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1. 发明授权

US08703986B1 Process for preparing 10-chloro-9, 10-dihydro-9-oxa-10-phosphaphenanthrene-10-oxide compound 有权
标题翻译：制备10-氯-9,10-二氢-9-氧杂-10-磷杂菲-10-氧化物化合物的方法
公开(公告)号：US08703986B1
公开(公告)日：2014-04-22
申请号：US13932111
申请日：2013-07-01
申请人： UFC Corporation
发明人： Yu-Chin Lee , Jen-Hai Liao , Sung-Chen Lo , Chu-Chun Wu
IPC分类号： C07F9/02
CPC分类号： C07F9/657181 , C07F9/65719
摘要： Provided is a process for preparing 10-chloro-9,10-dihydro-9-oxa-10-phosphaphenanthrene-10-oxide (DOPO-C) compound, the process having steps of: reacting a liquid chlorinating agent and 9,10-dihydro-10-hydroxy-9-oxa 10-phosphaphenanthrene 10-oxide compound represented by formula (B) to form a mixture, the mixture comprises DOPO-C compound represented by formula (A) and an unreacted liquid chlorinating agent, separating the DOPO-C compound and the unreacted liquid chlorinating agent from the mixture to obtain the DOPO-C compound; wherein X1, X2, and X3 are each independently selected from the group consisting of hydrogen atom, hydroxyl group, cyano group, sulfonic acid group, sulfonate ester group represented by —SO3R1, halogen atom, alkoxy group represented by —OR2, acyclic hydrocarbon group having 1 to 8 carbon atoms, cyclic alkyl group having 3 to 8 carbon atoms, aryl group, heteroaryl group, and arylalkyl group, wherein R1 and R2 are each an acyclic hydrocarbon group having 1 to 8 carbon atoms.
摘要翻译：本发明提供一种制备10-氯-9,10-二氢-9-氧杂-10-磷杂菲-10-氧化物（DOPO-C）化合物的方法，该方法具有以下步骤：使液体氯化剂与9,10- 由式（B）表示的二氢-10-羟基-9-氧杂10-磷杂菲10氧化物化合物以形成混合物，该混合物包含由式（A）表示的DOPO-C化合物和未反应的液体氯化剂，将DOPO -C化合物和未反应的液体氯化剂，得到DOPO-C化合物; 其中X 1，X 2和X 3各自独立地选自氢原子，羟基，氰基，磺酸基，-SO 3 R 1表示的磺酸酯基，卤素原子，-OR 2表示的烷氧基，无环烃基具有1至8个碳原子，具有3至8个碳原子的环状烷基，芳基，杂芳基和芳基烷基，其中R 1和R 2各自是具有1至8个碳原子的无环烃基。

2. 发明申请

US20120175573A1 COMPOSITIONS COMPRISING POLYPHOSPHONATES AND ADDITIVES THAT EXHIBIT AN ADVANTAGEOUS COMBINATION OF PROPERTIES, AND METHODS RELATED THERETO 审中-公开
标题翻译：包含有优势组合的聚磷酸酯和添加剂的组合物及其相关方法
公开(公告)号：US20120175573A1
公开(公告)日：2012-07-12
申请号：US13345539
申请日：2012-01-06
申请人： Dieter Freitag , Pin Go , Gad Stahl
发明人： Dieter Freitag , Pin Go , Gad Stahl
IPC分类号： C09K21/14 , C08K5/524 , C08K5/151 , C08K5/13
CPC分类号： C07F9/65719 , C07F9/4056 , C07F9/6571 , C08K5/13
摘要： Disclosed are new compositions consisting of polyphosphonates and specific additive compositions that exhibit superior resistance to degradation due to exposure to air, high temperature and air, moisture or combinations thereof. Also disclosed are polymer mixtures or blends comprising these polyphosphonates/additive compositions and commodity and engineering plastics and articles produced therefrom. Further disclosed are articles of manufacture produced from these materials, such as fibers, films, coated substrates, moldings, foams, fiber-reinforced articles, or any combination thereof.
摘要翻译：公开了由多聚膦酸盐和特定添加剂组合物组成的新组合物，其显示出优异的抗暴露于空气，高温和空气，水分或其组合的降解性。还公开了包含这些聚膦酸盐/添加剂组合物的聚合物混合物或共混物以及由其制备的商品和工程塑料和制品。进一步公开的是由这些材料制成的制品，例如纤维，薄膜，涂覆的基材，模制品，泡沫，纤维增强制品或其任何组合。

