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    • 22. 发明专利
    • STANDARD SAMPLE FOR EVALUATION PULVEROUS PARTICLE
    • JPS61251747A
    • 1986-11-08
    • JP9285885
    • 1985-04-30
    • TOSHIBA CORP
    • OGINO MASANOBUMIYASHITA MORIYA
    • G01N15/00G01N1/00G01N15/02
    • PURPOSE:To obtain a standard sample which makes possible the exact control of a pulverous particle measuring imstrument by sticking pulverous particles to a substrate and covering the particle-sticking surface with a transparent film. CONSTITUTION:The standard sample is prepd. by sticking the pulverous particles 2 onto the semiconductor substrate 1 and covering the particle-sticking surface thereof with the transparent film 5. The substrate 1 is, for example, a silicon wafer and the pulverous particles 2 are, for example, abrasive particles of SiO2. The transparent film 5 is obtd. by coating a polyamic acid by using a coating machine called spinner and baking the same for the prescribed time in an N2 atmosphere kept at a prescribed temp. to polymerize the polyamic acie thereby forming the transparent polyamide film to about 2mum on the abrasive SiO2 particle-sticking surface. The same number of particles and distribution conditions are thereby obtd. simply by washing and therefore the exact control of the pulverous particle measuring instrument is made possible.
    • 23. 发明专利
    • UNDERWATER COLLECTOR
    • JPS61247937A
    • 1986-11-05
    • JP9020685
    • 1985-04-26
    • TOSHIBA CORP
    • MIYASHITA MORIYA
    • G01N1/22
    • PURPOSE:To collect a sample in a short time and to discriminate the size of a minute particle entering into the pure water by providing an outside vessel storing a vessel containing the pure water and introducing positively the air of objective space to be analyzed therein and providing a filter on an air intake port of the outside vessel. CONSTITUTION:The vessel 1 containing the pure water 2 is stored in the outside vessel 3. The top of this outside vessel 3 is open and the filter 4 is fitted thereto and besides, a discharge port 5 is provided to the side and a wind discharging means 6 such as the vacuum piping or a vacuum pump is connected with the discharge port 5. Here, the filter 4 to prevent from passing of a minute article over 0.3[mum] is used. The vessel 1 containing the pure water and the outside vessel 3 are constituted of 'Tefuron(R)' easy for cleaning respectively but glass or the like may be used for the material.
    • 26. 发明专利
    • MANUFACTURE AND INSPECTION OF SEMICONDUCTOR SUBSTRATE
    • JPH09283529A
    • 1997-10-31
    • JP3211197
    • 1997-02-17
    • TOSHIBA MICRO ELECTRONICSTOSHIBA CORP
    • MIYASHITA MORIYAOGINO MASANOBUHOSHI TADAHIDENUMANO MASAKUNISAMATA SHUICHISEKIHARA AKIKOAKITA KEIKO
    • H01L21/66H01L21/322
    • PROBLEM TO BE SOLVED: To provide a method for manufacturing a semiconductor substrate which denuded zone(DZ) layer deep enough to prevent adverse influences to device characteristics is formed while avoiding a high-temperature annealing process at the time of manufacturing a semiconductor device with use wafer, and also to provide a method for suitably inspecting a density of oxygen precipitation (BMD) in the semiconductor substrate. SOLUTION: In the semiconductor substrate manufacturing method, oxygen precipitation nuclei are precipitated for a silicon single crystal having a region containing a first concentration of boron exceeding a predetermined value within a predetermined region on one major surface side, or oxygen precipitations are grown from the oxygen precipitation nuclei. Next, the substrate is annealed in a temperature range which is higher than a temperature of a first annealing step, sufficiently higher to reduce the oxygen precipitation nuclei or the oxygen precipitations grown therefrom and sufficiently lower to such an extent that boron re-distribution does not affect the oxygen precipitations to form a predetermined depth of denuded layer within the predetermined zone on one major surface side. The semiconductor substrate inspecting method further includes a step of measuring a density of odes of the oxygen precipitations grown from the oxygen precipitation nuclei precipitated within the silicon single crystal, following the above annealing process.
    • 27. 发明专利
    • CLEANING OF SEMICONDUCTOR SUBSTRATE
    • JPH0298928A
    • 1990-04-11
    • JP25125688
    • 1988-10-05
    • TOSHIBA CORP
    • MIYASHITA MORIYAYOSHII SHINTARO
    • B08B7/00G03F7/42H01L21/304
    • PURPOSE:To prevent the surface of a substrate from being contaminated and to realize a safe operation by a method wherein an extraction tank as a high- pressure container for substrate cleaning use and a heater used to heat the inside of the extraction tank are installed and a gas at a critical temperature or higher and at a critical pressure or higher is used. CONSTITUTION:A substrate 2 is arranged inside an extraction tank 1; a temperature of the extraction tank 1 is raised to 400 deg.C; carbon dioxide at 60 deg.C is introduced into the extraction tank 1 at a pressure of 400 atm. In this case, a critical temperature of the carbon dioxide is 31.06 deg.C and its critical pressure is 73.8 atm; the inside of the extraction tank 1 contains a supercritical gas. During this process, an outer wall of a separation tank 11 is cooled by using cooling water at 10 deg.C. Accordingly, an extracted organic substance is separated in the separation tank 11. When, e.g., a photoresist film coated on the substrate 2 in a photoetching process is stripped off, a silicon oxide film at 1000Angstrom is formed on a silicon substrate, an aluminum electrode thin film with a thickness of 1mum is evaporated on it and a test pattern where lines and spaces are repeated alternately is formed. After that, the resist is stripped off. Thereby, it is possible to prevent the surface of the substrate from being contaminated.
