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11. 发明授权

US06624279B2 Water-soluble carbamate materials 有权
公开(公告)号：US06624279B2
公开(公告)日：2003-09-23
申请号：US10042820
申请日：2002-01-09
申请人： Walter H. Ohrbom , David J. Law , Patricia A. Herrel
发明人： Walter H. Ohrbom , David J. Law , Patricia A. Herrel
IPC分类号： C08G1806
CPC分类号： C07C271/12 , C08F20/36 , C08G18/2815 , C08G18/3831 , C09D161/28 , C09D201/025 , Y10T428/31551 , Y10T428/31725 , Y10T428/31855
摘要： The invention provides water-soluble, &bgr;-hydroxy carbamate-functional materials and coating compositions, especially waterborne coating compositions, containing the carbamate-functional materials. The invention further provide a coating prepared from the coating composition and a coated substrate, especially an automotive substrate, having the coating thereon.

12. 发明授权

US06583212B2 Aqueous dispersions for coating compositions 失效
公开(公告)号：US06583212B2
公开(公告)日：2003-06-24
申请号：US10015095
申请日：2001-12-11
申请人： Joseph P. Borst , Sergio E Balatan , Walter H. Ohrbom , Robert D. Weise , Davide J. Law
发明人： Joseph P. Borst , Sergio E Balatan , Walter H. Ohrbom , Robert D. Weise , Davide J. Law
IPC分类号： C08J302
CPC分类号： C09D5/027 , C08J3/03 , C09D201/025
摘要： The invention provides curable coating compositions comprising an aqueous dispersion comprising a stabilizing resin (P1) and a compound (P2) comprising functional groups reactable with a crosslinking agent. Compound (P2) is dispersed into stabilizing resin (P1). The coating compositions of the invention may further comprise an optional crosslinking agent (P3) which may or may not be dispersed into stabilizing resin (P1). In a particularly preferred embodiment, both the stabilizing resin (P1) and compound (P2) will comprise functional groups which are carbamate or are convertible to carbamate.

13. 发明授权

US06531560B1 Carbamate-functional resins having improved adhesion, method of making the same, and method of improving intercoat adhesion 有权
公开(公告)号：US06531560B1
公开(公告)日：2003-03-11
申请号：US09677063
申请日：2000-09-29
申请人： Donald H. Campbell , Walter H. Ohrbom , Joseph Borst , Michael A. Gessner , Donald L. St. Aubin , Marvin L. Green , Bruce E. Oermann
发明人： Donald H. Campbell , Walter H. Ohrbom , Joseph Borst , Michael A. Gessner , Donald L. St. Aubin , Marvin L. Green , Bruce E. Oermann
IPC分类号： C08F12602
CPC分类号： C08G18/8116 , C08F8/00 , C08F2800/20 , C08F2810/50 , C08G18/3823 , C09D201/025 , Y10T428/31551 , Y10T428/31573 , Y10T428/31645 , C08F2220/325 , C08F220/34 , C08F220/20 , C08F212/08
摘要： The invention provides carbamate-functional resins and coating compositions incorporating said resins that have improved adhesion with respect to subsequently applied films or coatings. More particularly, the invention relates to carbamate-functional addition polymers having at least 250 grams of polymer per carbamate group which are made with less than 35 percent by weight of nonfunctional monomers, preferably with less than 20 percent by weight and most preferably from 0 to less than 10 percent by weight, based on the total weight of the polymer. The invention further provides a method of making a carbamate-functional polymer and carbamate-functional polymers made by the claimed method. Finally, the invention provides a method for improving the adhesion of a first coating composition to a subsequently applied material as well as a method of making a composite comprising a coated substrate, an adhesive composition, and a glass having at least one surface.