3. 发明申请

US20120130126A1 Processes of Synthesizing Multi-Functional Phosphorus-Containing Epoxy Curing Agent 有权
标题翻译：合成多功能含磷环氧固化剂的工艺
公开(公告)号：US20120130126A1
公开(公告)日：2012-05-24
申请号：US13103046
申请日：2011-05-07
申请人： Wen-Chiung Su , Ching-Hsuan Lin , Hung-Tse Lin
发明人： Wen-Chiung Su , Ching-Hsuan Lin , Hung-Tse Lin
IPC分类号： C07F9/32
CPC分类号： C07F9/657172 , C07F9/65719
摘要： A series of curing agents are provided. The curing agents are multi-functional and phosphorus-containing. The curing agents have excellent processability to be used as an epoxy resin curing agent. The curing agents can be cured to obtain a phosphorus-containing epoxy thermoset with flame retardancy characteristic. The epoxy thermosets are very fit for circuit board substrate having high glass transition temperature; semiconductor packaging material; and related materials.
摘要翻译：提供一系列固化剂。固化剂是多功能和含磷的。固化剂具有优异的加工性能，可用作环氧树脂固化剂。固化剂可以固化，得到具有阻燃特性的含磷环氧热固性材料。环氧热固性材料非常适合具有高玻璃化转变温度的电路板基材; 半导体封装材料; 和相关材料。

4. 发明授权

US07714149B2 Chiral spiro compounds and their use in asymmetric catalytic reactions 失效
标题翻译：手性螺环化合物及其在不对称催化反应中的应用
公开(公告)号：US07714149B2
公开(公告)日：2010-05-11
申请号：US11218105
申请日：2005-09-01
申请人： Xumu Zhang
发明人： Xumu Zhang
IPC分类号： C07F9/6571 , C07F9/655 , C07D493/10
CPC分类号： C07C231/18 , C07D311/78 , C07D487/10 , C07D493/10 , C07D495/10 , C07F9/6561 , C07F9/657154 , C07F9/65719 , C07F9/65744 , C07C233/47 , C07C233/51
摘要： The present invention provides a chiral ligand, represented by a formula or its enantiomer: X and X′ can be independently O, NH, NR, NCOR or S; each of Z1-Z7 and Z1′-Z7′ can be independently H, alkyl, aryl, substituted alkyl, substituted aryl, alkoxyl, aryloxyl, nitro, amide, aryoxide, halide, hydroxyl, carboxylate, hetereoaryl, or a cyclic alkene, fused aryl, or cyclic ether group formed from any two adjacent Z groups or any two adjacent Z′ groups; Y and Y′ can be independently OH, OR, NH2, NHR, NR2, SH, PR2, OPR2, NHPR2, OP(OR)2, COOH, COOR, CONHR, or a linking group formed from Y and Y′ groups together. Processes of preparing these ligands, catalysts that employ them and methods of using the catalysts are also provided.
摘要翻译：本发明提供由式或其对映异构体表示的手性配体：X和X'可以独立地为O，NH，NR，NCOR或S; Z1-Z7和Z1'-Z7'可以独立地为H，烷基，芳基，取代的烷基，取代的芳基，烷氧基，芳氧基，硝基，酰胺，芳氧基，卤素，羟基，羧酸酯，杂芳基或环烯烃由任何两个相邻的Z基团或任何两个相邻的Z'基团形成的芳基或环醚基团; Y和Y'可以独立地是OH，OR，NH 2，NHR，NR 2，SH，PR 2，OPR 2，NHPR 2，OP（OR）2，COOH，COOR，CONHR或由Y和Y'基团形成的连接基团。还提供了制备这些配体的方法，使用它们的催化剂和使用催化剂的方法。

