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1. 发明公开

US20230159416A1 DIFLUOROMETHYL IODO COMPOUNDS AND METHODS 审中-公开
公开(公告)号：US20230159416A1
公开(公告)日：2023-05-25
申请号：US17904477
申请日：2021-02-17
申请人： Recurium IP Holdings, LLC
发明人： Aditya Krishnan Unni , Joseph Robert Pinchman , Peter Qinhua Huang , Kevin Duane Bunker
IPC分类号： C07C17/363 , C07C17/275
CPC分类号： C07C17/363 , C07C17/275 , C07C2602/38
摘要： The present application is related to an improved process for synthesising 1-(difluoromethyl)-3-iodobicyclo[1.1.1]pentane from difluoromethyl iodide and [1.1.1]propellane. Difluoromethyl iodide is made by reacting an iodide salt with chlorodifluoroacetic acid in the presence of a solvent such as sulfolane and an inorganic base, [1.1.1]propellane is synthesised by reacting 1,1-dibromo-2,2-cis(chloromethyl)cyclopropane with a reagent such as magnesium, methyllithium or phenyllithium.

2. 发明授权

US10968187B2 Method for preparation of alkylated or fluoro, chloro and fluorochloro alkylated compounds by heterogeneous cobalt catalysis 有权
公开(公告)号：US10968187B2
公开(公告)日：2021-04-06
申请号：US16632572
申请日：2018-07-26
申请人： Lonza Ltd
发明人： Christoph Taeschler , Florencio Zaragoza Doerwald , Stefan Ellinger , Matthias Beller , Helfried Neumann , Florian Fischer
IPC分类号： C07D265/30 , B01J31/04 , C07C17/275 , C07C17/32 , C07C21/18 , C07D213/26 , C07D241/10 , C07D333/12 , C07D473/10 , C07C19/14 , C07C22/08 , C07C23/36
摘要： The invention discloses a method for preparation of alkylated, fluoro alkylated, chloro alkylated and fluorochloro alkylated compounds by a heterogeneous Co-catalysed alkylation or fluoro, chloro and fluorochloro alkylation with alkyl halides, fluoro alkyl halides, chloro alkyl halides or fluorochloro alkyl halides respectively.

3. 发明申请

US20210078923A1 METHOD FOR PRODUCTION OF A HALOGENATED ALKANE USING AN ABSORBER-REACTOR COMBINATION 有权
公开(公告)号：US20210078923A1
公开(公告)日：2021-03-18
申请号：US17041321
申请日：2019-04-02
申请人： BLUE CUBE IP LLC
发明人： John D. Myers , Max Tirtowidjojo , Marc Sell , Thomas Luebbe
IPC分类号： C07C17/275
摘要： The present invention provides improved processes for preparing halogenated alkanes. The processes comprise contacting at least one alkene, a halogenated alkene, or combinations thereof with a halogenated methane with at least one chlorine atom to form a liquid phase. This liquid phase is then contacted with at least one catalytic species which initiates the reaction with at least one alkene, a halogenated alkene, or combinations thereof with a halogenated methane with at least one chlorine atoms.

4. 发明申请

US20210061735A1 METHOD OF PRODUCING COMPOUND HAVING BUTADIENE SKELETON CONTAINING HYDROGEN AND FLUORINE AND/OR CHLORINE 有权
公开(公告)号：US20210061735A1
公开(公告)日：2021-03-04
申请号：US16959317
申请日：2019-02-01
申请人： KANTO DENKA KOGYO CO., LTD.
发明人： Wataru KASHIKURA , Yoshihiko IKETANI , Ryo KIMURA , Yukinobu SHIBUSAWA
IPC分类号： C07C17/275
摘要： An object of the present invention is to provide a simple, low-cost, and industrial method of producing a compound having a polyene skeleton containing hydrogen and fluorine and/or chlorine.
A method of producing a halogenated diene represented by formula (1): A1A2C═CA3-CA4═CA5A6[A1, A2, A5, and A6 are each independently hydrogen, fluorine, chlorine, a (perfluoro)alkyl group having 1 to 3 carbon atoms, or a (perfluoro)alkenyl group; A3 and A4 are each independently hydrogen, fluorine, or chlorine; at least one of A1 to A6 is hydrogen; at least one of A1 to A6 is fluorine or chlorine] comprises a step of subjecting the same or different halogenated olefin(s) represented by formula (2): A7A8C═CA9X[A7 and A8 are each independently hydrogen, fluorine, chlorine, a (perfluoro)alkyl group having 1 to 3 carbon atoms, or a (perfluoro)alkenyl group; A9 is each independently hydrogen, fluorine, or chlorine; X is bromine or iodine] to a coupling reaction in the presence of a zero-valent metal and a metal salt.

