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    • 21. 发明授权
    • Benzimidazole based aerogel materials
    • 苯并咪唑基气凝胶材料
    • US09434831B2
    • 2016-09-06
    • US14450942
    • 2014-08-04
    • Aspen Aerogels, Inc.
    • Wendell E RhineDavid Mihalcik
    • C08J9/20C08J9/28
    • C08J9/28C08J9/0066C08J9/0085C08J9/286C08J2201/0502C08J2205/024C08J2205/026C08J2205/042C08J2205/05C08J2205/06C08J2379/04D06M15/3562D06M2400/02
    • The present invention provides aerogel materials based on imidazoles and polyimidazoles. The polyimidazole based aerogel materials can be thermally stable up to 500° C. or more, and can be carbonized to produce a carbon aerogel having a char yield of 60% or more, specifically 70% or more. The present invention also provides methods of producing polyimidazole based aerogel materials by reacting at least one monomer in a suitable solvent to form a polybenzimidazole gel precursor solution, casting the polybenzimidazole gel precursor solution into a fiber reinforcement phase, allowing the at least one gel precursor in the precursor solution to transition into a gel material, and drying the gel materials to remove at least a portion of the solvent, to obtain an polybenzimidazole-based aerogel material.
    • 本发明提供了基于咪唑和聚咪唑的气凝胶材料。 基于聚咪唑的气凝胶材料可以在高达500℃或更高温度下是热稳定的,并且可以被碳化以产生炭黑产率为60%以上,特别是70%以上的碳气凝胶。 本发明还提供了通过使至少一种单体在合适的溶剂中反应以形成聚苯并咪唑凝胶前体溶液来生产聚咪唑基气凝胶材料的方法,将聚苯并咪唑凝胶前体溶液浇铸到纤维增强相中,使至少一种凝胶前体 转变成凝胶材料的前体溶液,并干燥凝胶材料以除去至少一部分溶剂,得到基于聚苯并咪唑的气凝胶材料。
    • 27. 发明申请
    • POLYACRYLIC ACID-TYPE WATER ABSORBENT RESIN AND METHOD FOR PRODUCING SAME
    • 聚丙烯酸型吸水树脂及其制造方法
    • US20150259494A1
    • 2015-09-17
    • US14723026
    • 2015-05-27
    • Nippon Shokubai Co., Ltd.
    • Toshihiro TakaaiHidenori WadaSinichi Fujino
    • C08J9/12
    • C08J9/122A61L15/24A61L15/60C08F2/01C08F20/00C08F220/06C08J3/245C08J9/20C08J9/36C08J2203/06C08J2205/05C08J2333/02C08J2335/02Y10T428/2982C08L33/02C08F2222/1013
    • Provided is a method for producing a water absorbent resin, which promotes the formation of interconnected voids (continuous gas bubbles) in a foamed polymer (foam-like water absorbent resin) by a more convenient method, and produces with high efficiency a water absorbent resin which exhibits a high water absorption rate even when stepped into a sheet form or a powder form in hygiene articles and the like. Disclosed is a method for producing a polyacrylic acid-type water absorbent resin, comprising (A) a step of obtaining an aqueous solution of acrylic acid-type monomers containing gas bubbles dispersed therein; (B) a step of polymerizing the aqueous monomer solution and thereby obtaining a foamed polymer; and (C) a step of heating and drying the foamed polymer, wherein gas bubbles are incorporated such that the volumetric expansion factor defined by the following formula (1); [Formula 1] Volumetric expansion factor=(Volume of aqueous monomer solution after gas bubble dispersion)/(volume of aqueous monomer solution before gas bubble dispersion)  Formula (1) ; exceeds 1.1 times, and the aqueous monomer solution having a monomer concentration defined by the following formula (2); [Formula 2] Monomer concentration [wt %]=(Weight of a monomer)/{(weight of a monomer)+(weight of solvent)}×100  Formula (2) ; of 40% by weight or greater is boiling polymerized at a temperature of 100° C. or higher.
    • 提供一种通过更方便的方法促进发泡聚合物(泡沫状吸水性树脂)中形成互连空隙(连续气泡)的吸水性树脂的制造方法,高效率地制造吸水性树脂 即使在卫生用品等中成为片状或粉末状时,也显示出高的吸水率。 公开了一种聚丙烯酸型吸水性树脂的制造方法,其特征在于,包括:(A)获得含有分散在其中的气泡的丙烯酸型单体的水溶液的工序; (B)使单体水溶液聚合,得到发泡聚合物的工序; 和(C)加热和干燥发泡聚合物的步骤,其中加入气泡,使得由下式(1)定义的体积膨胀系数; [式1]体积膨胀系数=(气泡分散后的单体水溶液体积)/(气泡分散前的单体溶液的体积)式(1) 超过1.1倍,单体浓度由下式(2)定义的单体水溶液; [式2]单体浓度[wt%] =(单体重量)/ {(单体重量)+(溶剂重量)}×100式(2) 为40重量%以上时,在100℃以上的温度下进行沸腾聚合。