14. 发明授权

US06391969B1 Powder slurry compositions with solid particulate carbamate resin component dispersed in liquid aminoplast resin carrier 失效
标题翻译：具有固体颗粒状氨基甲酸酯树脂组分的粉末浆料组合物分散在液体氨基塑料树脂载体中
公开(公告)号：US06391969B1
公开(公告)日：2002-05-21
申请号：US09633513
申请日：2000-08-07
申请人： Paul J. Harris , Walter H. Ohrbom , John W. Rehfuss
发明人： Paul J. Harris , Walter H. Ohrbom , John W. Rehfuss
IPC分类号： C08K507
CPC分类号： C09D201/06 , C08L2666/14
摘要： The invention provides a powder slurry composition comprising a first solid particulate component (a) dispersed in a crosslinking component (b) having at least one crosslinking resin which is liquid at 20° C. First component (a) is in solid particulate form having an average particle size of from 3 to 30 microns. Component (a) has a compound (i) having a Tg>40° C. and at least one carbamate or urea functional group, or a group convertible to a carbamate or urea group appended thereto. Crosslinking component (b) has at least one crosslinking resin (i) which is liquid at 20° C. Most preferably, crosslinking component (b) will further include a self-crosslinking aminoplast resin (ii) having at least two aminoplast groups and at least two groups which are nonreactive with solid particulate first component (a) but which are reactive with said aminoplast groups. The powder slurry composition of the invention has a VOC of less than 1.0 lbs./gal and provides performance and application improvements over the prior art.
摘要翻译：本发明提供一种粉末浆料组合物，其包含分散在具有至少一种在20℃下为液体的交联树脂的交联组分（b）中的第一固体颗粒组分（a）。第一组分（a）为固体颗粒形式，其具有平均粒径为3至30微米。组分（a）具有Tg> 40℃的化合物（i）和至少一个氨基甲酸酯或脲官能团，或可转化成氨基甲酸酯或脲基团的基团。交联组分（b）具有至少一种在20℃下为液体的交联树脂（i）。最优选地，交联组分（b）还包括具有至少两个氨基塑料基团的自交联氨基塑料树脂（ⅱ）至少两个与固体颗粒第一组分（a）反应但与所述氨基塑料基团反应的基团。本发明的粉末浆料组合物具有小于1.0lbs./gal的VOC，并且相对于现有技术提供了性能和应用改进。

15. 发明授权

US06300414B1 Additive for coating compositions for adhesion to TPO substrates 失效
标题翻译：用于粘附到TPO基材上的涂料组合物的添加剂
公开(公告)号：US06300414B1
公开(公告)日：2001-10-09
申请号：US09143156
申请日：1998-08-28
申请人： John D. McGee , Daniel Blickberndt , Craig Schang , Walter H. Ohrbom , Keri Krueger
发明人： John D. McGee , Daniel Blickberndt , Craig Schang , Walter H. Ohrbom , Keri Krueger
IPC分类号： C08L6702
CPC分类号： C08L71/02 , C08G63/00 , C08L53/005 , C09D5/002 , C09D7/65 , C09D201/00 , Y10T428/31909 , Y10T428/31913 , Y10T428/31917 , C08L2666/04 , C08L2666/24
摘要： The present invention provides an olefin-based block copolymer that has an olefin block that is substantially saturated and at least one (poly)ester or (poly)ether block. The olefin-based block copolymer of the invention can be prepared by reacting a liquid hydroxyl-functional, saturated or substantially saturated olefin polymer with a chain-extension reagent that is reactive with hydroxyl groups and will polymerize in a head-to-tail arrangement of monomer units. The olefin-based block copolymer of the invention can be used to prepare an adhesion promoter that provides excellent adhesion of subsequent coating layers to olefinic substrates like TPO and superior properties as compared to previously used adhesion promoters containing chlorinated polyolefins. Alternatively, the olefin-based copolymers of the invention can be used as an additive in a curable coating composition to provide excellent adhesion to olefinic substrates like TPO, even when used in very minor amounts compared to the amounts required for previously known agents.
摘要翻译：本发明提供一种具有基本上饱和的烯烃嵌段和至少一种（多）酯或（聚）醚嵌段的烯烃基嵌段共聚物。本发明的烯烃基嵌段共聚物可以通过使液体羟基官能的饱和或基本上饱和的烯烃聚合物与与羟基反应的链延长试剂反应来制备，并且将以头 - 尾排列的方式聚合单体单元。与先前使用的含有氯化聚烯烃的粘合促进剂相比，本发明的烯烃基嵌段共聚物可用于制备粘合促进剂，其对随后的涂层提供与TPO等烯烃基材的优异粘附性和优异的性能。或者，本发明的烯烃基共聚物可用作可固化涂料组合物中的添加剂，以提供与诸如TPO的烯烃基材的优异粘合性，即使以与先前已知的试剂所需量相比非常小的量使用。