5. 发明授权

US07696349B2 Method for asymmetric synthesis 失效
标题翻译：不对称合成方法
公开(公告)号：US07696349B2
公开(公告)日：2010-04-13
申请号：US12237154
申请日：2008-09-24
申请人： Christoph Jäkel , Martin Volland , Thomas Mackewitz , Rocco Paciello , Bernhard Breit , Wolfgang Seiche , Martine Weis , Christoph Waloch
发明人： Christoph Jäkel , Martin Volland , Thomas Mackewitz , Rocco Paciello , Bernhard Breit , Wolfgang Seiche , Martine Weis , Christoph Waloch
IPC分类号： C07F9/80
CPC分类号： B01J31/18 , B01J31/182 , B01J31/1865 , B01J31/189 , B01J31/2273 , B01J31/2409 , B01J31/2452 , B01J31/2495 , B01J2231/32 , B01J2231/321 , B01J2231/323 , B01J2231/325 , B01J2231/326 , B01J2231/341 , B01J2231/342 , B01J2231/44 , B01J2231/52 , B01J2231/543 , B01J2231/645 , B01J2531/0266 , B01J2531/0291 , B01J2531/821 , B01J2531/822 , B01J2531/824 , B01J2531/827 , B01J2531/828 , B01J2531/842 , B01J2531/847 , C07B53/00 , C07F9/58 , C07F9/65719
摘要： The present invention relates to a process for asymmetric synthesis in the presence of a chiral catalyst comprising at least one complex of a metal of transition group VIII with ligands capable of dimerization via noncovalent bonds, such catalysts and their use.
摘要翻译：本发明涉及在手性催化剂存在下不对称合成的方法，其包含至少一个过渡基团VIII的金属与能够通过非共价键二聚的配体的复合物，以及它们的用途。

6. 发明授权

US07256302B2 Substituted paracyclophane derivatives in asymmetric catalysis 失效
标题翻译：非对称催化中的取代对环芳烃衍生物
公开(公告)号：US07256302B2
公开(公告)日：2007-08-14
申请号：US10560387
申请日：2004-06-08
申请人： Beatriz Dominguez , William Patrick Hems , Antonio Zanotti-Gerosa
发明人： Beatriz Dominguez , William Patrick Hems , Antonio Zanotti-Gerosa
IPC分类号： C07F9/30
CPC分类号： B01J31/2457 , B01J31/1608 , B01J2231/4211 , B01J2231/4261 , B01J2231/4283 , B01J2231/643 , B01J2231/645 , B01J2531/0263 , B01J2531/821 , B01J2531/822 , B01J2531/824 , B01J2531/827 , B01J2531/828 , C07B53/00 , C07B2200/07 , C07C29/145 , C07C39/42 , C07C47/55 , C07C49/813 , C07C63/72 , C07C69/76 , C07C205/12 , C07C231/18 , C07C2603/92 , C07F9/5027 , C07F9/65719 , C07F9/6581 , C07F15/0053 , C07C233/47 , C07C33/22 , C07C33/50
摘要： A substituted paracyclophane is described of formula (I) wherein X1 and X2 are linking groups comprising between 2 to 4 carbon atoms, Y1 and Y2 are selected from the group consisting of hydrogen, halide, oxygen, nitrogen, alkyl, cycloalkyl, aryl or heteroaryl, Z1, Z2 and Z3 are substituting groups that optionally contain functional groups, a, b, c, d, e and f are 0 or 1 and a+b+c+d+e+f=1 to 6. Preferably X1 and X2 are —(C2H4)— and a+b+c+d+e+f=1 or 2. The substituted paracyclophane provides transition metal catalysts that demonstrate high activity and selectivity for asymmetric reactions
摘要翻译：描述了式（I）的取代的对环芳烷，其中X 1和X 2 2是包含2至4个碳原子的连接基团，Y 1，和Y 2选自氢，卤素，氧，氮，烷基，环烷基，芳基或杂芳基，Z 1，Z 2， SUP>和Z 3是用任选含有官能团a，b，c，d，e和f分别为0或1和a + b + c + d + e + f = 1的基团 X 1和X 2优选为 - （C 2 H 4 H 4） - 和 - + b + c + d + e + f = 1或2.取代的对环烷烷提供过渡金属催化剂，其表现出对不对称反应的高活性和选择性

