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21. 发明授权

US07364908B2 Separation of fluorous compounds 有权
标题翻译：氟化合物的分离
公开(公告)号：US07364908B2
公开(公告)日：2008-04-29
申请号：US10870514
申请日：2004-06-17
申请人： Dennis P. Curran , Masato Matsugi , Marvin S. Yu
发明人： Dennis P. Curran , Masato Matsugi , Marvin S. Yu
IPC分类号： G01N37/00 , G01N33/22 , C07C19/08 , C07C17/266
CPC分类号： C07C17/263 , C07B39/00 , C07C17/38 , C07C21/18 , C07C22/08 , C07C67/56 , Y10T436/13 , Y10T436/19 , C07C69/63
摘要： A method of separating at least a first non-fluorous compound from a mixture of compounds including at least the first non-fluorous compound and a second fluorous compound includes: charging the of compounds to a non-fluorous solid (stationary) phase and eluting with a fluorous eluting fluid (mobile phase). In one embodiment, the non-fluorous solid phase is polar in nature. The method can further include a second phase elution with a suitable organic solvent. A method conducting a chemical reaction, includes: mixing at least a first fluorous compound and a second compound, the first fluorous compound differing in fluorous nature from the second compound; exposing the first mixture to conditions to convert at least one of the first fluorous compound and the second compound to give a second mixture containing at least a third compound, charging the second mixture to a non-fluorous solid phase; and eluting with a fluorous fluid.
摘要翻译：从至少包含第一非氟化合物和第二氟化合物的化合物的混合物中分离至少第一非氟化合物的方法包括：将化合物装入非氟固体（固定）相并用氟洗脱液（流动相）。在一个实施方案中，非氟固体本质上是极性的。该方法还可以包括用合适的有机溶剂进行第二相洗脱。进行化学反应的方法包括：将至少第一氟化合物和第二化合物混合，所述第一氟化合物与所述第二化合物不同; 将第一混合物暴露于转化至少一种第一种氟化合物和第二种化合物的条件以产生含有至少第三种化合物的第二混合物，将第二种混合物装入非氟固体; 并用氟液洗脱。

22. 发明申请

US20080087879A1 Tetrasubstituted coronenes 失效
标题翻译：四取代的冠醚
公开(公告)号：US20080087879A1
公开(公告)日：2008-04-17
申请号：US11580386
申请日：2006-10-13
申请人： Alex Sergey Ionkin , Ying Wang
发明人： Alex Sergey Ionkin , Ying Wang
IPC分类号： H01L51/00 , C07C15/20 , H01L51/54
CPC分类号： C07C15/20 , C07C17/25 , C07C17/263 , C07C22/08 , C07C25/22 , C07C2603/54 , H01L51/0056 , H01L51/5012 , Y10S428/917
摘要： Tetrasubstituted coronenes are provided. Also provided are electronic devices in which the active layer includes a tetrasubstituted coronene.
摘要翻译：提供了四取代的冠醚。还提供了其中活性层包含四取代的冠烯的电子器件。