16. 发明授权

US06080825A Curable coating compositions containing blends of carbamate-functional compounds 有权
标题翻译：含有氨基甲酸酯官能化合物的混合物的可固化涂料组合物
公开(公告)号：US06080825A
公开(公告)日：2000-06-27
申请号：US184197
申请日：1998-11-02
申请人： Walter H Ohrbom , Gregory G. Menovcik , Donald L. St. Aubin , John E. Boisseau , John W. Rehfuss , John D. McGee , Brian D. Bammel , Danielle Regulski , Christopher Bradford
发明人： Walter H Ohrbom , Gregory G. Menovcik , Donald L. St. Aubin , John E. Boisseau , John W. Rehfuss , John D. McGee , Brian D. Bammel , Danielle Regulski , Christopher Bradford
IPC分类号： C09D175/04 , C07D251/34 , C08F8/30 , C08G12/40 , C08G18/08 , C08G18/10 , C08G18/28 , C08G18/30 , C08G18/38 , C08G18/46 , C08G18/66 , C08G18/79 , C08G18/80 , C08G59/14 , C08G71/00 , C08G81/02 , C08K5/3492 , C08L61/20 , C09D133/06 , C09D161/20 , C09D167/00 , C09D167/04 , C09D169/00 , C09D175/00 , C09D175/02 , C09D201/02 , C09D201/06 , C08G8/28 , C08L63/00 , C08L67/04
CPC分类号： C07D251/34 , C08G12/40 , C08G18/0823 , C08G18/10 , C08G18/2865 , C08G18/302 , C08G18/3829 , C08G18/3831 , C08G18/3853 , C08G18/4615 , C08G18/6633 , C08G18/792 , C08G18/8077 , C08G59/1438 , C08G59/1477 , C08G59/1494 , C08G71/00 , C08G81/021 , C08K5/34924 , C09D133/062 , C09D161/20 , C09D167/00 , C09D167/04 , C09D169/00 , C09D175/00 , C09D175/02 , C09D175/04 , C09D201/02 , C09D201/025 , C09D201/06 , C08L61/20
摘要： The present invention provides a curable coating composition that includes at least three components. The coating composition includes a component (a) that includes one or both of a compound (a)(1) having at least one carbamate group or terminal urea group according to the invention and having at least two linking groups that are urethane or urea or a compound (a)(2) having at least two groups selected from carbamate groups, terminal urea groups, or combinations of the two and at least four urethane or urea linking groups. The second component (b) of the coating composition includes a polymer resin comprising active hydrogen-containing functional groups reactive with the third component (c). The resins is selected from polyester, polyurethane, or polyester-polyurethane copolymers Component (c) of the coating composition is a curing agent that is reactive with the first two components. Preparation of coated articles using the compositions of the invention is also disclosed.
摘要翻译：本发明提供了包含至少三种组分的可固化涂料组合物。涂料组合物包括组分（a），其包含根据本发明的具有至少一个氨基甲酸酯基团或末端脲基团的化合物（a）（1）中的一种或两种，并且具有至少两个氨基甲酸酯或脲的连接基团或具有至少两个选自氨基甲酸酯基，末端脲基团或两个和至少四个氨基甲酸酯或脲连接基团的组合的化合物（a）（2）。涂料组合物的第二组分（b）包括含有与第三组分（c）反应的含活性氢官能团的聚合物树脂。树脂选自聚酯，聚氨酯或聚酯 - 聚氨酯共聚物涂料组合物的组分（c）是与前两种组分反应的固化剂。还公开了使用本发明组合物制备涂层制品。

17. 发明授权

US6048443A Low bake cathodic electrocoat having dual cure mechanism 有权
标题翻译：低烘烤阴极电泳具有双重固化机理
公开(公告)号：US6048443A
公开(公告)日：2000-04-11
申请号：US217565
申请日：1998-12-21
申请人： Timothy S. December , Walter H Ohrbom , Gregory G. Menovcik
发明人： Timothy S. December , Walter H Ohrbom , Gregory G. Menovcik
IPC分类号： C09D133/14 , C08F220/36 , C08F220/56 , C09D5/00 , C09D5/44 , C25D13/04
CPC分类号： C09D5/4407
摘要： The invention provides cathodic electrocoat compositions having a carbamate functional resin with a cationic salting site, a crosslinking agent reactive with the carbamate functional resin and a carbonate curing agent. The invention also provides methods of cathodically electrodepositing a coating on a substrate using the coating compositions of the invention. The compositions of the invention provide urethane crosslinking sites without the use of disadvantageous blocked isocyanates and cure at temperatures lower than prior art cathodic electrocoat compositions.
摘要翻译：本发明提供了具有阳离子盐析位点的氨基甲酸酯官能树脂，与氨基甲酸酯官能树脂反应的交联剂和碳酸酯固化剂的阴极电泳涂料组合物。本发明还提供了使用本发明的涂料组合物阴极电沉积在基材上的涂层的方法。本发明的组合物提供氨基甲酸酯交联位点，而不使用不利的封闭异氰酸酯，并且在比现有技术的阴极电泳涂料组合物低的温度下固化。

