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1. 发明授权

US4033911A Process for catalyzing polyurethane foam formation using N,N-dimethyl-aminoalkoxy-propionitriles 失效
标题翻译：使用N，N-二甲基 - 氨基烷氧基 - 丙腈催化聚氨酯泡沫形成的方法
公开(公告)号：US4033911A
公开(公告)日：1977-07-05
申请号：US699459
申请日：1976-06-24
申请人： Michael Ray Sandner , Bela Prokai
发明人： Michael Ray Sandner , Bela Prokai
IPC分类号： C08G18/18 , C08G18/14
CPC分类号： C08G18/185 , Y10S521/904
摘要： Cellular urethane polymers are provided by effecting the reaction of an organic polyol reactant comprising a polyether polyol and an organic polyisocyanate reactant in the presence of a blowing agent and a catalyst system comprising an N,N-dimethylaminoalkoxypropionitrile. The said N,N-dimethylaminoalkoxypropionitriles are versatile, low odor catalysts and are useful in forming cellular urethane polymers ranging from all water-blown flexible polyether foam to all fluorocarbon-blown rigid foam products. Especially preferred for use in the practice of the invention are 3-(2-dimethylaminoethoxy)propionitrile and 3-[2-(2-dimethylaminoethoxy)ethoxy]propionitrile either as such or in combination with other catalysts including other tertiary-amine components and/or organic compounds of tin. Also provided are blended catalyst systems comprising said dimethylaminoalkoxypropionitriles.
摘要翻译：通过在发泡剂和包含N，N-二甲基氨基烷氧基丙腈的催化剂体系的存在下进行包含聚醚多元醇和有机聚异氰酸酯反应物的有机多元醇反应物的反应来提供蜂窝状聚氨酯聚合物。所述N，N-二甲基氨基烷氧基丙氧基化合物是通用的，低气味的催化剂，并且可用于形成细胞聚氨酯聚合物，范围从所有水吹柔性聚醚泡沫塑料到所有碳氟化合物吹塑硬质泡沫产品。特别优选用于实施本发明的是3-（2-二甲基氨基乙氧基）丙腈和3- [2-（2-二甲基氨基乙氧基）乙氧基]丙腈，或者与包括其它叔胺组分在内的其它催化剂和/ 或锡的有机化合物。还提供了包含所述二甲基氨基烷氧基丙纶的共混催化剂体系。

2. 发明授权

US4115321A Catalyst systems containing N,N-dimethylaminoalkoxypropionitriles for polyurethane foam formulation 失效
标题翻译：含有聚氨酯泡沫塑料配方的N，N-二甲基氨基烷氧基丙烯腈的催化剂体系
公开(公告)号：US4115321A
公开(公告)日：1978-09-19
申请号：US784418
申请日：1977-04-04
申请人： Michael Ray Sandner , Bela Prokai
发明人： Michael Ray Sandner , Bela Prokai
IPC分类号： C08G18/18 , B01J31/04 , B01J27/22 , B01J31/02 , C08G18/14
CPC分类号： C08G18/185 , Y10S521/904
摘要： Cellular urethane polymers are provided by effecting the reaction of an organic polyol reactant comprising a polyether polyol and an organic polyisocyanate reactant in the presence of a blowing agent and a catalyst system comprising an N,N-dimethylaminoalkoxypropionitrile. The said N,N-dimethylaminoalkoxypropionitriles are versatile, low odor catalysts and are useful in forming cellular urethane polymers ranging from all water-blown flexible polyether foam to all fluorocarbon-blown rigid foam products. Especially preferred for use in the practice of the invention are 3-(2-dimethylaminoethoxy)propionitrile and 3-[2-(2-dimethylaminoethoxy)ethoxy]propionitrile either as such or in combination with other catalysts including other tertiary-amine components and/or organic compounds of tin. Also provided are blended catalyst systems comprising said dimethylaminoalkoxypropionitriles.
摘要翻译：通过在发泡剂和包含N，N-二甲基氨基烷氧基丙腈的催化剂体系的存在下进行包含聚醚多元醇和有机聚异氰酸酯反应物的有机多元醇反应物的反应来提供蜂窝状聚氨酯聚合物。所述N，N-二甲基氨基烷氧基丙氧基化合物是通用的，低气味的催化剂，并且可用于形成细胞聚氨酯聚合物，范围从所有水吹柔性聚醚泡沫塑料到所有碳氟化合物吹塑硬质泡沫产品。特别优选用于实施本发明的是3-（2-二甲基氨基乙氧基）丙腈和3- [2-（2-二甲基氨基乙氧基）乙氧基]丙腈，或者与包括其它叔胺组分的其它催化剂和/ 或锡的有机化合物。还提供了包含所述二甲基氨基烷氧基丙纶的共混催化剂体系。

