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1. 发明授权

US5482610A Cathode for coating a substrate 失效
标题翻译：用于涂覆基材的阴极
公开(公告)号：US5482610A
公开(公告)日：1996-01-09
申请号：US20361
申请日：1993-02-22
申请人： Bernd Wolf , Juergen Mueller , Hans Neudert
发明人： Bernd Wolf , Juergen Mueller , Hans Neudert
IPC分类号： C23C14/34 , H01J37/34
CPC分类号： H01J37/3497 , C23C14/3407 , H01J37/3408 , H01J37/3455 , H01J37/3458
摘要： In a cathode system for coating a substrate (46), having a cathode which is connected to a direct-current and/or alternating-current source (high-frequency source) and is disposed in an evacuable coating chamber (2), and is electrically connected to a target (29) which is sputtered and whose sputtered particles deposit themselves on the substrate, a process gas is brought into the coating chamber. The cathode is formed from a substantially pot-like housing (3) whose solid bottom (39) is fixedly joined to the target (29) and whose open end facing away from the target (29) is sealingly held in an opening (49) in the outer wall (30) of the coating chamber such that the interior (49) of the housing (3) is exposed to atmospheric pressure, while the target (29) and the outer surface of the shell-like part of the housing (3) joined thereto are affected by the pressure prevailing in the coating chamber.
摘要翻译：在用于涂覆基板（46）的阴极系统中，具有连接到直流和/或交流电源（高频源）的阴极并设置在可抽真空的涂覆室（2）中，并且是电连接到溅射的靶（29），并且其溅射的颗粒自身沉积在基板上，处理气体被引入涂覆室。阴极由基本上为盆状的外壳（3）形成，其实体底部（39）固定地连接到靶（29），并且其开口端远离靶（29）被密封地保持在开口（49）中，在涂覆室的外壁（30）中，使得壳体（3）的内部（49）暴露于大气压力的同时，靶（29）和壳体的壳状部分的外表面（ 3）受涂层室压力的影响。

2. 发明授权

US09062012B2 Process for manufacturing 4-substituted amino-benzoxazinones 有权
标题翻译：制备4-取代氨基 - 苯并恶嗪酮的方法
公开(公告)号：US09062012B2
公开(公告)日：2015-06-23
申请号：US14365774
申请日：2012-12-20
申请人： Bernd Wolf , Joachim Gebhardt , Uwe Josef Vogelbacher , Maximilian Dochnahl , Michael Rack , Michael Keil , Timo Frassetto , Volker Maywald
发明人： Bernd Wolf , Joachim Gebhardt , Uwe Josef Vogelbacher , Maximilian Dochnahl , Michael Rack , Michael Keil , Timo Frassetto , Volker Maywald
IPC分类号： C07D265/36 , C07D413/04
CPC分类号： C07D265/36 , C07D413/04
摘要： The present invention relates to a process for manufacturing 4-substituted amino-benzoxazinones of formula (I), by reacting a NH-benzoxazinone of formula (II) with a compound of formula (III); wherein the variables are defined according to the description.
摘要翻译：本发明涉及式（I）的4-取代氨基 - 苯并恶嗪酮的制备方法，其中式（II）的N-苯并恶嗪酮与式（III）的化合物反应; 其中根据描述定义变量。

