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    • 10. 发明专利
    • MEASURING METHOD OF PROGRESS STATE OF CROSS-LINKING REACTION OF RUBBER BY ELECTRICAL CHARACTERISTIC VALUE
    • JPH08285802A
    • 1996-11-01
    • JP11228795
    • 1995-04-13
    • JAPAN ATOMIC ENERGY RES INSTOILES INDUSTRY CO LTD
    • OOKAWA YOSHINAOAKUTSU YOICHISHIMODA IKUOIKENAGA MASAYOSHISASAKI KOSUKE
    • G01N27/02
    • PURPOSE: To obtain a measuring method in which the cross-linking progress state of an uncross-linked rubber can be measured by a method wherein one pair of specific steels plates out of a plurality of internal steel plates which support uncross-linked laminated rubber are used as electrodes, a cycle voltage is applied and an electrical characteristic value is detected. CONSTITUTION: Sheetlike unvulcanized rubber and steel plates 14 to 18 are arranged alternately inside a mold 20 which has been preheated to the vulcanizing temperature of the rubbers, and an axial-direction load is applied to the sheetlike unvulcanized rubber and the steel plates 14 to 18 by an upper plate 41 and a push plate 43 by means of a press machine 50. The laminated rubber 13 which are arranged in the mold 20 raise their temperature with the passage of time so as to reach the vulcanizing temperature, of the rubber, which is the same temperature as the mold. Thereby, as the cross-linking reaction of the laminated rubbers 13 progresses, an electrical AC resistance value is raised once, it is then lowered, and it then displays a constant value. This indicates a point of time in which the time change rate of an AC resistance becomes nearly zero, and it is a point of time in which the cross- linking reaction of the laminated rubber 13 has been completed. Consequently, when a change in the time change rate of the electrical AC resistance is traced, the progress degree of the cross-linking reaction of the rubber can be observed.