3. 发明申请

US20180194889A1 NITROGEN-CONTAINING COMPOUNDS SUITABLE FOR USE IN THE PRODUCTION OF POLYURETHANES 审中-公开
公开(公告)号：US20180194889A1
公开(公告)日：2018-07-12
申请号：US15323154
申请日：2015-07-23
申请人： Evonik Degussa GmbH
发明人： Thomas Günther , Michael Fiedel , Olga Fiedel , Martin Glos , Roland Hubel
IPC分类号： C08G18/20 , C08G18/76 , C08G18/48 , C07D207/06 , C07D403/12 , C07D403/14
CPC分类号： C08G18/2018 , C07D207/06 , C07D403/12 , C07D403/14 , C08G18/165 , C08G18/1825 , C08G18/1833 , C08G18/1841 , C08G18/185 , C08G18/1858 , C08G18/2081 , C08G18/244 , C08G18/48 , C08G18/4816 , C08G18/4829 , C08G18/6688 , C08G18/7621 , C08G18/7664 , C08G18/7671 , C08G2101/0008 , C08G2101/0016 , C08G2101/0025 , C08G2101/0041 , C08G2101/0083 , C08G2105/02 , C08G2170/60 , C08G2290/00 , C08G2340/00 , C08G2350/00 , C08G2410/00 , C08J9/141 , C08J2203/02 , C08J2203/14 , C08J2203/204 , C08J2375/04
摘要： The present invention provides for the use of nitrogen compounds of formula (I) and/or of corresponding quaternized and/or protonated compounds for production of polyurethanes, compositions containing these compounds and polyurethane systems, especially polyurethane foams, which have been obtained using the compounds.

4. 发明申请

US20160002426A1 Additives for Improving Polyurethane Foam Performance 审中-公开
标题翻译：改善聚氨酯泡沫性能的添加剂
公开(公告)号：US20160002426A1
公开(公告)日：2016-01-07
申请号：US14851081
申请日：2015-09-11
申请人： AIR PRODUCTS AND CHEMICALS, INC..
发明人： Juan Jesus Burdeniuc , James Douglas Tobias , Renee Jo Keller , You-Moon Jeon
IPC分类号： C08J9/00
CPC分类号： C08J9/0028 , C08G18/0838 , C08G18/16 , C08G18/185 , C08G18/4072 , C08G18/6552 , C08G2101/00 , C08G2101/0008 , C08J9/0033 , C08J9/0042 , C08J2205/05 , C08J2375/04 , C08J2375/08
摘要： A composition and process useful to make flexible polyurethane foams and in particular flexible molded polyurethane foams is disclosed. The usage of dipolar aprotic liquids such as DMSO, DMI, sulfolane, N-methyl-acetoacetamide, N,N-dimethylacetoacetamide as well as glycols containing hydroxyl numbers OH#≦1100 as cell opening aides for 2-cyanoacetamide or other similar molecules containing active methylene or methine groups to make a polyurethane foam is also disclosed. The advantage of using cell opener aids results in a) no foam shrinkage; b) lower use levels of cell opener; c) foam performance reproducibility d) optimum physical properties. In addition, combining the acid blocked amine catalyst together with the cell opener and the cell opener aid results in a less corrosive mixture as well as provides a method that does not require mechanical crushing for cell opening.
摘要翻译：公开了用于制备柔性聚氨酯泡沫，特别是柔性模塑聚氨酯泡沫的组合物和方法。使用偶极非质子液体如DMSO，DMI，环丁砜，N-甲基 - 乙酰乙酰胺，N，N-二甲基乙酰乙酰胺以及含有羟基数OH＃＆amp; 1100的二醇作为2-氰基乙酰胺或其它类似分子的开放助剂还公开了制备聚氨酯泡沫的活性亚甲基或次甲基。使用细胞开放助剂的优点导致a）没有泡沫收缩; b）细胞开放剂的使用水平较低; c）泡沫性能重现性d）最佳物理性能。此外，将酸封闭的胺催化剂与开孔剂和开孔剂组合在一起导致较少的腐蚀性混合物，并且提供了不需要机械破碎以进行开孔的方法。