3. 发明授权

US08541611B2 Bifunctional phenyl iso(thio)cyanates, processes and intermediates products for their preparation 失效
标题翻译：双官能苯基异（硫代）氰酸酯，其制备方法和中间体产品
公开(公告)号：US08541611B2
公开(公告)日：2013-09-24
申请号：US13535544
申请日：2012-06-28
申请人： Gerhard Hamprecht , Michael Puhl , Bernd Wolf , Norbert Götz , Michael Keil , Robert Reinhard , Ingo Sagasser , Werner Seitz
发明人： Gerhard Hamprecht , Michael Puhl , Bernd Wolf , Norbert Götz , Michael Keil , Robert Reinhard , Ingo Sagasser , Werner Seitz
IPC分类号： C07C331/28
CPC分类号： C07D213/76 , C07C303/34 , C07C307/06 , C07C331/28 , C07C2601/14 , C07D207/20 , C07D211/18 , C07D211/70 , C07D295/26 , C07D307/52 , C07D319/06 , C07D333/20
摘要： A process for preparing phenyl iso(thio)cyanates of the formula I in which a compound of the formula II or its HCl adduct is reacted with a phosgenating agent where W is oxygen or sulfur and Ar and A are as defined in claim 1 is described. Moreover, the invention relates to the use of the phenyl iso(thio)cyanates for preparing crop protection agents.
摘要翻译：描述式I的苯基异（硫代）氰酸酯的方法，其中将式II化合物或其HCl加合物与W是氧或硫的光气反应剂和Ar和A如权利要求1中所定义的相同。此外，本发明涉及苯基异（硫代）氰酸酯用于制备作物保护剂的用途。

4. 发明申请

US20110004002A1 Process for preparing alkyl 2-alkoxymethylene-4,4-difluoro-3-oxobutyrates 有权
标题翻译：制备2-烷氧基亚甲基-4,4-二氟-3-氧代丁酸烷基酯的方法
公开(公告)号：US20110004002A1
公开(公告)日：2011-01-06
申请号：US12919842
申请日：2009-02-27
申请人： Volker Maywald , Sebastian Peer Smidt , Bernd Wolf , Christopher Koradin , Thomas Zierke , Michael Rack , Michael Keil
发明人： Volker Maywald , Sebastian Peer Smidt , Bernd Wolf , Christopher Koradin , Thomas Zierke , Michael Rack , Michael Keil
IPC分类号： C07D231/14 , C07C69/66
CPC分类号： C07D231/14 , C07C67/343 , C07C69/72
摘要： A process for preparing alkyl 2-alkoxymethylene-4,4-difluoro-3-oxobutyrates (VI) where R is methyl or ethyl, from crude reaction mixtures of alkyl 4,4-difluoroacetoacetates (I) by a) reacting where M is a sodium or potassium ion, and without additional solvent to form an enolate (V) b) releasing the corresponding alkyl 4,4-difluoroacetoacetate (I) from the enolate (V) by means of acid, c) removing the salt formed from cation M and acid anion as a solid and d) converting (I), without isolation from the crude reaction mixture, to the alkyl 2-alkoxymethylene-4,4-difluoro-3-oxobutyrate (VI), and the use of (VI) for preparing 1-methyl-3-difluoromethyl-pyrazol-3-ylcarboxyates VII
摘要翻译：由烷基4,4-二氟乙酰乙酸酯（I）的粗反应混合物制备R为甲基或乙基的2-烷氧基亚甲基-4,4-二氟-3-氧代丁酸烷基酯（VI）的方法，通过a）使M 钠离子或钾离子，无另外的溶剂以形成烯醇化物（Ⅴ）b）通过酸从烯醇化物（Ⅴ）中释出相应的4,4-二氟乙酰乙酸烷基酯（Ⅰ），c）除去由阳离子M形成的盐和酸阴离子作为固体，以及d）将（I）从粗反应混合物中分离出来，转化为2-烷氧基亚甲基-4,4-二氟-3-氧代丁酸烷基酯（VI），以及（VI）用于制备1-甲基-3-二氟甲基 - 吡唑-3-基羧酸酯VII