7. 发明申请

US20060069257A1 Ligands for metals and improved metal-catalyzed processes based thereon 有权
标题翻译：金属配体和基于其的改进的金属催化方法
公开(公告)号：US20060069257A1
公开(公告)日：2006-03-30
申请号：US11229043
申请日：2005-09-16
申请人： Stephen Buchwald , David Old , John Wolfe , Michael Palucki , Ken Kamikawa
发明人： Stephen Buchwald , David Old , John Wolfe , Michael Palucki , Ken Kamikawa
IPC分类号： C07F15/00 , C07F9/28 , C07C209/10
CPC分类号： C07C1/26 , C07C1/321 , C07C17/16 , C07C17/263 , C07C29/32 , C07C29/38 , C07C37/18 , C07C41/30 , C07C45/68 , C07C45/71 , C07C49/675 , C07C67/31 , C07C201/12 , C07C209/10 , C07C209/18 , C07C211/59 , C07C213/02 , C07C213/08 , C07C221/00 , C07C225/12 , C07C227/08 , C07C227/18 , C07C231/08 , C07C231/12 , C07C249/02 , C07C249/16 , C07C251/24 , C07C253/30 , C07C2531/24 , C07C2531/26 , C07C2601/02 , C07C2601/08 , C07C2601/14 , C07C2601/16 , C07C2602/08 , C07C2602/10 , C07D209/08 , C07D213/50 , C07D213/72 , C07D213/74 , C07D295/023 , C07D295/033 , C07D295/096 , C07D295/112 , C07D295/13 , C07D295/155 , C07D307/33 , C07D317/22 , C07D317/26 , C07D317/66 , C07D333/08 , C07D333/66 , C07D401/04 , C07F7/1892 , C07F9/4875 , C07F9/5022 , C07F9/5027 , C07F9/5728 , C07F9/653 , C07F9/6547 , C07F9/65719 , C07F15/0066 , C07C25/18 , C07C49/255 , C07C49/213 , C07C49/657 , C07C49/67 , C07C49/84 , C07C49/245 , C07C49/755 , C07C49/215 , C07C49/683 , C07C47/575 , C07C49/782 , C07C69/92 , C07C211/48 , C07C211/55 , C07C217/40 , C07C217/84 , C07C217/92 , C07C225/22 , C07C229/36 , C07C229/60 , C07C233/07 , C07C235/46 , C07C251/86 , C07C255/33 , C07C255/50 , C07C255/54 , C07C255/56 , C07C255/58 , C07C15/14 , C07C35/21 , C07C33/24 , C07C205/04 , C07C205/06 , C07C43/205 , C07C43/225 , C07C39/15 , C07C35/08
摘要： One aspect of the present invention relates to novel ligands for transition metals. A second aspect of the present invention relates to the use of catalysts comprising these ligands in transition metal-eatalyzed carbon-heteroatom and carbon-carbon bond-forming reactions. The subject methods provide improvements in many features of the transition metal-catalyzed reactions, including the range of suitable substrates, reaction conditions, and efficiency.
摘要翻译：本发明的一个方面涉及用于过渡金属的新配体。本发明的第二方面涉及包含这些配位体的催化剂在过渡金属分解的碳 - 杂原子和碳 - 碳键形成反应中的用途。本发明方法提供了过渡金属催化反应的许多特征的改进，包括合适底物的范围，反应条件和效率。

