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1. 发明公开

EP4364849A2 NANOSTRUCTURED BATTERY ACTIVE MATERIALS AND METHODS OF PRODUCING SAME 审中-公开
公开(公告)号：EP4364849A2
公开(公告)日：2024-05-08
申请号：EP24163995.4
申请日：2012-07-24
申请人： OneD Material, Inc.
发明人： CAO, Wanqing , ROBBINS, Virginia , ZHU, Yimin
IPC分类号： B01J37/02
CPC分类号： H01M4/134 , C01B33/02 , C01B33/029 , C01P2004/1620130101 , C01P2004/6420130101 , B01J21/18 , B01J23/72 , B01J37/0211 , C30B11/12 , C30B29/60 , C01B33/021 , C30B29/06 , Y02E60/10
摘要： Methods for producing nanostructures from copper-based catalysts on porous substrates, particularly silicon nanowires on carbon-based substrates for use as battery active materials, are provided. Related compositions are also described. In addition, novel methods for production of copper-based catalyst particles are provided. Methods for producing nanostructures from catalyst particles that comprise a gold shell and a core that does not include gold are also provided.

2. 发明公开

EP3046895A1 SUBSTRAT À REVÊTEMENT PEU PERMÉABLE POUR SOLIDIFICATION DE SILICIUM 审中-公开
标题翻译：与低渗透固结硅的涂装基材
公开(公告)号：EP3046895A1
公开(公告)日：2016-07-27
申请号：EP14780618.6
申请日：2014-09-12
申请人： Commissariat à l'Energie Atomique et aux Energies Alternatives
发明人： GARANDET, Jean-Paul , CAMEL, Denis , DREVET, Béatrice , EUSTATHOPOULOS, Nicolas , HUGUET, Charles , TESTARD, Johann , VOYTOVYCH, Rayisa
IPC分类号： C04B41/87 , C04B41/89 , C30B11/00 , C30B15/10
CPC分类号： C30B11/002 , C01B33/021 , C04B41/009 , C04B41/5035 , C04B41/52 , C04B41/87 , C04B41/89 , C04B2111/00879 , C09D1/00 , C30B29/06 , C04B35/565 , C04B35/584 , C04B35/522 , C04B41/4519 , C04B41/4539 , C04B41/455 , C04B41/457 , C04B41/5059 , C04B41/5066 , C04B41/5096 , C04B41/522 , C04B41/4582
摘要： The invention relates to a substrate characterised in that it is at least partially surface-coated with a coating containing at least one so-called "barrier" layer comprising silica and one or more material(s) X selected from among SiC, Si, Si
3 N
4 , in which layer the amount of X varies between 25 -wt.% and 50.-wt.% in relation to the total weight of the barrier layer, said barrier layer being formed by grains of one or more materials X covered at least partially in a silica shell, and said barrier layer being in direct contact with the substrate.

3. 发明公开

EP3036190A1 POLYKRISTALLINE SILICIUMBRUCHSTÜCKE UND VERFAHREN ZUM ZERKLEINERN VON POLYKRISTALLINEN SILICIUMSTÄBEN 有权
标题翻译：多晶硅片段和方法用于破碎多晶硅棒
公开(公告)号：EP3036190A1
公开(公告)日：2016-06-29
申请号：EP14752592.7
申请日：2014-08-07
申请人： Wacker Chemie AG
发明人： PECH, Reiner , GRUEBL, Peter
IPC分类号： C01B33/02 , C30B15/00 , C30B29/06
CPC分类号： C30B35/007 , B02C1/10 , B02C2/005 , B02C4/305 , B02C13/28 , B02C17/20 , B02C2210/02 , C01B33/02 , C01B33/021 , C30B15/00 , C30B29/06
摘要： Polycrystalline silicon fragments with tungsten carbide particles on the surface, where the mass-weighted average size of the tungsten carbide particles is less than or equal to 0.5μm, preferably less than or equal to 0.2 μm or is greater than or equal to 0.8 μm, preferably greater than or equal to 1.3 μm. Process for comminuting polycrystalline silicon rods to give fragments by means of at least one comminuting implement with a surface containing tungsten carbide, where the tungsten carbide content of the implement surface is less than or equal to 95% and the mass-weighted average grain size of the tungsten carbide particles is greater than or equal to 0.8 μm or where the tungsten carbide content of the implement surface is greater than or equal to 80% and the grain size of the tungsten carbide particles is less than or equal to 0.5 μm.

4. 发明公开

EP2607311A4 METHOD FOR PRODUCING SILICON MICROPARTICLES 审中-公开
标题翻译： PROCESS FOR硅纳米颗粒
公开(公告)号：EP2607311A4
公开(公告)日：2016-06-15
申请号：EP11818154
申请日：2011-08-12
申请人： BRIDGESTONE CORP
发明人： SATO SEIICHI , MIYANO MARI , ENDO SHIGEKI , SHIINO OSAMU , ONO SHINGO , YOSHIKAWA MASATO
IPC分类号： C01B33/025
CPC分类号： C01B33/021 , C01B33/025 , C01P2004/61