5. 发明授权

US07820846B2 Bifunctional phenyliso(thio)cyanates, processes and intermediates products for their preparation 有权
标题翻译：双官能苯基（硫代）氰酸酯，其制备方法和中间体产品
公开(公告)号：US07820846B2
公开(公告)日：2010-10-26
申请号：US10532931
申请日：2003-10-29
申请人： Gerhard Hamprecht , Michael Puhl , Bernd Wolf , Norbert Götz , Michael Keil , Robert Reinhard , Ingo Sagasser , Werner Seitz
发明人： Gerhard Hamprecht , Michael Puhl , Bernd Wolf , Norbert Götz , Michael Keil , Robert Reinhard , Ingo Sagasser , Werner Seitz
IPC分类号： C07C255/50
CPC分类号： C07D213/76 , C07C303/34 , C07C307/06 , C07C331/28 , C07C2601/14 , C07D207/20 , C07D211/18 , C07D211/70 , C07D295/26 , C07D307/52 , C07D319/06 , C07D333/20
摘要： A process for preparing phenyl iso(thio)cyanates of the formula I in which a compound of the formula II or its HCl adduct is reacted with a phosgenating agent where W is oxygen or sulfur and Ar and A are as defined in claim 1 is described. Moreover, the invention relates to the use of the phenyl iso(thio)cyanates for preparing crop protection agents.
摘要翻译：描述式I的苯基异（硫代）氰酸酯的方法，其中将式II化合物或其HCl加合物与W是氧或硫的光气反应剂和Ar和A如权利要求1中所定义的相同。此外，本发明涉及苯基异（硫代）氰酸酯用于制备作物保护剂的用途。

6. 发明申请

US20100087640A1 Method for production of aryl-substituted annelated pyrimidines 审中-公开
标题翻译：芳基取代的环状嘧啶的制备方法
公开(公告)号：US20100087640A1
公开(公告)日：2010-04-08
申请号：US12521877
申请日：2008-01-10
申请人： Bernd Wolf , Volker Maywald , Michael Keil , Manuel Budich , Michael Rack , Manfred Ehresmann
发明人： Bernd Wolf , Volker Maywald , Michael Keil , Manuel Budich , Michael Rack , Manfred Ehresmann
IPC分类号： C07D487/04
CPC分类号： C07D487/04
摘要： The present invention relates to a process for preparing aryl-substituted fused pyrimidines of the general formula (I) in which L1 to L5 are H, halogen, CN, NO2, C1-C4-alkyl, C1-C4-haloalkyl, C1-C4-alkoxy, C1-C4-haloalkoxy etc.; Y1 to Y3 are C—RY or N; RY is H or optionally substituted C1-C4-alkyl or two adjacent RY together form a ring; X is OH, Cl or Br; which comprises (i) the reaction of a 2-phenylmalonate with a compound (III) or a tautomer thereof, in the presence of a suitable base, where the alcohol, released during the reaction, of the formula R—OH is continuously removed from the reaction mixture under reduced pressure; giving a compound of the formula (I) or a salt thereof in which X is OH, and, if X in the compounds of the general formula (I) is chlorine or bromine, (ii) the reaction of the compounds of the formula (I) obtained in step (i) or the salts with a halogenating agent.
摘要翻译：本发明涉及制备通式（I）的芳基取代的稠合嘧啶的方法，其中L 1至L 5为H，卤素，CN，NO 2，C 1 -C 4烷基，C 1 -C 4卤代烷基，C 1 -C 4 - 烷氧基，C1-C4-卤代烷氧基等; Y1至Y3为C-RY或N; RY为H或任选取代的C 1 -C 4烷基或两个相邻的RY一起形成环; X是OH，Cl或Br; 其包括（i）2-苯基丙二酸酯与化合物（III）或其互变异构体在合适的碱的存在下反应，其中反应期间释放的醇与式R-OH的连续从减压下的反应混合物; 得到其中X是OH的式（I）化合物或其盐，并且如果通式（I）的化合物中的X是氯或溴，则（ii）式（I）化合物 I）或与卤化剂的盐。