23. 发明申请

US20080033171A1 Ligands for Metals and Improved Metal-Catalyzed Processes Based Thereon 有权
标题翻译：金属配体和改进的金属催化工艺
公开(公告)号：US20080033171A1
公开(公告)日：2008-02-07
申请号：US11781651
申请日：2007-07-23
申请人： Stephen Buchwald , David Old , John Wolfe , Michael Palucki , Ken Kamikawa
发明人： Stephen Buchwald , David Old , John Wolfe , Michael Palucki , Ken Kamikawa
IPC分类号： C07D295/00 , C07D211/70 , C07F7/04 , C07F9/02
CPC分类号： C07C1/26 , C07C1/321 , C07C17/16 , C07C17/263 , C07C29/32 , C07C29/38 , C07C37/18 , C07C41/30 , C07C45/68 , C07C45/71 , C07C49/675 , C07C67/31 , C07C201/12 , C07C209/10 , C07C209/18 , C07C211/59 , C07C213/02 , C07C213/08 , C07C221/00 , C07C225/12 , C07C227/08 , C07C227/18 , C07C231/08 , C07C231/12 , C07C249/02 , C07C249/16 , C07C251/24 , C07C253/30 , C07C2531/24 , C07C2531/26 , C07C2601/02 , C07C2601/08 , C07C2601/14 , C07C2601/16 , C07C2602/08 , C07C2602/10 , C07D209/08 , C07D213/50 , C07D213/72 , C07D213/74 , C07D295/023 , C07D295/033 , C07D295/096 , C07D295/112 , C07D295/13 , C07D295/155 , C07D307/33 , C07D317/22 , C07D317/26 , C07D317/66 , C07D333/08 , C07D333/66 , C07D401/04 , C07F7/1892 , C07F9/4875 , C07F9/5022 , C07F9/5027 , C07F9/5728 , C07F9/653 , C07F9/6547 , C07F9/65719 , C07F15/0066 , C07C25/18 , C07C49/255 , C07C49/213 , C07C49/657 , C07C49/67 , C07C49/84 , C07C49/245 , C07C49/755 , C07C49/215 , C07C49/683 , C07C47/575 , C07C49/782 , C07C69/92 , C07C211/48 , C07C211/55 , C07C217/40 , C07C217/84 , C07C217/92 , C07C225/22 , C07C229/36 , C07C229/60 , C07C233/07 , C07C235/46 , C07C251/86 , C07C255/33 , C07C255/50 , C07C255/54 , C07C255/56 , C07C255/58 , C07C15/14 , C07C35/21 , C07C33/24 , C07C205/04 , C07C205/06 , C07C43/205 , C07C43/225 , C07C39/15 , C07C35/08
摘要： One aspect of the present invention relates to novel ligands for transition metals. A second aspect of the present invention relates to the use of catalysts comprising these ligands in transition metal-catalyzed carbon-heteroatom and carbon-carbon bond-forming reactions. The subject methods provide improvements in many features of the transition metal-catalyzed reactions, including the range of suitable substrates, reaction conditions, and efficiency.
摘要翻译：本发明的一个方面涉及用于过渡金属的新配体。本发明的第二方面涉及包含这些配体的催化剂在过渡金属催化的碳 - 杂原子和碳 - 碳键形成反应中的用途。本发明方法提供了过渡金属催化反应的许多特征的改进，包括合适底物的范围，反应条件和效率。

24. 发明申请

US20070298501A1 Congeneric, Chlorinated, Brominated And/Or Iodised, Fluorinated Aromatic Compounds Comprising Two Benzol Rings In Their Basic Structure, Method For Their Production And Use Thereof 审中-公开
标题翻译：包含两个苯环在其基本结构中的同系，氯化，溴化和/或碘化的氟化芳族化合物，其生产和使用方法
公开(公告)号：US20070298501A1
公开(公告)日：2007-12-27
申请号：US10589597
申请日：2005-02-16
申请人： Huiling Liu , Gregor Luthe , Jon Johnsen
发明人： Huiling Liu , Gregor Luthe , Jon Johnsen
IPC分类号： C07C22/08 , C07C17/00 , C07D307/91 , C07D319/24 , G01N31/00
CPC分类号： C07C43/29 , C07C17/12 , C07C17/263 , C07C17/269 , C07C25/18 , C07D307/91 , C07D319/24 , Y10T436/10 , Y10T436/19 , Y10T436/193333 , Y10T436/196666 , Y10T436/24
摘要： Congeneric, halogenated, fluorinated aromatic compounds where A and B are each phenyl radicals, L=oxygen atom, sulfur atom or alkylene radical and p=0 or 1; processes for their preparation and their use.
摘要翻译：其中A和B各自为苯基，L =氧原子，硫原子或亚烷基，p = 0或1的同系卤代氟化芳族化合物; 其准备和使用过程。

25. 发明申请

US20070010683A1 Carbon-carbon bond creation method comprising the coupling of a transferable group and an acceptor group 失效
标题翻译：包括可转移基团和受体基团的偶联的碳 - 碳键的制备方法
公开(公告)号：US20070010683A1
公开(公告)日：2007-01-11
申请号：US10569941
申请日：2004-08-24
申请人： Johann Vastra
发明人： Johann Vastra
IPC分类号： C07C67/00
CPC分类号： B01J31/1805 , B01J2531/824 , C07B37/04 , C07C1/321 , C07C17/263 , C07C41/30 , C07C2531/22 , C07C15/14 , C07C22/08 , C07C43/205
摘要： The invention relates to a carbon-carbon bond creation method comprising the coupling of a transferable group and an acceptor group. The inventive method comprises the following steps: a) activation of a siliceous compound bearing a transferable group by an activation agent; b) addition of an acceptor group-bearing derivative; and, simultaneously or in any consecutive order, c) addition of a palladacycle-type compound acting as a catalyst of the coupling reaction between the transferable group and the acceptor group with the creation of the carbon-carbon bond.
摘要翻译：本发明涉及包含可转移基团和受体基团的偶联的碳 - 碳键的制备方法。本发明的方法包括以下步骤：a）通过活化剂活化带有可转移基团的硅质化合物; b）加入受体基团衍生物; 并且同时或以任何连续的顺序，c）添加作为可转移基团和受体基团之间的偶联反应的催化剂的帕拉多环型化合物，并产生碳 - 碳键。

