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81. 发明申请

US20150376111A1 METHOD FOR PRODUCING NITROALKANES IN A MICROSTRUCTURED REACTOR 有权
标题翻译：在微结构反应器中生产硝基的方法
公开(公告)号：US20150376111A1
公开(公告)日：2015-12-31
申请号：US14768391
申请日：2014-04-25
申请人： BASF SE
发明人： Ralf BOEHLING , Michael HAYER , Alwin REHFINGER , Michael SCHELPER , Johann-Peter MELDER , Martin ERNST , Joaquim Henrique TELES
IPC分类号： C07C201/08
CPC分类号： C07C201/08 , B01J19/0093 , B01J2219/00792 , B01J2219/00795 , B01J2219/00824 , B01J2219/00826 , B01J2219/00831 , B01J2219/00835 , B01J2219/00842 , B01J2219/0086 , B01J2219/00867 , B01J2219/00873 , B01J2219/00889 , B01J2219/00891 , Y02P20/582 , C07C205/02
摘要： The invention relates to a process for preparing nitroalkanes by reaction of at least one alkane with at least one nitrating agent in the gas phase, wherein the nitration is carried out in a microstructured reaction zone having parallel channels having hydraulic diameters of less than 2.5 mm and a total specific internal surface area of more than 1600 m2/m3 and the alkane and the nitrating agent are conveyed under a pressure of from 1 bar to 20 bar through the reaction zone and reacted at a temperature of from 150° C. to 650° C. and the reaction products are cooled downstream of the reaction zone and discharged and the at least one nitrating agent is introduced over from two to ten introduction points along the reaction zone.
摘要翻译：本发明涉及通过在气相中至少一种烷烃与至少一种硝化剂反应来制备硝基烷烃的方法，其中硝化在具有水力直径小于2.5mm的平行通道的微结构反应区中进行，以及超过1600m 2 / m 3的总比表面积和烷烃和硝化剂在1巴-20巴的压力下通过反应区输送，并在150℃至650℃的温度下反应并且反应产物在反应区的下游冷却并排出，并且将至少一种硝化剂沿着反应区引入二至十个引入点。

82. 发明申请

US20140377144A1 In Situ Mixing in Microchannels 审中-公开
标题翻译：微通道原位混合
公开(公告)号：US20140377144A1
公开(公告)日：2014-12-25
申请号：US14176976
申请日：2014-02-10
申请人： VELOCYS, INC.
发明人： Anna Lee Tonkovich , KAI JAROSCH , DAVID J. HESSE , SEAN P. FITZGERALD
IPC分类号： B01L3/00
CPC分类号： B01L3/502715 , B01F5/0475 , B01F5/0682 , B01F5/0691 , B01F13/0059 , B01F2215/0427 , B01F2215/0431 , B01J19/0093 , B01J2219/00783 , B01J2219/00822 , B01J2219/00824 , B01J2219/00835 , B01J2219/00844 , B01J2219/0086 , B01J2219/00873 , B01J2219/00889 , B01J2219/00891 , B01L2400/04 , Y10T137/0329
摘要： The present invention provides methods, systems and apparatus in which one fluid passes through an orifice or orifices and mixes with another fluid as it flows through a microchannel.
摘要翻译：本发明提供了一种方法，系统和装置，其中一种流体在其流过微通道时通过孔或孔并与另一流体混合。

83. 发明申请

US20140217328A1 Electroless Plating in Microchannels 审中-公开
标题翻译：微通道中的化学镀
公开(公告)号：US20140217328A1
公开(公告)日：2014-08-07
申请号：US14177116
申请日：2014-02-10
申请人： Velocys, Inc.
发明人： Francis P. Daly , Richard Q. Long , Barry Lee-Mean Yang , Terry J. Mazanec , Rachid Taha , Junko Ida
IPC分类号： B01J19/00 , C01B3/40 , B01J23/42
CPC分类号： B01J19/0053 , B01J19/0093 , B01J21/066 , B01J23/42 , B01J23/464 , B01J23/628 , B01J23/892 , B01J23/8926 , B01J35/002 , B01J35/006 , B01J37/0225 , B01J37/0226 , B01J37/0244 , B01J37/14 , B01J37/16 , B01J37/18 , B01J2219/00783 , B01J2219/00822 , B01J2219/00824 , B01J2219/00831 , B01J2219/00835 , B01J2219/00844 , B01J2219/0086 , B01J2219/00873 , B01J2219/00891 , C01B3/384 , C01B3/40 , C01B32/40 , C01B2203/0233 , C01B2203/0238 , C01B2203/0244 , C01B2203/0261 , C01B2203/0811 , C01B2203/0822 , C01B2203/0827 , C01B2203/1047 , C01B2203/107 , C01B2203/1241 , C07C5/48 , C07C2523/42 , C07C2523/46 , C23C18/1216 , C23C18/1644 , C23C18/1803 , C23C18/1817 , C23C18/44 , Y02E60/364 , Y02P20/128 , Y02P20/142 , Y02P20/52 , Y02T50/67 , Y02T50/6765 , C07C11/04
摘要： Novel methods of electroless plating are described. Catalyst coatings can be applied within microchannel apparatus. Various reactions, including combustion and steam reforming, can be conducted over electroless catalyst coatings.
摘要翻译：描述了无电镀的新方法。催化剂涂层可以应用于微通道设备内。可以通过无电催化剂涂层进行各种反应，包括燃烧和蒸汽重整。