7. 发明授权

US06680410B2 Method for producing oxime ethers 失效
标题翻译：生产肟醚的方法
公开(公告)号：US06680410B2
公开(公告)日：2004-01-20
申请号：US10257327
申请日：2002-10-10
申请人： Roland Götz , Bernd Wolf , Michael Rack
发明人： Roland Götz , Bernd Wolf , Michael Rack
IPC分类号： C07C25156
CPC分类号： C07C249/12 , C07C251/38
摘要： A process for preparing oxime ethers of the formula I, in which the substituents R1 and R2 can be identical or different and can each be cyano, alkyl, haloalkyl, cycloalkyl, phenyl and naphthyl, and R3 can be alkyl, by alkylation of oximes of the formula II under basic conditions with an alkylating agent from the group of alkyl halides, dialkyl sulfates and dialkyl carbonates, wherein the reaction is carried out in a mixture consisting of 5 to 25% by weight of polar aprotic solvents selected from the group of nitrites, N-alkylpyrrolidones, cyclic urea derivatives, dimethylformamide and dimethylacetamide, 55 to 95% by weight of nonpolar solvents selected from the group of aliphatic hydrocarbons, aromatic hydrocarbons, alkyl alkylcarboxylates and ethers, and 0 to 25% by weight of water, the contents thereof totaling 100%.
摘要翻译：制备式I的肟醚的方法，其中取代基R 1和R 2可以相同或不同，并且各自可以是氰基，烷基，卤代烷基，环烷基，苯基和萘基，R 3，可以通过烷基化剂从烷基卤化物，二烷基硫酸盐和碳酸二烷基酯在碱性条件下将式II的肟烷基化，其中该反应以5至25重量％的极性非质子选自亚硝酸盐，N-烷基吡咯烷酮，环脲衍生物，二甲基甲酰胺和二甲基乙酰胺的溶剂，55至95重量％的选自脂族烃，芳烃，烷基烷基羧酸盐和醚的非极性溶剂，和0至25％水重量，总含量为100％。

8. 发明授权

US5446199A Preparation of halomethylbenzoyl cyanides and novel halomethylbenzoyl cyanides 失效
标题翻译：制备卤代甲基苯甲酰氰和新的卤代甲基苯甲酰氰
公开(公告)号：US5446199A
公开(公告)日：1995-08-29
申请号：US216416
申请日：1994-03-23
申请人： Heinz Isak , Thomas Wettling , Michael Keil , Bernd Wolf , Reinhard Doetzer
发明人： Heinz Isak , Thomas Wettling , Michael Keil , Bernd Wolf , Reinhard Doetzer
IPC分类号： C07C253/14 , C07C255/32 , C07C255/40
CPC分类号： C07C255/40 , C07C253/14
摘要： A process for preparing halomethylbenzoyl cyanides IPh-CO-CN I(Ph=phenyl radical substituted by chloromethyl or bromomethyl which, if desired, can additionally carry 1-4 further radicals) by reacting halomethylbenzoyl chlorides IIPh-CO-Cl IIwith an alkali metal cyanide or transition metal cyanide, if appropriate in an organic diluent, and novel halomethylbenzoyl cyanides I' ##STR1## (X=halogen, C.sub.1 -C.sub.4 -alkyl, C.sub.1 -C.sub.4 -alkoxy, CF.sub.3, C.sub.1 -C.sub.5 -alkyl-(C.sub.1 -C.sub.5 -alkyl)hydroxyimino or C.sub.1 -C.sub.5 -alkyl-(C.sub.2 -C.sub.5 -alkenyl)hydroxyimino; m=0 to 4 and Y=chloromethyl or bromomethyl) are described.The halomethylbenzoyl cyanides I are important intermediates for the synthesis of plant protection agents.
摘要翻译：制备卤代甲基苯甲酰基氰化物I Ph-CO-CNI（Ph =被氯甲基或溴甲基取代的苯基，如果需要，还可以另外携带1-4个基团），卤代甲基苯甲酰氯II Ph-CO-ClII与碱金属氰化物或过渡金属氰化物，如果合适，在有机稀释剂中，和新的卤代甲基苯甲酰氰I'（X =卤素，C 1 -C 4 - 烷基，C 1 -C 4 - 烷氧基，CF 3，C 1 -C 5烷基 - （ C 1 -C 5 - 烷基）羟基亚氨基或C 1 -C 5 - 烷基 - （C 2 -C 5 - 烯基）羟基亚氨基; m = 0至4，Y =氯甲基或溴甲基）。卤代甲基苯甲酰氰I是合成植物保护剂的重要中间体。