26. 发明申请

US20060224011A1 Catalyst composition and process for producing cross-coupled compound using same 有权
标题翻译：催化剂组合物和使用其制备交联化合物的方法
公开(公告)号：US20060224011A1
公开(公告)日：2006-10-05
申请号：US11391567
申请日：2006-03-29
申请人： Shinichi Ishikawa , Hiroshi Awano , Hirokazu Yano , Hisao Equchi
发明人： Shinichi Ishikawa , Hiroshi Awano , Hirokazu Yano , Hisao Equchi
IPC分类号： C07C69/76
CPC分类号： C07C41/30 , B01J31/1805 , B01J31/2404 , B01J2231/4211 , B01J2531/847 , C07B37/04 , C07C1/321 , C07C17/263 , C07C43/215 , C07C253/30 , C07F15/045 , C07C15/52 , C07C15/14 , C07C22/08 , C07C255/54 , C07C43/205
摘要： A catalyst composition for a cross-coupling reaction comprising a nickel salt-amine complex of formula (1), and triphenylphosphine. where R1 thru R4 independently represent alkyl, aryl, heteroaryl or alkenyl; n is an integer of 1-6; and X independently represents halo, hydroxyl, nitrate or acetate group. Using the catalyst composition, a cross-coupling reaction is carried out between a boron-containing compound of formula (2) and a compound of formula (3). where R5 and R6 are the same as R1-R4 defined above; Y independently represents hydroxyl or alkoxy, Z is halo, methanesulfonate or trifluoromethanesulfonate.
摘要翻译：包含式（1）的镍盐 - 胺络合物和三苯基膦的用于交叉偶联反应的催化剂组合物。其中R 1至R 4独立地代表烷基，芳基，杂芳基或烯基; n为1-6的整数; X独立地表示卤素，羟基，硝酸根或乙酸基。使用催化剂组合物，在式（2）的含硼化合物和式（3）的化合物之间进行交叉偶联反应。其中R 5和R 6与上述R 1〜R 4相同; Y独立地表示羟基或烷氧基，Z是卤素，甲磺酸酯或三氟甲磺酸酯。

27. 发明授权

US07026409B2 Polymer-supported arylbis(perfluoroalkylsulfonyl)-methane 失效
标题翻译：聚合物负载的芳基双（全氟烷基磺酰基） - 甲烷
公开(公告)号：US07026409B2
公开(公告)日：2006-04-11
申请号：US10471447
申请日：2002-03-12
申请人： Kazuaki Ishihara , Hisashi Yamamoto
发明人： Kazuaki Ishihara , Hisashi Yamamoto
IPC分类号： C08C19/20
CPC分类号： B01J31/0224 , B01J31/06 , B01J31/10 , B01J2231/342 , B01J2231/346 , B01J2231/348 , B01J2231/40 , B01J2231/44 , C07B2200/11 , C07C17/14 , C07C17/263 , C07C29/38 , C07C41/56 , C07C45/511 , C07C45/64 , C07C45/673 , C07C67/08 , C07C2601/14 , C07C25/18 , C07C49/83 , C07C69/78 , C07C43/303 , C07C33/30
摘要： The present invention provides a solid acid catalyst that is excellent from the point of toxicity, environment and others, wherein reaction can be progressed effectively with Bronsted acid or Lewis acid catalyst. For example, the benzoylation reaction of alcohol can also be progressed easily, and further, the catalyst can be recovered and recycled easily. The para position of arylbis(perfluoroalkylsulfonyl)methane represented by the general formula [1] (wherein R1 shows a substituted or unsubstituted aryl group, Rf1 and Rf2 are independent to each other and show a perfluoroalkyl group), a pentafluorophenylbis(perfluoroalkylsulfonyl)methane, for example, is supported on a polystyrene resin, and a polystyrene-supported arylbis(perfluoroalkylsulfonyl)methane represented by the general formula [3] (wherein R3 shows a substituted or unsubstituted arylene group, Rf1 and Rf2 are the same as described above) is obtained.
摘要翻译：本发明提供从毒性，环境等方面优异的固体酸催化剂，其中可以使用布朗斯台德酸或路易斯酸催化剂有效地进行反应。例如，醇的苯甲酰化反应也可以容易地进行，此外，可以容易地回收和回收催化剂。由通式[1]表示的芳基双（全氟烷基磺酰基）甲烷的对位（其中R 1表示取代或未取代的芳基，Rf 1和R f） 2个彼此独立并且表示全氟烷基），五氟苯基双（全氟烷基磺酰基）甲烷例如负载在聚苯乙烯树脂上，由通式[D]表示的聚苯乙烯担载的芳基双（全氟烷基磺酰基）甲烷， 3]（其中R 3表示取代或未取代的亚芳基，Rf 1和R 2 2与上述相同）。