84. 发明申请

US20140134547A1 INTEGRATED REACTORS, METHODS OF MAKING SAME, AND METHODS OF CONDUCTING SIMULTANEOUS EXOTHERMIC AND ENDOTHERMIC REACTIONS 审中-公开
标题翻译：一体化反应器，其制备方法以及导致同时发生和内毒素反应的方法
公开(公告)号：US20140134547A1
公开(公告)日：2014-05-15
申请号：US14053500
申请日：2013-10-14
申请人： Battelle Memorial Institute
发明人： Anna Lee Tonkovich , Gary Roberts , Steven T. Perry , Sean P. Fitzgerald , Robert S. Wegeng , Yong Wang , David Vanderwiel , Jennifer L. Marco
IPC分类号： B01J8/02 , F23N1/00
CPC分类号： B01J8/0285 , B01J12/007 , B01J19/0093 , B01J19/249 , B01J2208/00309 , B01J2219/00783 , B01J2219/00822 , B01J2219/00824 , B01J2219/00833 , B01J2219/00835 , B01J2219/00844 , B01J2219/0086 , B01J2219/00873 , B01J2219/00891 , B01J2219/2453 , B01J2219/2458 , B01J2219/2459 , B01J2219/2465 , B01J2219/247 , B01J2219/2471 , B01J2219/2474 , B01J2219/2475 , B01J2219/2479 , B01J2219/2482 , B01J2219/2497 , B01J2219/2498 , C01B3/38 , C01B3/384 , C01B3/501 , C01B13/0251 , C01B2203/0233 , C01B2203/0244 , C01B2203/0261 , C01B2203/0283 , C01B2203/041 , C01B2203/0495 , C01B2203/0811 , C01B2203/0822 , C01B2203/0827 , C01B2203/0833 , C01B2203/0844 , C01B2203/0883 , C01B2203/1005 , C01B2203/1029 , C01B2203/1035 , C01B2203/1041 , C01B2203/1064 , C01B2203/1076 , C01B2203/1082 , C01B2203/1205 , C01B2203/1241 , C01B2203/1276 , C01B2203/1288 , C01B2203/141 , C01B2203/142 , C01B2203/148 , C01B2203/1604 , C01B2203/1619 , C01B2203/1633 , C01B2203/1652 , C01B2203/1676 , C01B2203/169 , C01B2203/1695 , C01B2203/82 , F23C13/00 , F23N1/007 , H01M8/0631 , Y02E60/324 , Y02P20/128 , Y02P20/52 , Y02P70/56 , Y10T29/49826
摘要： Integrated Combustion Reactors (ICRs) and methods of making ICRs are described in which combustion chambers (or channels) are in direct thermal contact to reaction chambers for an endothermic reaction. Superior results were achieved for combustion chambers which contained a gap for free flow through the chamber. Particular reactor designs are also described. Processes of conducting reactions in integrated combustion reactors are described and results presented. Some of these processes are characterized by unexpected and superior results.
摘要翻译：描述了集成燃烧反应器（ICR）和制造ICR的方法，其中燃烧室（或通道）与用于吸热反应的反应室直接热接触。对于具有通过室的自由流动的间隙的燃烧室实现了优异的结果。还描述了特定的反应器设计。介绍了综合燃烧反应器中进行反应的过程，并提出了结果。其中一些过程的特征是意想不到的和优异的结果。