18. 发明授权

US5994479A Curable coating compositions containing blends of carbamate-functional compounds 失效
标题翻译：含有氨基甲酸酯官能化合物的混合物的可固化涂料组合物
公开(公告)号：US5994479A
公开(公告)日：1999-11-30
申请号：US997317
申请日：1997-12-23
申请人： Marvin L. Green , John D. McGee , Brian D. Bammel , Danielle A. Regulski , Walter H. Ohrbom
发明人： Marvin L. Green , John D. McGee , Brian D. Bammel , Danielle A. Regulski , Walter H. Ohrbom
IPC分类号： C08G18/40 , C08G18/80 , C09D5/02 , C09D5/03 , C09D161/20 , C09D175/00 , C09D201/02 , C08G8/28 , C08G59/14 , C08L63/00 , C08L67/04
CPC分类号： C09D161/20 , C08G18/8077 , C09D201/025 , Y10T428/31551
摘要： The present invention provides a curable coating composition comprising(a) a first component comprising at least two functional groups, at least one of which is a carbamate or urea group that is the reaction product of:(1) a hydroxyl group that is the result of a ring-opening reaction between an epoxy group and an organic acid group, and(2) cyanic acid or a carbamate or urea group;(b) a curing agent having a plurality of functional groups that are reactive with component (a), and(c) a second component having functional groups that are reactive with component (a) or component (b) or both components (a) and (b).
摘要翻译：本发明提供一种可固化涂料组合物，其包含（a）包含至少两个官能团的第一组分，其中至少一个为氨基甲酸酯或脲基，其为：（1）作为结果的羟基的反应产物的环氧基和有机酸基之间的开环反应，和（2）氰酸或氨基甲酸酯或脲基; （b）具有多个与组分（a）反应的官能团的固化剂，和（c）具有与组分（a）或组分（b）或两种组分（a）反应的官能团的第二组分）和（b）。

19. 发明授权

US5827931A Polyurethane polymer or oligomer having carbamate groups, method for its preparation, and coating composition 失效
公开(公告)号：US5827931A
公开(公告)日：1998-10-27
申请号：US950950
申请日：1997-10-15
申请人： Gregory L. Menovcik , Walter H. Ohrbom
发明人： Gregory L. Menovcik , Walter H. Ohrbom
IPC分类号： C08G18/08 , C08G18/32 , C08G18/38 , C08G18/46 , C08G18/66 , C08G18/80 , C08G71/00 , C08G71/04 , C09D175/00 , C09D175/04 , C09D201/02 , C08G18/28
CPC分类号： C09D201/025 , C08G18/0823 , C08G18/3831 , C08G18/6633 , C08G18/8077 , C09D175/04
摘要： Polyurethane polymers having pendant carbamate groups are disclosed. The polymers are prepared by: (a) reacting a mixture comprising a polyol having at least one pendant carbamate group and a polyisocyanate to form a polyurethane having pendant carbamate groups, and (b) optionally, capping the polyurethane from (b) with an active hydrogen-containing capping agent.

20. 发明授权

US5760127A Curable coating composition 失效
标题翻译：可固化涂料组合物
公开(公告)号：US5760127A
公开(公告)日：1998-06-02
申请号：US698526
申请日：1996-08-15
申请人： Brian D. Bammel , John D. McGee , Walter H. Ohrbom , Todd A. Seaver , Gregory G. Menovcik , Paul J. Harris , John W. Rehfuss
发明人： Brian D. Bammel , John D. McGee , Walter H. Ohrbom , Todd A. Seaver , Gregory G. Menovcik , Paul J. Harris , John W. Rehfuss
IPC分类号： C08G71/00 , C09D167/04 , C09D201/02 , C08J3/00 , B32B27/00 , C08K3/20 , C08L75/00
CPC分类号： C09D201/02 , C08G71/00 , C09D167/04 , C09D201/025 , Y10T428/31551
摘要： A curable coating composition is described comprising (A) a carbamate- or urea-functional compound that is the reaction product of a mixture comprising (1) a compound comprising a carbamate or urea group or a group that can be converted to carbamate or urea, and a hydroxyl functional group that is the reaction product of (a) a compound comprising a carbamate or urea group or a group that can be converted to a carbamate or urea group, and an active hydrogen group that is reactive with a lactone ring or a hydroxy carboxylic acid, and (b) a lactone or a hydroxy carboxylic acid, and (2) a compound that is reactive with hydroxyl groups on a plurality of molecules of compound (A)(1), but that is not reactive with the carbamate or urea groups on compound (A)(1), (B) a compound comprising a plurality of groups that are reactive with carbamate or urea.
摘要翻译：描述了可固化涂料组合物，其包含（A）氨基甲酸酯或脲官能化合物，其为包含（1）包含氨基甲酸酯或脲基团的化合物或可转化为氨基甲酸酯或脲的基团的混合物的反应产物，和作为（a）包含氨基甲酸酯或脲基的化合物或可以转化为氨基甲酸酯或脲基的基团的反应产物的羟基官能团以及与内酯环或羟基羧酸和（b）内酯或羟基羧酸，和（2）与多个化合物（A）（1）分子上的羟基反应但不与氨基甲酸酯反应的化合物或化合物（A）（1）上的脲基，（B）包含与氨基甲酸酯或脲反应的多个基团的化合物。

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