8. 发明授权

US06946560B2 Ligands for metals and improved metal-catalyzed processes based thereon 有权
标题翻译：金属配体和基于其的改进的金属催化方法
公开(公告)号：US06946560B2
公开(公告)日：2005-09-20
申请号：US10420950
申请日：2003-04-22
申请人： Stephen L. Buchwald , David W. Old , John P. Wolfe , Michael Palucki , Ken Kamikawa
发明人： Stephen L. Buchwald , David W. Old , John P. Wolfe , Michael Palucki , Ken Kamikawa
IPC分类号： C07C1/26 , C07C17/26 , C07C41/16 , C07C45/68 , C07C45/71 , C07C67/31 , C07C205/04 , C07C205/06 , C07C209/10 , C07C209/18 , C07C211/48 , C07C211/55 , C07C211/59 , C07C213/02 , C07C213/08 , C07C217/40 , C07C217/84 , C07C217/92 , C07C221/00 , C07C225/12 , C07C225/22 , C07C227/08 , C07C227/18 , C07C229/36 , C07C229/60 , C07C231/12 , C07C233/07 , C07C235/46 , C07C249/02 , C07C249/16 , C07C251/24 , C07C251/86 , C07C253/30 , C07C255/33 , C07C255/50 , C07C255/54 , C07C255/56 , C07C255/58 , C07D209/08 , C07D213/50 , C07D213/72 , C07D213/74 , C07D295/02 , C07D295/023 , C07D295/033 , C07D295/096 , C07D295/112 , C07D295/13 , C07D295/155 , C07D307/33 , C07D317/22 , C07D317/26 , C07D317/66 , C07D333/08 , C07D333/66 , C07D401/04 , C07F7/18 , C07F9/48 , C07F9/50 , C07F9/572 , C07F9/653 , C07F9/6547 , C07F9/6571 , C07F15/00 , C07D211/70 , C07C209/00 , C07D207/04
CPC分类号： C07C1/26 , C07C1/321 , C07C17/16 , C07C17/263 , C07C29/32 , C07C29/38 , C07C37/18 , C07C41/30 , C07C45/68 , C07C45/71 , C07C49/675 , C07C67/31 , C07C201/12 , C07C209/10 , C07C209/18 , C07C211/59 , C07C213/02 , C07C213/08 , C07C221/00 , C07C225/12 , C07C227/08 , C07C227/18 , C07C231/08 , C07C231/12 , C07C249/02 , C07C249/16 , C07C251/24 , C07C253/30 , C07C2531/24 , C07C2531/26 , C07C2601/02 , C07C2601/08 , C07C2601/14 , C07C2601/16 , C07C2602/08 , C07C2602/10 , C07D209/08 , C07D213/50 , C07D213/72 , C07D213/74 , C07D295/023 , C07D295/033 , C07D295/096 , C07D295/112 , C07D295/13 , C07D295/155 , C07D307/33 , C07D317/22 , C07D317/26 , C07D317/66 , C07D333/08 , C07D333/66 , C07D401/04 , C07F7/1892 , C07F9/4875 , C07F9/5022 , C07F9/5027 , C07F9/5728 , C07F9/653 , C07F9/6547 , C07F9/65719 , C07F15/0066 , C07C25/18 , C07C49/255 , C07C49/213 , C07C49/657 , C07C49/67 , C07C49/84 , C07C49/245 , C07C49/755 , C07C49/215 , C07C49/683 , C07C47/575 , C07C49/782 , C07C69/92 , C07C211/48 , C07C211/55 , C07C217/40 , C07C217/84 , C07C217/92 , C07C225/22 , C07C229/36 , C07C229/60 , C07C233/07 , C07C235/46 , C07C251/86 , C07C255/33 , C07C255/50 , C07C255/54 , C07C255/56 , C07C255/58 , C07C15/14 , C07C35/21 , C07C33/24 , C07C205/04 , C07C205/06 , C07C43/205 , C07C43/225 , C07C39/15 , C07C35/08
摘要： One aspect of the present invention relates to novel ligands for transition metals. A second aspect of the present invention relates to the use of catalysts comprising these ligands in transition metal-catalyzed carbon-heteroatom and carbon-carbon bond-forming reactions. The subject methods provide improvements in many features of the transition metal-catalyzed reactions, including the range of suitable substrates, reaction conditions, and efficiency.
摘要翻译：本发明的一个方面涉及用于过渡金属的新配体。本发明的第二方面涉及包含这些配体的催化剂在过渡金属催化的碳 - 杂原子和碳 - 碳键形成反应中的用途。本发明方法提供了过渡金属催化反应的许多特征的改进，包括合适底物的范围，反应条件和效率。