5. 发明授权

US10005705B2 Process for the production of fluorinated cyclobutane 有权
公开(公告)号：US10005705B2
公开(公告)日：2018-06-26
申请号：US15807033
申请日：2017-11-08
申请人： Honeywell International Inc.
发明人： Haridasan K. Nair , Rajiv Banavali , Yian Zhai , Glenn Matthies
IPC分类号： C07C17/275
CPC分类号： C07C17/275 , C07C2601/04 , Y02P20/582 , C07C23/06
摘要： The production of 1, 1, 2-trifluoro-2-(trifluoromethyl)cyclobutane (TFMCB). More specifically, the present invention relates to a process for making 1, 1, 2-trifluoro-2-(trifluoromethyl)cyclobutane via a continuous catalytic reaction from commercially available raw materials ethylene and hexafluoropropene.

6. 发明申请

US20180127447A1 METATHESIS CATALYSTS AND METHODS THEREOF 审中-公开
公开(公告)号：US20180127447A1
公开(公告)日：2018-05-10
申请号：US15816816
申请日：2017-11-17
申请人： Trustees of Boston College , Massachusetts Institute of Technology
发明人： Amir H. Hoveyda , Hanmo Zhang , Ming Joo Koh , Richard Royce Schrock
IPC分类号： C07F11/00 , C07C17/361 , C07C17/266 , C07D333/54 , C07D209/10 , C07D209/48 , C07F5/02 , C07F7/18 , C07J9/00 , C07J51/00 , C07C17/10 , C07C41/30 , C07C67/333 , C07C67/307 , B01J31/22 , C07B37/04 , C07C17/14 , C07C17/278 , C07C17/275 , C07C17/269 , C07C17/02 , C07C21/19 , C07C21/14 , C07C21/04 , C07C25/24 , C07C21/18 , C07C22/04 , C07C22/08 , C07C25/28 , C07C43/225 , C07C43/192 , C07C43/17 , C07C69/65 , C07C69/63 , C07C69/753
CPC分类号： C07F11/00 , B01J31/2265 , B01J2231/543 , B01J2531/64 , B01J2531/66 , C07B37/04 , C07C17/02 , C07C17/10 , C07C17/14 , C07C17/266 , C07C17/269 , C07C17/275 , C07C17/278 , C07C17/361 , C07C21/14 , C07C21/18 , C07C22/08 , C07C37/62 , C07C41/30 , C07C45/63 , C07C67/307 , C07C67/333 , C07C69/753 , C07C2601/14 , C07C2603/26 , C07D209/10 , C07D209/48 , C07D333/54 , C07F5/025 , C07F7/1804 , C07J9/00 , C07J51/00 , C07C21/19 , C07C21/04 , C07C25/24 , C07C22/04 , C07C22/00 , C07C22/02 , C07C25/28 , C07C43/225 , C07C43/192 , C07C43/17 , C07C69/65 , C07C69/63
摘要： The present application provides, among other things, compounds and methods for metathesis reactions. In some embodiments, the present disclosure provides methods for preparing alkenyl halide with regioselectivity and/or stereoselectivity. In some embodiments, the present disclosure provides methods for preparing alkenyl halide with regioselectivity and Z-selectivity. In some embodiments, the present disclosure provides methods for preparing alkenyl halide with regioselectivity and E-selectivity. In some embodiments, provided technologies are particularly useful for preparing alkenyl fluorides. In some embodiments, a provided compound useful for metathesis reactions has the structure of formula II-a. In some embodiments, a provided compound useful for metathesis reactions has the structure of formula II-b.