28. 发明授权

US06969693B2 Immobilised ionic liquids 失效
标题翻译：固定离子液体
公开(公告)号：US06969693B2
公开(公告)日：2005-11-29
申请号：US10138511
申请日：2002-05-06
申请人： Emmanuelle Sauvage , Michael H Valkenberg , Christovao P De Castro-Moreira , Wolfgang F Hoelderich
发明人： Emmanuelle Sauvage , Michael H Valkenberg , Christovao P De Castro-Moreira , Wolfgang F Hoelderich
IPC分类号： B01J31/30 , B01J31/02 , B01J31/16 , B01J37/02 , C07B39/00 , C07B61/00 , C07C2/66 , C07C2/68 , C07C15/107 , C07C15/24 , C07C17/26 , C07C37/14 , C07C39/06 , C07C45/45 , C07C45/46 , C07C49/84 , G01J31/00
CPC分类号： C07C2/68 , B01J31/0295 , B01J31/1608 , B01J37/0207 , B01J37/0209 , B01J2231/4205 , C07B39/00 , C07C17/263 , C07C37/14 , C07C41/06 , C07C45/455 , C07C45/46 , C07C15/107 , C07C49/84 , C07C39/06 , C07C43/205
摘要： Ionic liquids are immobilized on a functionalized support which carries or contains one component of the ionic liquid, or a precursor to such a component. The ionic liquid may be immobilized via the anion by treating a support with an anion source, e.g., an inorganic halide, before the ionic liquid is applied or formed. Alternatively, the ionic liquid may be immobilized by having the cation covalently bound to the support, e.g., through silyl groups, or incorporated in the support by synthesizing the support in the presence of a suitable base. The immobilized ionic liquids are of use as catalysts, for example, for the Friedel-Crafts reaction, such as alkylation reaction.
摘要翻译：离子液体被固定在携带或含有离子液体的一种组分的官能化载体上，或这种组分的前体。离子液体可以在施加或形成离子液体之前通过用阴离子源（例如无机卤化物）处理载体通过阴离子固定。或者，离子液体可以通过使阳离子与载体共价键合而固定，例如通过甲硅烷基，或通过在合适的碱的存在下合成载体而引入到载体中。固定化的离子液体可用作催化剂，例如用于Friedel-Crafts反应，如烷基化反应。

29. 发明申请

US20050197514A1 Highly branched perfluoroolefins, super-stable perfluoroalkyl radicals and production methods thereof 审中-公开
标题翻译：高分支全氟烯烃，超稳定全氟烷基及其制备方法
公开(公告)号：US20050197514A1
公开(公告)日：2005-09-08
申请号：US11123035
申请日：2005-05-06
申请人： Taizo Ono , Masakazu Nishida , Masaharu Okazaki , Kazumi Toriyama , Tetsuo Shimizu
发明人： Taizo Ono , Masakazu Nishida , Masaharu Okazaki , Kazumi Toriyama , Tetsuo Shimizu
IPC分类号： C07B61/00 , C07C17/04 , C07C17/26 , C07C17/263 , C07C19/08 , C07C21/18
CPC分类号： C07C17/04 , C07C17/263 , C07C19/08 , C07C21/18
摘要： The present invention is to provide a method for producing a highly branched perfluoroolefin conveniently in a high yield, a novel highly branched perfluoroolefin, a method for producing a super-stable perfluoroalkyl radical and a novel super-stable perfluoroalkyl radical. The present invention is a production method of a perfluoroolefin which comprises reacting a hexafluoropropene trimer with a trialkylperfluoroalkylsilane in an aprotic polar solvent using a fluoride ion as a catalyst.
摘要翻译：本发明提供一种以高产率方便地制备高支化全氟烯烃的方法，一种新型高支化全氟烯烃，一种制备超稳定全氟烷基的方法和一种新的超稳定全氟烷基。本发明是一种全氟烯烃的制造方法，其特征在于，使用氟离子作为催化剂，使六氟丙烯三聚物与三烷基全氟烷基硅烷在非质子极性溶剂中反应。