85. 发明申请

US20140115871A1 SYSTEMS AND METHODS FOR SCALE-UP OF CONTINUOUS FLOW REACTORS 审中-公开
标题翻译：连续流动反应器定标系统及方法
公开(公告)号：US20140115871A1
公开(公告)日：2014-05-01
申请号：US14125720
申请日：2012-06-07
申请人： Roland Guidat , Olivier Lobet , Pierr Woehl
发明人： Roland Guidat , Olivier Lobet , Pierr Woehl
IPC分类号： B01J19/00
CPC分类号： B01J19/0053 , B01J19/0093 , B01J2219/00015 , B01J2219/00824 , B01J2219/00831 , B01J2219/0086 , B01J2219/00873 , B01J2219/00995 , Y10T29/49
摘要： A method is disclosed for the seamless scale-up of a micro reactor process, to transfer lab test to a pilot or production unit, the process comprising the steps of using a wall material for the lab reactor with a thermal conductivity lower than 3 W/m-K, and using a wall material for the production reactor with a thermal conductivity higher than 5 W/m-K. According to one preferred embodiment, the velocity is kept constant, and the height of the channel is determined, in order to keep the volumetric heat transfer properties constant, according to the formula: wherein HG is the overall volumetric heat transfer coefficient in the pilot or production process; A B and C are constants; Dh is the hydraulic diameter of the channel in the pilot or production process; λw is the thermal conductivity of the wall in the pilot or production process; b is the empirically determined power to which the Reynolds number is raised in the equation for the Nusselt criteria (Nu=a−RebPrc) for the type of flow in the pilot or production process; h is the height of the channel in the pilot or production process; and HG0 is the overall volumetric heat transfer coefficient in the lab-scale process.
摘要翻译：公开了一种用于微反应器过程的无缝放大以将实验室测试转移到先导或生产单元的方法，该方法包括以下步骤：使用导热率低于3W / mK，并且使用导热率高于5W / mK的生产反应器的壁材料。根据一个优选实施例，速度保持恒定，并且确定通道的高度，以便保持体积传热性能恒定，其中HG是飞行员中的总体积传热系数，或生产过程; A B和C是常数; Dh是先导或生产过程中通道的液压直径; λw是先导或生产过程中墙壁的导热系数; b是在试点或生产过程中的流量类型的努塞尔标准（Nu = a-RebPrc）的方程中提高雷诺数的经验确定的功率; h是飞行员或生产过程中通道的高度; HG0是实验室规模过程中的总体积传热系数。

86. 发明申请

US20140087036A1 FLUID PROCESSING APPARATUS 有权
标题翻译：流体加工设备
公开(公告)号：US20140087036A1
公开(公告)日：2014-03-27
申请号：US14032575
申请日：2013-09-20
申请人： TOTAL SYNTHESIS LTD.
发明人： Michael ORGAN , Debasis MALLIK
IPC分类号： B01J19/12 , A23L3/01
CPC分类号： B01J19/126 , A23L3/01 , B01J19/0093 , B01J2219/00792 , B01J2219/00824 , B01J2219/00831 , B01J2219/00873 , B01J2219/00941 , B01J2219/00963 , B01J2219/00986 , G01N1/44 , G01N35/1097
摘要： A fluid processing assembly comprises a lumen for receiving at least one inlet stream and dispensing a primary product stream, and an energizing device for supplying energy to an energizable portion of the lumen. A primary product collection assembly is in fluid communication with the lumen for receiving the primary product stream. The energizable portion is positioned exterior to the primary product collection assembly. A pressurized gas source is downstream of the lumen. The pressurized gas source supplies pressurized gas to the primary product collection assembly for pressurizing at least a portion of the primary product collection assembly and the lumen.
摘要翻译：流体处理组件包括用于接收至少一个入口流并分配初级产物流的内腔，以及用于向内腔的可激发部分供应能量的激励装置。初级产品收集组件与内腔流体连通以接收初级产品流。可激励部分位于主要产品收集组件的外部。加压气源在管腔的下游。加压气体源将加压气体供应到初级产品收集组件，用于对主要产品收集组件和内腔的至少一部分进行加压。