7. 发明授权

US09896400B2 Process for producing a chlorinated C3-6 alkane 有权
公开(公告)号：US09896400B2
公开(公告)日：2018-02-20
申请号：US14882492
申请日：2015-10-14
申请人： SPOLEK PRO CHEMICKOU A HUTNI VYROBU A.S.
发明人： Karel Filas , Pavel Kubicek , Zdenek Ondrus , Petr Sladek
IPC分类号： C07C17/275 , C07C17/38 , C07C17/383 , C07C17/02 , C07C19/01
CPC分类号： C07C17/02 , C07C17/275 , C07C17/38 , C07C17/383 , C07C19/01 , Y02P20/582
摘要： Disclosed is a process for producing a chlorinated C3-6 alkane comprising providing a reaction mixture comprising an alkene and carbon tetrachloride in a principal alkylation zone to produce chlorinated C3-6 alkane in the reaction mixture, and extracting a portion of the reaction mixture from the principal alkylation zone, wherein: a) the concentration of the chlorinated C3-6 alkane in the reaction mixture in the principal alkylation zone is maintained at a level such that the molar ratio of chlorinated C3-6 alkane:carbon tetrachloride in the reaction mixture extracted from the alkylation zone does not exceed 95:5 when the principal alkylation zone is in continuous operation; and/or b) the reaction mixture extracted from the principal alkylation zone additionally comprises alkene and the reaction mixture is subjected to a dealkenation step in which at least about 50% or more by weight of the alkene present in the reaction mixture is extracted therefrom and at least about 50% of the extracted alkene is fed back into the reaction mixture provided in the principal alkylation zone; and/or c) the reaction mixture present in the principal alkylation zone and extracted from the principal alkylation zone additionally comprises a catalyst, and the reaction mixture extracted from the principal alkylation zone is subjected to an aqueous treatment step in which the reaction mixture is contacted with an aqueous medium in an aqueous treatment zone, a biphasic mixture is formed and an organic phase comprising catalyst is extracted from the biphasic mixture.

8. 发明授权

US09840448B2 Processes for producing very high purity 1,1,1,2,3-pentachloropropane 有权
公开(公告)号：US09840448B2
公开(公告)日：2017-12-12
申请号：US14883648
申请日：2015-10-15
申请人： SPOLEK PRO CHEMICKOU A HUTNI VYROBU A.S.
发明人： Zdenek Ondrus , Pavel Kubicek , Karel Filas , Petr Sladek
IPC分类号： C07C17/275 , C07C17/25 , C07C17/04 , C07C17/38 , C07C17/383 , C07C17/087 , C07C17/266 , C07C19/01
CPC分类号： C07C17/087 , C07C17/04 , C07C17/25 , C07C17/266 , C07C17/275 , C07C17/38 , C07C17/383 , C07C19/01 , Y02P20/582 , C07C21/04
摘要： Disclosed is a process for preparing a highly pure 1,1,1,2,3-pentachloropropane product, comprising 1-a) providing a reaction mixture comprising ethylene, carbon tetrachloride and a catalyst in a principal alkylation zone to produce 1,1,1,3-tetrachloropropane in the reaction mixture, and 1-btreating the reaction mixture obtained in step 1-a) to obtain a 1,1,1,3-tetrachloropropane feedstock; 2-a) contacting the 1,1,1,3-tetrachloropropane feedstock with a catalyst in a dehydrochlorination zone to produce a reaction mixture comprising 1,1,1,3-tetrachloropropane and 1,1,3-trichloropropene, and 2-b) treating the reaction mixture obtained in step 2-a) to obtain a 1,1,3-trichloropropene feedstock; 3-a) contacting the 1,1,3-trichloropropene feedstock with chlorine in a reaction zone to produce a reaction mixture containing 1,1,1,2,3-pentachloropropane and 1,1,3-trichloropropene, the reaction zone being different from the dehydrochlorination zone, and 3-b) treating the reaction mixture obtained in step 3-a) to obtain the highly pure 1,1,1,2,3-pentachloropropane product.