9. 发明授权

US5342972A Preparation of 6-bromo-2,2-dialkyl-2,3-dihydrobenzofurans which are optionally fluoro-substituted 失效
标题翻译：任选氟取代的6-溴-2,2-二烷基-2,3-二氢苯并呋喃的制备
公开(公告)号：US5342972A
公开(公告)日：1994-08-30
申请号：US19685
申请日：1993-02-19
申请人： Albrecht Harreus , Bernd Wolf , Jochen Wild
发明人： Albrecht Harreus , Bernd Wolf , Jochen Wild
IPC分类号： C07C39/24 , C07C45/54 , C07C49/825 , C07D307/79 , C07D307/82
CPC分类号： C07D307/79 , C07C39/245 , C07C45/54 , C07C49/825
摘要： A process for the preparation of a 2,3-dihydrobenzofuran I ##STR1## or a derivative thereof, where R.sup.a and R.sup.b are C-organic radicals, involves reacting a 2-hydroxybenzyl alcohol II ##STR2## in the presence of an acidic ion exchanger resin and in the presence of an inert dehydrating substance. Novel 2,3-dihydrobenzofurans Ia, 2-acylphenols IVa and 2-hydroxybenzyl alcohols IIa, a process for their preparation, and their use as intermediates are also described.
摘要翻译：制备2,3-二氢苯并呋喃I或其衍生物的方法，其中Ra和Rb是C-有机基团，包括在酸性存在下使2-羟基苄醇II II 离子交换树脂，并在惰性脱水物质的存在下进行。还描述了新的2,3-二氢苯并呋喃Ia，2-酰基苯酚IVa和2-羟基苄醇IIa，其制备方法及其作为中间体的用途。

10. 发明授权

US5214187A Benzonitriles, benzaldehydes and benzyl alcohols 失效
公开(公告)号：US5214187A
公开(公告)日：1993-05-25
申请号：US946586
申请日：1992-09-18
申请人： Bernd Wolf , Hans Theobald , Norbert Goetz
发明人： Bernd Wolf , Hans Theobald , Norbert Goetz
IPC分类号： C07C25/02 , C07C25/18 , C07C25/22 , C07C25/24 , C07C33/20 , C07C33/30 , C07C33/34 , C07C33/46 , C07C33/50 , C07C45/44 , C07C47/542 , C07C47/546 , C07C47/548 , C07C47/55 , C07C255/50
CPC分类号： C07C33/20 , C07C25/02 , C07C25/18 , C07C25/22 , C07C25/24 , C07C255/50 , C07C33/30 , C07C33/34 , C07C33/46 , C07C33/50 , C07C45/44 , C07C47/542 , C07C47/546 , C07C47/548 , C07C47/55 , C07C2101/02 , C07C2101/08 , C07C2101/10 , C07C2101/14 , C07C2101/16 , C07C2101/18 , C07C2102/42
摘要： Novel benzonitriles, benzaldehydes and benzyl alcohols of the formula I ##STR1## where R.sup.1 is methyl or ethyl, R.sup.2 is alkyl, alkenyl, cycloalkyl, cycloalkenyl, bicycloalkyl, bicycloalkenyl, or C.sub.1 -C.sub.5 -alkyl-substituted cycloalkyl, cycloalkenyl, bicycloalkyl or bicycloalkenyl, X is hydrogen, chlorine or fluorine and Z is --CN, CHO or ##STR2## where R.sup.3 is hydrogen, cyano, C.sub.2 -C.sub.4 -alkynyl, C.sub.2 -C.sub.4 -alkenyl or C.sub.1 -C.sub.4 -alkyl, with the proviso that R.sup.2 is not --CH.sub.2 --CH.dbd.CH--B when B is hydrogen, alkyl or alkenyl and at the same time R.sup.1 is methyl and Z is ##STR3## and with the proviso that R.sup.2 is not methyl or ethyl when R.sup.1 is methyl and at the same time Z is ##STR4## and furthermore with the proviso that R.sup.2 is not methyl when R.sup.1 is methyl or ethyl and at the same time Z is --CN or --CHO.

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