30. 发明申请

US20050065033A1 Method to inhibit ethylene responses in plants 审中-公开
标题翻译：抑制植物乙烯反应的方法
公开(公告)号：US20050065033A1
公开(公告)日：2005-03-24
申请号：US10645431
申请日：2003-08-21
申请人： Richard Jacobson , Martha Kelly , Fiona Wehmeyer , Karen Evans
发明人： Richard Jacobson , Martha Kelly , Fiona Wehmeyer , Karen Evans
IPC分类号： A01N27/00 , A01N29/04 , A01N31/14 , A01N33/06 , A01N37/10 , A01N37/18 , A01N37/42 , A01N41/04 , A01N43/08 , A01N43/10 , A01N43/12 , A01N43/32 , A01N43/36 , A01N43/40 , A01N43/50 , A01N43/54 , A01N43/56 , A01N43/60 , A01N43/653 , A01N43/80 , A01N43/82 , A01N55/00 , A01N55/08 , A01N55/10 , A01N57/12 , C07C13/04 , C07C17/00 , C07C17/23 , C07C17/25 , C07C17/26 , C07C17/275 , C07C17/278 , C07C23/18 , C07C43/215 , C07C43/225 , C07C43/23 , C07C45/00 , C07C45/29 , C07C211/55 , C07C309/73 , C07C321/10 , C07C323/09 , C07D207/16 , C07D213/70 , C07D231/16 , C07D233/54 , C07D237/14 , C07D249/12 , C07D307/68 , C07D317/12 , C07D333/08 , C07F7/08 , C07F7/18 , C07F9/177 , A01N25/26 , A01N47/40 , A01N35/00 , A01N35/10
CPC分类号： C07D213/70 , A01N27/00 , A01N29/04 , A01N31/14 , A01N33/06 , A01N37/10 , A01N37/18 , A01N37/42 , A01N41/04 , A01N43/08 , A01N43/10 , A01N43/12 , A01N43/32 , A01N43/36 , A01N43/40 , A01N43/50 , A01N43/54 , A01N43/56 , A01N43/60 , A01N43/653 , A01N43/80 , A01N43/82 , A01N55/00 , A01N55/08 , A01N57/12 , C07C13/04 , C07C17/00 , C07C17/23 , C07C17/25 , C07C17/263 , C07C17/2632 , C07C17/275 , C07C17/278 , C07C23/18 , C07C43/215 , C07C43/225 , C07C43/23 , C07C45/00 , C07C45/29 , C07C211/55 , C07C309/73 , C07C321/10 , C07C323/09 , C07C2601/02 , C07D207/16 , C07D231/16 , C07D233/54 , C07D237/14 , C07D249/12 , C07D307/68 , C07D317/12 , C07D333/08 , C07F7/0805 , C07F7/1804 , C07F9/177 , C07C22/04 , C07C23/04 , C07C21/14 , C07C25/24 , C07C49/213 , C07C47/225
摘要： The present invention generally relates to methods of inhibiting ethylene responses in plants and plant materials, and particularly relates to methods of inhibiting various ethylene responses including plant maturation and degradation, by exposing plants to cyclopropene derivatives and compositions thereof wherein: 1) at least one substituent on the cyclopropene ring contains a carbocyclic or heterocyclic ring, or 2) . a substituent contains silicon, sulfur, phosphorous, or boron, or 3) least one substituent contains from one to four non-hydrogen atoms and at least one substituent contains more than four non-hydrogen atoms.
摘要翻译：本发明一般涉及在植物和植物材料中抑制乙烯应答的方法，特别涉及通过将植物暴露于环丙烯衍生物及其组合物来抑制各种乙烯应答（包括植物成熟和降解）的方法，其中：1）至少一个取代基在环丙烯环上含有碳环或杂环，或2）。取代基含有硅，硫，磷或硼，或3）至少一个取代基含有一至四个非氢原子，至少一个取代基含有四个以上的非氢原子。

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