    • 28. 发明专利
    • PROCESSING OF SEMICONDUCTOR SUBSTRATE
    • JPH01143218A
    • 1989-06-05
    • JP30042187
    • 1987-11-28
    • TOSHIBA CORP
    • MATSUSHITA YOSHIAKIMIYASHITA MORIYAWAKATSUKI MAKIKOTSUCHIYA NORIHIKOKUBOTA ATSUKO
    • H01L21/304H01L21/306H01L21/322
    • PURPOSE:To form damage to the rear for fine gettering and allow a clearance process to be independent of some adverse effect, by immersing a substrate in a treating liquid and cleaning the surface of the substrate by causing ultrasonic waves to be propagated to the surface of its substrate through this treating liquid, thereby damaging the surface for use in gettering as well. CONSTITUTION:A treatment vessel 10 is filled with ultra-pure water and this device makes an ultrasonic wave generating part 12 operate to perform its treatment. In such a case, the output of ultrasonic waves are selected within a range 50-500W and their frequencies are selected within a range 10-100kHz. As the ultrasonic waves which are propagated in ultra-pure water abut on each wafer 14, damage is formed at both sides and simultaneously the surface is cleaned as well. When its output is less than 50W, the rear is not damaged and further, when it is more than 500W, damage to the rear becomes so large that such damage is not removed by merely polishing the face of a mirror later on and the oxidation inductive stacking fault(OSF) density of the surface side increases. In this way, as the rear damage for use in fine gettering is formed; besides, fine particles that stick to a wafer can be lessened to a minimum, a post-processing in succession to the above formation of the rear damage is not affected very much.
    • 29. 发明专利
    • MANUFACTURE OF SEMICONDUCTOR DEVICE
    • JPS637635A
    • 1988-01-13
    • JP14981786
    • 1986-06-27
    • TOSHIBA CORP
    • MIYASHITA MORIYA
    • H01L21/314
    • PURPOSE:To prevent deterioration of an MOS field effect type semiconductor device, by accumulating alkali metal ions and the like in the surface layer of an insulating film by corona charging, and removing the surface layer. CONSTITUTION: In corona charging, a semiconductor substrate 3 is mounted on a grounding plate 2 so that an SiO2 film 32 is directed toward a grid 1, and a DC voltage of -8,000 V is applied to the grid 1. Therefore, corona is charged on the surface of the SiO2 film 32, and the surface potential of -5 V is generated. At the same time, the grounding plate 2 is heated to 250 deg.C, and the temperature is kept for about 30 minutes. Then, Na ions in the SiO2 film, whose temperature is increased to said temperature, are moved readily and are attracted to the surface, which is negatively charged. Then, with the voltage being applied to the grid 1, the grounding plate 2 is cooled, and the temperature of a wafer is decreased to normal temperature. Then, the Na ions are accumulated in the surface of the SiO2 film 32, and a semiconductor substrate, in which said state is fixed, is obtained. Said wafer is immersed in treating liquid, in which, e.g., 30% hydroflouric acid is dilluted by 100 times. Thus the surface layer of the SiO2 film, in which the Na ions are accumulated, is removed by the thickness of about 20Angstrom .
    • 30. 发明专利
    • DECOMPOSITION UNIT FOR SEMICONDUCTOR THIN FILM
    • JPS622546A
    • 1987-01-08
    • JP14023185
    • 1985-06-28
    • TOSHIBA CORPTOSHIBA MICRO CUMPUTER ENG
    • MIYASHITA MORIYASAKUMA KEIKO
    • H01L21/306
    • PURPOSE:To realizeaa semiconductor film decomposing unit, small in size and easy to transport, capable of decomposing semiconductor thin film in a short time without exposing the testing personnel to the danger of hydrofluoric acid by a method wherein the vessel bottom is made of a plate of silver or the like so that the easily transmitted to the hydrofluoric acid in the vessel. CONSTITUTION:The bottom section of a closable vessel 6 serves as a sump for hydrofluoric acid L and the closable vessel 6 is installd on a planar heater 7. A semiconductor sustrate W provided with a thin film (f) is accommodated in a wafer carrier 9 housed in the closed vessel 6. A cover 6a is installed for the closure of the closable vessel 6, whereafter the heater 7 starts warming the bottom of the closable vessel 6 until the temperature reaches 80 deg.C. The thin film (f) is decomposed into liquid (l) in the presence of a quantity of hydrofluoric vapor originating in the hydrofluoric acid L. The liquid (l) collects in a pan 8. A drain/exhaust port 10 is coupled to a waste hydrofluoric acid tank with the intermediary of a pump. A valve 11 is then opened for the discharge for the hydrofluoric acid L out of the closable vessel 6, whereafter the closable vessel 6 is evacuated of the hydrofluoric vapor. With the planar heater 7 accelerating the generation of hydrofluoric vapor, the vapor pressure inside the closable vessel 6 promptly reaches saturation.