87. 发明授权

US08557186B2 Integrated reactors, methods of making same, and methods of conducting simultaneous exothermic and endothermic reactions 有权
公开(公告)号：US08557186B2
公开(公告)日：2013-10-15
申请号：US12891800
申请日：2010-09-27
申请人： Anna Lee Tonkovich , Gary Roberts , Steven T. Perry , Sean P. Fitzgerald , Robert S. Wegeng , Yong Wang , David Vanderwiel , Jennifer L. Marco
发明人： Anna Lee Tonkovich , Gary Roberts , Steven T. Perry , Sean P. Fitzgerald , Robert S. Wegeng , Yong Wang , David Vanderwiel , Jennifer L. Marco
IPC分类号： B01J19/00 , B01J8/00 , B01J8/02 , B01J35/02
CPC分类号： B01J8/0285 , B01J12/007 , B01J19/0093 , B01J19/249 , B01J2208/00309 , B01J2219/00783 , B01J2219/00822 , B01J2219/00824 , B01J2219/00833 , B01J2219/00835 , B01J2219/00844 , B01J2219/0086 , B01J2219/00873 , B01J2219/00891 , B01J2219/2453 , B01J2219/2458 , B01J2219/2459 , B01J2219/2465 , B01J2219/247 , B01J2219/2471 , B01J2219/2474 , B01J2219/2475 , B01J2219/2479 , B01J2219/2482 , B01J2219/2497 , B01J2219/2498 , C01B3/38 , C01B3/384 , C01B3/501 , C01B13/0251 , C01B2203/0233 , C01B2203/0244 , C01B2203/0261 , C01B2203/0283 , C01B2203/041 , C01B2203/0495 , C01B2203/0811 , C01B2203/0822 , C01B2203/0827 , C01B2203/0833 , C01B2203/0844 , C01B2203/0883 , C01B2203/1005 , C01B2203/1029 , C01B2203/1035 , C01B2203/1041 , C01B2203/1064 , C01B2203/1076 , C01B2203/1082 , C01B2203/1205 , C01B2203/1241 , C01B2203/1276 , C01B2203/1288 , C01B2203/141 , C01B2203/142 , C01B2203/148 , C01B2203/1604 , C01B2203/1619 , C01B2203/1633 , C01B2203/1652 , C01B2203/1676 , C01B2203/169 , C01B2203/1695 , C01B2203/82 , F23C13/00 , F23N1/007 , H01M8/0631 , Y02E60/324 , Y02P20/128 , Y02P20/52 , Y02P70/56 , Y10T29/49826
摘要： Integrated Combustion Reactors (ICRs) and methods of making ICRs are described in which combustion chambers (or channels) are in direct thermal contact to reaction chambers for an endothermic reaction. Superior results were achieved for combustion chambers which contained a gap for free flow through the chamber. Particular reactor designs are also described. Processes of conducting reactions in integrated combustion reactors are described and results presented. Some of these processes are characterized by unexpected and superior results.

88. 发明授权

US08524173B2 Microchannel structure and fine-particle production method using the same 有权
标题翻译：微通道结构和微粒生产方法使用相同
公开(公告)号：US08524173B2
公开(公告)日：2013-09-03
申请号：US11847788
申请日：2007-08-30
申请人： Maho Yamanaka , Akira Kawai , Koji Katayama , Hiroki Takamiya
发明人： Maho Yamanaka , Akira Kawai , Koji Katayama , Hiroki Takamiya
IPC分类号： B01F3/08
CPC分类号： B01F3/0807 , B01F5/0475 , B01F5/0478 , B01F13/0059 , B01F13/1013 , B01F13/1022 , B01J19/0093 , B01J2219/00783 , B01J2219/00822 , B01J2219/00824 , B01J2219/00826 , B01J2219/00828 , B01J2219/00831 , B01J2219/00833 , B01J2219/0086 , B01J2219/00889 , B01J2219/00891 , B01J2219/00903 , Y10T137/0396
摘要： A microchannel structure including a dispersed-phase introduction channel which communicates with a dispersed-phase introduction inlet; a continuous-phase introduction channel which communicates with a continuous-phase introduction inlet; a discharge channel which communicates with a discharge outlet; a fine-particle formation channel; and a plurality of branch channels for dispersed-phase introduction which are microchannels; wherein one end of the fine-particle formation channel in a fluid traveling direction communicates with the continuous-phase introduction channel whereas the other end thereof communicates with the discharge channel; and wherein a side part of the dispersed-phase introduction channel and side part of the fine-particle formation channel communicate via the plurality of branch channel for dispersed-phase introduction.
摘要翻译：一种微通道结构，包括与分散相引入口连通的分散相导入通道; 与连续相导入口连通的连续相导入流路; 排出通道，其与排出口连通; 细颗粒形成通道; 以及用于分散相导入的多个分支通道，它们是微通道; 其特征在于，所述细粒形成流路的流体行进方向的一端与所述连续相导入流路连通，而所述微粒形成流路的另一端与所述排出流路连通。并且其中分散相导入通道的侧部和细颗粒形成通道的侧部通过多个用于分散相引入的分支通道连通。