5. 发明授权

US4049591A Foams and elastomers prepared in the presence of high tertiary amine content polyurethane catalysts 失效
标题翻译：在高叔胺含量的聚氨酯催化剂存在下制备的泡沫和弹性体
公开(公告)号：US4049591A
公开(公告)日：1977-09-20
申请号：US733548
申请日：1976-10-18
申请人： Edward E. McEntire , George P. Speranza
发明人： Edward E. McEntire , George P. Speranza
IPC分类号： C08G18/18 , C08G18/14 , C08G18/48
CPC分类号： C08G18/1841 , C08G18/185
摘要： Covers compounds of the formula ##STR1## where R" is lower alkyl, R is hydrogen or lower alkyl and Y is selected from the group consisting of CN, CONH.sub.2, CO.sub.2 R', CONR'.sub.2 and COR' where R' independently is hydrogen, lower alkyl or aryl. Also covers a method of producing a polyurethane by utilizing said above compounds as catalysts in reacting an organic polyisocyanate with an organic polyester polyol or polyether polyol in the presence of said catalyst.
摘要翻译：包括式“IMAGE”的化合物，其中R“为低级烷基，R为氢或低级烷基，Y选自CN，CONH 2，CO 2 R'，CONR'2和COR'，其中R'独立地为氢，低级烷基或芳基。还涉及在所述催化剂存在下，通过利用上述化合物作为有机多异氰酸酯与有机聚酯多元醇或聚醚多元醇反应的催化剂制备聚氨酯的方法。

6. 发明授权

US4038210A Beta-amino nitrile catalysts for polyurethane preparation 失效
标题翻译：用于聚氨酯制备的BETA-AMINO NITRILE催化剂
公开(公告)号：US4038210A
公开(公告)日：1977-07-26
申请号：US596628
申请日：1975-07-17
申请人： Walter Richard Rosemund , Michael Ray Sandner , David John Trecker
发明人： Walter Richard Rosemund , Michael Ray Sandner , David John Trecker
IPC分类号： C08G18/18 , C08G18/40 , B01J31/02
CPC分类号： C08G18/185 , C08G18/4009
摘要： Cellular urethane polymers essentially free of the strong, objectionable amine odor characteristic of N-ethylmorpholine, are provided by effecting the polyurethane forming reaction in the presence of beta-tertamino nitriles. In view of their low residual odor and effectiveness in the catalysis of the water-isocyanate reaction, the beta-amino nitriles either alone or in combination with other tertiary amines, are used with particular advantage as direct replacements for N-ethylmorpholine in the manufacture of water-blown flexible polyurethanes, both molded and free-rise, including high-resilience foam as well as foams stabilized with either organosilicone or silicon-free organic surfactants. Especially effective for the formation of flexible polyester foam stabilized with either type of surfactant are blends of the beta-amino nitrile catalyst such as, in particular, 3-(N,N-dimethylamino)propionitrile, with dimethylethanolamine or a bis[2-(N,N-dimethylamino)alkyl]-ether.