9. 发明申请

US20050184277A1 Method for preparing arylphosphonite antioxidant 有权
标题翻译：芳基亚膦酸酯抗氧化剂的制备方法
公开(公告)号：US20050184277A1
公开(公告)日：2005-08-25
申请号：US10983620
申请日：2004-11-09
申请人： Wen-Chiung Su , Tseng-Rong Wu , Chin-Shang Sheng
发明人： Wen-Chiung Su , Tseng-Rong Wu , Chin-Shang Sheng
IPC分类号： C07F9/6571 , C09K15/32
CPC分类号： C07F9/65719 , C09K15/322
摘要： A method for preparing an arylphosphonite antioxidant of the formula (I) below is disclosed, wherein Ar is First, the reactants 2-phenylphenol and phosphorus trichloride are heated under the existence of a zinc chloride catalyst for producing 6-chloro-6H-dibenz[c,e][1,2]oxaphosphorin (CDOP) of the formula (II) below: Next, the excess phosphorus trichloride is removed. Finally, an organic solution of a di-hydroxylphenol compound of the formula (III), Ar—(OH)2 (III) wherein Ar is defined as the above, is heated with the CDOP of formula (II) to form the product of the formula (I).
摘要翻译：公开了下述式（I）的芳基亚膦酸酯抗氧化剂的制备方法，其中Ar为首先，在存在氯化锌催化剂的情况下，将2-苯基苯酚和三氯化磷的反应物加热，生成6-氯-6H-二苯并[ c，e] [1,2]氧杂磷素（CDOP）：接下来，除去过量的三氯化磷。最后，将式（III）的二羟基苯酚化合物的有机溶液<？in-line-formula description =“In-line Formulas”end =“lead”→> Ar-（OH）（III）将式（Ⅱ）的CDOP与式（II）的CDOP一起加热，形成产物的式（I）。

10. 发明申请

US20050038278A1 Process for the preparation of 9, 10-dihydro-9-OXA-10-organyloxyphosphaphenanthrene-10-oxide or -thione and derivatives of the same substituted on the phenyl groups 失效
标题翻译：制备9,10-二氢-9-OXA-10-有机氧基菲啶-10-氧化物或硫代酮的方法及其在苯基上取代的衍生物
公开(公告)号：US20050038278A1
公开(公告)日：2005-02-17
申请号：US10918836
申请日：2004-08-13
申请人： Uwe Dittrich , Berthold Just , Manfred Doring , Michael Ciesielski
发明人： Uwe Dittrich , Berthold Just , Manfred Doring , Michael Ciesielski
IPC分类号： C07F9/6571 , C07F9/02
CPC分类号： C08K5/5313 , C07F9/657181 , C07F9/65719
摘要： A process is provided for the preparation of 9,10-dihydro-9-oxa-10-organyloxyphosphaphenanthrene-10-oxide or -thione and derivatives of same substituted on the phenyl groups, in which: (a) 9,10-dihydro-9-oxa-10-phosphaphenanthrene-10-oxide (DOP) or a derivative of same is reacted in the presence of at least one mono- or polyhydric alcohol with at least one ortho ester with formation of a first intermediate product, (b) the intermediate product from step (a) is optionally reacted with at least one further mono- or polyhydric alcohol with formation of a further intermediate product and (c) the intermediate product from steps (a) or (b) is transformed by addition of oxidation agent into 9,10-dihydro-9-oxa-10-organyloxyphosphaphenanthrene-10-oxide or -thione or a derivative of same substituted on the phenyl groups.
摘要翻译：提供了用于制备9,10-二氢-9-氧杂-10-有机氧基菲啶-10-氧化物或硫代酮及其在苯基上取代的相同衍生物的方法，其中：（a）9,10-二氢 - 9-氧杂-10-磷杂菲-10-氧化物（DOP）或其衍生物在至少一种一元醇或多元醇与至少一种原酸酯的存在下反应，形成第一中间产物，（b）来自步骤（a）的中间产物任选地与至少一种另外的一元醇或多元醇反应形成另外的中间产物，和（c）通过加入氧化来转化来自步骤（a）或（b）的中间产物试剂转化成9,10-二氢-9-氧杂-10-有机氧基亚磷酰-10-氧化物或硫代酮或其在苯基上取代的相同衍生物。

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