89. 发明授权

US08338325B2 Tethered catalyst processes in microchannel reactors and systems containing a tethered catalyst or tethered chiral auxiliary 失效
标题翻译：在微通道反应器和含有拴系催化剂或系链手性助剂的体系中的连结催化剂工艺
公开(公告)号：US08338325B2
公开(公告)日：2012-12-25
申请号：US10642439
申请日：2003-08-14
申请人： John H. Brophy , Kai Jarosch
发明人： John H. Brophy , Kai Jarosch
IPC分类号： B01J21/00 , B01J23/00 , B01J25/00 , B01J29/00 , B01J31/00 , B01J21/04 , B01J23/02
CPC分类号： B01J19/0093 , B01J21/08 , B01J31/0212 , B01J31/0237 , B01J31/08 , B01J31/1633 , B01J31/1815 , B01J31/185 , B01J31/1855 , B01J31/20 , B01J31/226 , B01J31/24 , B01J31/2404 , B01J2219/00783 , B01J2219/00788 , B01J2219/00822 , B01J2219/00824 , B01J2219/00826 , B01J2219/00835 , B01J2219/0086 , B01J2219/00873 , B01J2219/00891 , B01J2231/12 , B01J2231/20 , B01J2231/32 , B01J2231/321 , B01J2231/325 , B01J2231/341 , B01J2231/342 , B01J2231/348 , B01J2231/40 , B01J2231/4205 , B01J2231/4211 , B01J2231/4261 , B01J2231/4266 , B01J2231/52 , B01J2231/543 , B01J2231/643 , B01J2231/72 , B01J2531/80 , B01J2531/824 , C07B37/00 , C07B37/02 , C07B37/04 , C07B61/00 , C07C45/38 , C07C45/39 , C07C45/46 , C07C67/343 , C07C205/45 , C07C253/30 , F28F2260/02 , Y02P20/588 , C07C69/618 , C07C255/41
摘要： The invention provides systems and methods for conducting reactions in which a reactant contacts a tethered catalyst and/or tethered chiral auxiliary in a microchannel and is converted to product.
摘要翻译：本发明提供用于进行反应的系统和方法，其中反应物在微通道中接触系留的催化剂和/或连接的手性助剂并转化成产物。

90. 发明申请

US20120288417A1 Assembly of Flat on Structured Glass Layers 有权
标题翻译：结构玻璃层上的平面装配
公开(公告)号：US20120288417A1
公开(公告)日：2012-11-15
申请号：US13522388
申请日：2011-01-28
申请人： Antoine Gaston Denis Bisson , Thierry Luc Alain Dannoux , Anne Paris
发明人： Antoine Gaston Denis Bisson , Thierry Luc Alain Dannoux , Anne Paris
IPC分类号： B01J19/00
CPC分类号： B81C1/00119 , B01J19/0093 , B01J2219/00783 , B01J2219/00824 , B01J2219/00831 , B01J2219/0086 , B01J2219/00873 , B81B2201/058 , B81C2201/019
摘要： A microfluidic device (100) made from glass, ceramic or vitroceramic, comprises an upper layer (122), a lower layer (124) and an intermediate layer (114), the intermediate layer (114) comprising an upper face (114b) and a lower face (114a), the lower face (114a) comprising a first open structured surface defining a first microfluidic channel (126) and the upper face (114b) comprising a second open structured surface defining a second microfluidic channel (112); the lower surface of the intermediate layer (114) cooperating with a first planar layer closing the first microchannel (126); the upper face (114b) of the intermediate layer (114) cooperating with a second planar layer (130), closing the second microfluidic channel (112) in a sealed manner, and the second planar layer constituting an intermediate layer (130) which cooperates, on its face opposite the intermediate layer (114), with another layer (122) comprising on its inner face (122a) a structured surface defining a third microfluidic channel (128).
摘要翻译：由玻璃，陶瓷或陶瓷制成的微流体装置（100）包括上层（122），下层（124）和中间层（114），中间层（114）包括上表面（114b）和下表面（114a），所述下表面（114a）包括限定第一微流体通道（126）的第一开放结构化表面，并且所述上表面（114b）包括限定第二微流体通道（112）的第二开放结构化表面; 中间层（114）的下表面与闭合第一微通道（126）的第一平面层协作; 所述中间层（114）的上表面（114b）与第二平面层（130）配合，密封地封闭所述第二微流体通道（112），所述第二平面层构成中间层（130），所述中间层在其与中间层（114）相对的表面上，另一层（122）在其内表面（122a）上包括限定第三微流体通道（128）的结构化表面。

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