9. 发明授权

US09255048B2 Process for producing chlorinated hydrocarbons 有权
标题翻译：氯化烃生产工艺
公开(公告)号：US09255048B2
公开(公告)日：2016-02-09
申请号：US14503942
申请日：2014-10-01
申请人： Axiall Ohio, Inc.
发明人： Scott A. Sherwood , Stephen Robert Lester
IPC分类号： C07C17/35 , C07C17/10 , C07C17/25 , C07C17/275 , B01J27/10
CPC分类号： C07C17/35 , B01J27/10 , C07C17/10 , C07C17/25 , C07C17/275 , C07C19/01 , C07C21/04
摘要： The preparation of chlorinated hydrocarbons, such as pentachloropropanes, such as 1,1,1,2,3-pentachloropropane, from tetrachloropropanes, such as 1,1,1,3-tetrachloropropane, in the presence of a polyvalent antimony compound that includes a pentavalent antimony compound, such as antimony pentachloride, is described. Also described are methods for preparing optionally chlorinated alkenes, such as, tetrachloropropenes, from chlorinated alkanes, such as pentachloropropanes, in the presence of ferric chloride and a polyvalent antimony compound that includes a pentavalent antimony compound.
摘要翻译：四氯丙烷如1,1,1,3-四氯丙烷等氯代烃如五氯丙烷如1,1,1,2,3-五氯丙烷在多价锑化合物存在下的制备，包括描述了五价锑化合物，例如五氯化锑。还描述了在氯化铁存在下由氯代烷烃如五氯丙烷和包含五价锑化合物的多价锑化合物制备任选氯代烯烃如四氯丙烯的方法。

10. 发明授权

US09162946B2 Process for preparing C3-6 (hydro)fluoroalkenes by dehydrohalogenating C3-6 halo(hydro)fluoroalkanes in the presence of a zinc/chromia catalyst 有权
标题翻译：在锌/氧化铬催化剂存在下，通过使C3-6卤代（氢）氟烷烃脱卤化氢制备C 3-6（氢）氟代烯烃的方法
公开(公告)号：US09162946B2
公开(公告)日：2015-10-20
申请号：US14043191
申请日：2013-10-01
申请人： MEXICHEM AMANCO HOLDING S.A. DE C.V.
发明人： Andrew Paul Sharratt , Leslie Richard Seddon
IPC分类号： C07C21/00 , C07C17/04 , C07B39/00 , C07C17/20 , C09K5/04 , C07C17/275 , C07C17/18 , C07C21/18 , C07C45/63 , C07C17/087 , C07C17/23 , C07C17/25 , C07C17/358
CPC分类号： C07C17/25 , B01J23/06 , B01J23/26 , C07B39/00 , C07B2200/09 , C07C17/04 , C07C17/087 , C07C17/18 , C07C17/206 , C07C17/21 , C07C17/23 , C07C17/275 , C07C17/358 , C07C21/18 , C07C45/63 , C09K5/045 , C09K2205/126 , C07C19/10 , C07C19/01 , C07C19/08 , C07C49/16
摘要： The invention relates to a process for preparing a C3-6 (hydro)fluoroalkene comprising dehydrohalogenating a C3-6 hydro(halo)fluoroalkane in the presence of a zinc/chromia catalyst, wherein the C3-6 (hydro)fluoroalkene produced is isomerised in the presence of the zinc/chromia catalyst.
摘要翻译：本发明涉及一种制备C3-6（氢）氟代烯烃的方法，该方法包括在锌/氧化铬催化剂存在下将C3-6氢（卤代）氟代烷烃脱卤化氢，其中制备的C 3-6（氢）氟代烯烃异构化为存在锌/氧化铬催化剂。

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