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    • 6. 发明授权
    • Method of producing large diameter silicon carbide crystals
    • 生产大直径碳化硅晶体的方法
    • US5746827A
    • 1998-05-05
    • US579277
    • 1995-12-27
    • Donovan L. BarrettRichard N. ThomasRaymond G. Seidensticker, deceasedRichard H. Hopkins
    • Donovan L. BarrettRichard N. ThomasRaymond G. Seidensticker, deceasedRichard H. Hopkins
    • C30B23/00
    • C30B23/00C30B29/36
    • A method for producing crystals of silicon carbide in a furnace. The furnace has a crucible with a cavity in which the cavity has first and second spaced-apart regions. The crucible cavity of the furnace is capable of being heated, preferably by induction or resistance heating, with insulation placed around the crucible and crucible cavity. A source material of silicon carbide is provided at the first region of the crucible cavity, and a monocrystalline seed is placed at the second region of the crucible cavity. A first growth stage is then conducted in which the first region and the second region of the crucible cavity are heated to at least the sublimation temperature of silicon carbide under substantially isothermal conditions. Then, a second growth stage is conducted in which a temperature gradient is provided between the first and the second region of the crucible cavity, such that the seed in the second crucible region is kept at a temperature lower than a temperature of the first crucible region.
    • 一种在炉中制造碳化硅晶体的方法。 炉具有具有空腔的坩埚,其中空腔具有第一和第二间隔开的区域。 炉的坩埚腔能够被加热,优选地通过感应或电阻加热,绝缘体放置在坩埚和坩埚腔周围。 碳坩埚的源材料设置在坩埚腔的第一区域,单晶种子放置在坩埚腔的第二区域。 然后进行第一生长阶段,其中坩埚腔的第一区域和第二区域在基本上等温条件下被加热至至少碳化硅的升华温度。 然后,进行第二生长阶段,其中在坩埚腔的第一和第二区域之间设置温度梯度,使得第二坩埚区域中的种子保持在比第一坩埚区域的温度低的温度 。
    • 10. 发明授权
    • Apparatus for growing large silicon carbide single crystals
    • 用于生长大型碳化硅单晶的装置
    • US5683507A
    • 1997-11-04
    • US523303
    • 1995-09-05
    • Donovan L. BarrettRaymond G. Seidensticker, deceasedRichard H. Hopkins
    • Donovan L. BarrettRaymond G. Seidensticker, deceasedRichard H. Hopkins
    • C30B23/00C30B35/00
    • C30B23/00C30B29/36Y10S117/90Y10S117/902Y10T117/10Y10T117/1008Y10T117/1016
    • An apparatus for growing single-polytype, single crystals of silicon carbide utilizing physical vapor transport as the crystal growth technique. The apparatus has a furnace which has a carbon crucible with walls that border and define a crucible cavity. A silicon carbide source material provided at a first location of the crucible cavity, and a monocrystalline silicon carbide seed is provided at a second location of the crucible cavity. A heat path is also provided in the furnace above the crucible cavity. The crucible has a stepped surface that extends into the crucible cavity. The stepped surface has a mounting portion upon which the seed crystal is mounted. The mounting portion of the stepped surface is bordered at one side by the crucible cavity and is bordered at an opposite side by the furnace heat path. The stepped surface also has a sidewall that is bordered at one side by and surrounds the furnace heat path. The apparatus may also have a thermal insulating member, in which a side of the stepped surface sidewall opposite to the furnace heat path is bordered by the thermal insulating member.
    • 使用物理气相传输作为晶体生长技术生长单多晶单晶碳化硅的装置。 该装置具有炉子,该炉具有边界并限定坩埚腔的壁的碳坩埚。 提供在坩埚腔的第一位置处的碳化硅源材料和在坩埚腔的第二位置处提供单晶碳化硅种子。 在坩埚腔上方的炉内还设置有热路径。 坩埚具有延伸到坩埚腔中的台阶表面。 台阶表面具有安装在晶圆上的安装部分。 阶梯式表面的安装部分在坩埚腔的一侧边界,并且通过炉子热路与另一边相接。 台阶表面还具有侧壁,并且围绕炉子热路径包围着侧壁。 该设备还可以具有绝热构件,其中与炉热路相对的台阶表面侧壁的一侧由隔热构件界定。