至少一种处于超临界状态的条件下，在不存在催化剂的情况下使脂肪和油与醇反应制备的脂肪酸酯可用作燃料如柴油燃料，润滑基础油或燃料添加剂。

9. 发明授权

US4725635A Silicone-based synthetic fiber finishing agent 失效
标题翻译：硅胶合成纤维整理剂
公开(公告)号：US4725635A
公开(公告)日：1988-02-16
申请号：US48695
申请日：1987-05-12
申请人： Fumio Okada , Masaki Tanaka , Hiroshi Ohashi
发明人： Fumio Okada , Masaki Tanaka , Hiroshi Ohashi
IPC分类号： D06M13/50 , C08K5/1515 , C08K5/5435 , D06M13/02 , D06M13/11 , D06M13/165 , D06M13/203 , D06M13/51 , D06M13/513 , D06M15/643 , D06M101/00 , D06M101/16 , C08K5/15
CPC分类号： D06M13/513 , C08K5/1515 , C08K5/5435 , D06M13/11 , D06M13/203 , Y10T428/31663
摘要： The silicone-based fiber finishing agent is particularly suitable for synthetic fiber-made fabric materials such as waddings of polyester fibers to impart excellent softness and smoothness in touch and free from yellowing even by heating with high resistance against dry cleaning. The fiber finishing agent comprises (A) an organopolysiloxane of a substantially linear molecular structure terminated at each molecular chain end with a silanolic hydroxy group or alkoxy group and having at least one amino-substituted hydrocarbon group bonded to the silicon atom in a molecule, (B) an epoxy-containing alkoxy silane compound such as methyl dimethoxy 3-glycidyloxypropyl silane and (C) an epoxy-containing organic compound free from silicon such as glycidyl alcohol and glycidyl methacrylate.
摘要翻译：硅氧烷类纤维整理剂特别适用于合成纤维制造的织物材料，例如聚酯纤维的缠绕，以赋予极好的柔软性和平滑感，并且即使通过加热而具有高的抗干洗性也不会发黄。纤维整理剂包含（A）在每个分子链末端具有硅烷醇羟基或烷氧基并在分子中具有至少一个与硅原子键合的氨基取代烃基的基本上线性分子结构的有机聚硅氧烷（ B）含环氧基的烷氧基硅烷化合物如甲基二甲氧基3-缩水甘油氧基丙基硅烷和（C）不含硅的含环氧基的有机化合物，如缩水甘油基醇和甲基丙烯酸缩水甘油酯。

10. 发明授权

US09102810B2 Alkaline earth metal carbonate micropowder 有权
标题翻译：碱土金属碳酸盐微粉
公开(公告)号：US09102810B2
公开(公告)日：2015-08-11
申请号：US13985328
申请日：2012-02-15
申请人： Fumio Okada , Takeshi Himoto , Masayuki Fujimoto
发明人： Fumio Okada , Takeshi Himoto , Masayuki Fujimoto
IPC分类号： C01F11/18 , C09C3/08 , C09C1/02 , C08K3/26 , C01F11/08 , C08K5/09 , B82Y30/00
CPC分类号： C08K3/26 , B82Y30/00 , C01F11/08 , C01F11/185 , C01F11/187 , C01P2004/10 , C01P2004/51 , C01P2004/52 , C01P2004/54 , C01P2004/62 , C01P2004/64 , C08K5/09 , C09C1/02 , C09C1/021 , C09C1/024 , C09C3/08
摘要： Dispersibility of an alkaline earth metal carbonate micropowder in a polymer resin or in an organic solvent is improved by treating the surface of the alkaline earth metal micropowder with a surfactant having hydrophilic groups and hydrophobic groups and groups that form anions in water.
摘要翻译：碱土金属碳酸盐微粉在聚合物树脂或有机溶剂中的分散性通过用具有亲水基团的表面活性剂和在水中形成阴离子的疏水性基团和基团进行处理来提高碱土金属微粉的表面。

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