7. 发明授权

US3925268A Beta-amino nitrile catalysts for polyurethane preparation 失效
标题翻译：用于聚氨酯制备的BETA-AMINO NITRILE催化剂
公开(公告)号：US3925268A
公开(公告)日：1975-12-09
申请号：US36955673
申请日：1973-06-13
申请人： UNION CARBIDE CORP
发明人： ROSEMUND WALTER RICHARD , SANDNER MICHAEL RAY , TRECKER DAVID JOHN
IPC分类号： C08G18/00 , C08F4/00 , C08G18/18 , C08G18/40 , C08G18/63 , C08G18/14 , C08G18/20
CPC分类号： C08G18/632 , C08G18/185 , C08G18/4009 , C08G18/4072 , Y10S521/904
摘要： Cellular urethane polymers essentially free of the strong, objectionable amine odor characteristic of N-ethylmorpholine, are provided by effecting the polyurethane forming reaction in the presence of beta-tert-amino nitriles. In view of their low residual odor and effectiveness in the catalysis of the waterisocyanate reaction, the beta-amino nitriles either alone or in combination with other tertiary amines, are used with particular advantage as direct replacements for N-ethyl-morpholine in the manufacture of water-blown flexible polyurethanes, both molded and free-rise, including high-resilience foam as well as foams stabilized with either organosilicone or silicon-free organic surfactants. Especially effective for the formation of flexible polyester foam stabilized with either type of surfactant are blends of the beta-amino nitrile catalyst such as, in particular, 3-(N,N-dimethylamino)propionitrile, with dimethylethanolamine or a bis(2-(N,N-dimethylamino)alkyl)-ether.

8. 发明授权

US10059823B2 Additives for improving polyurethane foam performance 有权
公开(公告)号：US10059823B2
公开(公告)日：2018-08-28
申请号：US14851081
申请日：2015-09-11
申请人： Evonik Degussa GmbH
发明人： Juan Jesus Burdeniuc , James Douglas Tobias , Renee Jo Keller , You-Moon Jeon
IPC分类号： C08J9/00 , C08G18/16 , C08G18/18 , C08G18/40 , C08G18/65 , C08G18/08 , C08G101/00
CPC分类号： C08J9/0028 , C08G18/0838 , C08G18/16 , C08G18/185 , C08G18/4072 , C08G18/6552 , C08G2101/00 , C08G2101/0008 , C08J9/0033 , C08J9/0042 , C08J2205/05 , C08J2375/04 , C08J2375/08
摘要： A composition and process useful to make flexible polyurethane foams and in particular flexible molded polyurethane foams is disclosed. The usage of dipolar aprotic liquids such as DMSO, DMI, sulfolane, N-methyl-acetoacetamide, N,N-dimethylacetoacetamide as well as glycols containing hydroxyl numbers OH#≤1100 as cell opening aides for 2-cyanoacetamide or other similar molecules containing active methylene or methine groups to make a polyurethane foam is also disclosed. The advantage of using cell opener aids results in a) no foam shrinkage; b) lower use levels of cell opener; c) foam performance reproducibility d) optimum physical properties. In addition, combining the acid blocked amine catalyst together with the cell opener and the cell opener aid results in a less corrosive mixture as well as provides a method that does not require mechanical crushing for cell opening.

9. 发明授权

US09334382B2 Process for producing flexible polyurethane foam 有权
标题翻译：生产柔性聚氨酯泡沫的方法
公开(公告)号：US09334382B2
公开(公告)日：2016-05-10
申请号：US13178562
申请日：2011-07-08
申请人： Juan Jesus Burdeniuc , James Douglas Tobias , You-Moon Jeon , Renee Jo Keller
发明人： Juan Jesus Burdeniuc , James Douglas Tobias , You-Moon Jeon , Renee Jo Keller
IPC分类号： C08J9/00 , C08G18/16 , C08G18/18 , C08G18/40 , C08G18/65 , C08G18/08 , C08G101/00
CPC分类号： C08J9/0028 , C08G18/0838 , C08G18/16 , C08G18/185 , C08G18/4072 , C08G18/6552 , C08G2101/00 , C08G2101/0008 , C08J9/0033 , C08J9/0042 , C08J2205/05 , C08J2375/04 , C08J2375/08
摘要： A composition and process useful to make flexible polyurethane foams and in particular flexible molded polyurethane foams is disclosed. The usage of dipolar aprotic liquids such as DMSO, DMI, sulfolane, N-methyl-acetoacetamide, N,N-dimethylacetoacetamide as well as glycols containing hydroxyl numbers OH#≦1100 as cell opening aides for 2-cyanoacetamide or other similar molecules containing active methylene or methine groups to make a polyurethane foam is also disclosed. The advantage of using cell opener aids results in a) no foam shrinkage; b) lower use levels of cell opener; c) foam performance reproducibility d) optimum physical properties. In addition, combining the acid blocked amine catalyst together with the cell opener and the cell opener aid results in a less corrosive mixture as well as provides a method that does not require mechanical crushing for cell opening.
摘要翻译：公开了用于制备柔性聚氨酯泡沫，特别是柔性模塑聚氨酯泡沫的组合物和方法。使用偶极非质子液体如DMSO，DMI，环丁砜，N-甲基 - 乙酰乙酰胺，N，N-二甲基乙酰乙酰胺以及含有羟基数OH＃＆amp; 1100的二醇作为2-氰基乙酰胺或其它类似分子的细胞开放助剂还公开了制备聚氨酯泡沫的活性亚甲基或次甲基。使用细胞开放助剂的优点导致a）没有泡沫收缩; b）细胞开放剂的使用水平较低; c）泡沫性能重现性d）最佳物理性能。此外，将酸封闭的胺催化剂与开孔剂和开孔剂组合在一起导致较少的腐蚀性混合物，并且提供了不需要机械破碎以进行开孔的方法。

10. 发明申请

US20120178839A1 Process For Producing Flexible Polyurethane Foam 有权
标题翻译：生产柔性聚氨酯泡沫的方法
公开(公告)号：US20120178839A1
公开(公告)日：2012-07-12
申请号：US13178562
申请日：2011-07-08
申请人： Juan Jesus Burdeniuc , James Douglas Tobias , You-Moon Jeon , Renee Jo Keller
发明人： Juan Jesus Burdeniuc , James Douglas Tobias , You-Moon Jeon , Renee Jo Keller
IPC分类号： C08J9/00 , C09K3/00
CPC分类号： C08J9/0028 , C08G18/0838 , C08G18/16 , C08G18/185 , C08G18/4072 , C08G18/6552 , C08G2101/00 , C08G2101/0008 , C08J9/0033 , C08J9/0042 , C08J2205/05 , C08J2375/04 , C08J2375/08
摘要： A composition and process useful to make flexible polyurethane foams and in particular flexible molded polyurethane foams is disclosed. The usage of dipolar aprotic liquids such as DMSO, DMI, sulfolane, N-methyl-acetoacetamide, N,N-dimethylacetoacetamide as well as glycols containing hydroxyl numbers OH#≦1100 as cell opening aides for 2-cyanoacetamide or other similar molecules containing active methylene or methine groups to make a polyurethane foam is also disclosed. The advantage of using cell opener aids results in a) no foam shrinkage; b) lower use levels of cell opener; c) foam performance reproducibility d) optimum physical properties. In addition, combining the acid blocked amine catalyst together with the cell opener and the cell opener aid results in a less corrosive mixture as well as provides a method that does not require mechanical crushing for cell opening.
摘要翻译：公开了用于制备柔性聚氨酯泡沫，特别是柔性模塑聚氨酯泡沫的组合物和方法。使用偶极非质子液体如DMSO，DMI，环丁砜，N-甲基 - 乙酰乙酰胺，N，N-二甲基乙酰乙酰胺以及含有羟基数OH＃＆amp; 1100的二醇作为2-氰基乙酰胺或其它类似分子的细胞开放助剂还公开了制备聚氨酯泡沫的活性亚甲基或次甲基。使用细胞开放助剂的优点导致a）没有泡沫收缩; b）细胞开放剂的使用水平较低; c）泡沫性能重现性d）最佳物理性能。此外，将酸封闭的胺催化剂与开孔剂和开孔剂组合在一起导致较少的腐蚀性混合物，并且提供了不需要机械破碎以进行开孔的方法。

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