5. 发明公开

EP2900596A1 MESOPOROUS SILICON/CARBON COMPOSITE FOR USE AS LITHIUM ION BATTERY ANODE MATERIAL AND PROCESS OF PREPARING THE SAME 有权
标题翻译：介孔硅/碳复合用作锂离子电池负极材料及其制造方法
公开(公告)号：EP2900596A1
公开(公告)日：2015-08-05
申请号：EP11876699.7
申请日：2011-11-30
申请人： Robert Bosch GmbH
发明人： YANG, Jun , FENG, Xuejiao , ZHANG, Jingjun , ZHOU, Longjie
IPC分类号： C01B31/02 , C01B33/02 , H01M4/583 , H01M10/05
CPC分类号： H01M4/366 , C01B33/021 , H01M4/0428 , H01M4/0471 , H01M4/134 , H01M4/1393 , H01M4/1395 , H01M4/386 , H01M4/587 , H01M4/625 , H01M10/052 , H01M10/0525 , H01M2004/021 , Y02E60/122
摘要： A silicon/carbon composite comprises mesoporous silicon particles and carbon coating provided on the silicon particles, wherein the silicon particles have two pore size distribution of 2~4 nm and 20~40 nm. A process of preparing the silicon/carbon composite comprises the steps of preparing mesoporous silicon particles via a mechanochemical reaction between SiCl
4 and Li
13 Si
4 under ball milling and subsequent thermal treatment and washing process, and coating the mesoporous silicon particles with carbon. An anode for lithium ion battery comprises the silicon/carbon composite. A lithium ion battery comprises the silicon/carbon composite.
摘要翻译：甲硅/碳复合材料包含设置在硅颗粒中孔硅颗粒和碳涂层，具有worin 2-4纳米和20-40纳米2个的孔径分布。制备硅/碳复合物的过程中的硅粒子包括以下步骤经由下球磨和随后的热处理和洗涤处理的SiCl 4和Li33Si4之间的机械化学反应制备中孔硅颗粒，和涂布碳的中孔硅颗粒。用于锂离子电池的阳极包括硅/碳复合物。的锂离子电池由硅/碳复合物。

6. 发明公开

EP2883613A1 METHOD FOR PREPARING HIGH SPHERICITY SEED CRYSTAL AND FLUIDIZED BED PARTICLE SILICON 有权转让
标题翻译：工艺生产高种子球形和流化床颗粒硅
公开(公告)号：EP2883613A1
公开(公告)日：2015-06-17
申请号：EP13829331.1
申请日：2013-08-13
申请人： Jiangsu Zhongnen Polysilicon Technology Development Co., Ltd.
发明人： MIXON, David , NELAN, Christopher
IPC分类号： B02C4/30 , B01J8/24 , C01B33/00
CPC分类号： B02C4/32 , B02C4/02 , B02C4/286 , B02C23/16 , B02C23/18 , B02C23/24 , C01B33/021
摘要： The present invention discloses a method for generating high sphericity seed for the operation of a fluidized bed reactor to produce granular polysilicon. The method comprises: using fluidized bed granular silicon as a raw material, passing through a roll crusher apparatus to fracture, the roll crusher apparatus comprises at least one set of rollers, by adjusting the roller gap width between the sets of rollers, the silicon particles which size larger than the roller gap width are crushed, the silicon particles which size smaller than the roller gap width directly pass through the gap, thereby generating the high sphericity seed, then recycle back into fluidized bed reactor for reaction and generate granular silicon. According to the present invention, the generating seeds have a high sphericity and narrow PSD, compared to the low sphericity seeds, the porosity of the FBR in present invention is lower, and easier to avoid the formation of silicon powder and other negative impact.
摘要翻译：本发明盘松动的产生高球形种子的流化床反应器的外科手术，以产生粒状多晶硅的方法。该方法包括：使用流化床颗粒状硅作为原料，经过辊式破碎机装置破裂，辊式破碎机装置包括辊子的至少一组，通过调整组辊，该硅颗粒之间的辊隙宽度其尺寸比辊间隙宽度大被压碎，硅颗粒，其尺寸比辊间隙较小宽度直接穿过间隙，由此生成高球形种子，然后再循环回到流化床反应器以进行反应并生成粒状硅。。根据本发明，产生的种子具有高的球度和窄PSD相比低球形种子，所述FBR的在本发明的气孔率较低，更容易避免硅粉末和其它负面影响的形成。

7. 发明公开

EP2863212A1 POLYCRYSTALLINE SILICON CRYSTAL ORIENTATION DEGREE EVALUATION METHOD, POLYCRYSTALLINE SILICON ROD SELECTION METHOD, POLYCRYSTALLINE SILICON ROD, POLYCRYSTALLINE SILICON INGOT, AND POLYCRYSTALLINE SILICON FABRICATION METHOD 有权
标题翻译：评估方法引导DEGREE多晶硅CRYSTAL，FOR多晶硅棒，多晶硅BAR，多晶硅BLOCK AND METHOD FOR多晶硅竞争
公开(公告)号：EP2863212A1
公开(公告)日：2015-04-22
申请号：EP13806297.1
申请日：2013-06-18
申请人： Shin-Etsu Chemical Co., Ltd.
发明人： MIYAO, Shuichi , OKADA, Junichi , NETSU, Shigeyoshi
IPC分类号： G01N23/20 , C01B33/02 , C01B33/035
CPC分类号： G01N23/20 , C01B33/02 , C01B33/021 , C01B33/035 , C30B13/00 , C30B29/06 , C30B29/605 , G01N23/207 , G01N2223/3306 , G01N2223/606
摘要： When the degree of crystalline orientation of polycrystalline silicon is evaluated by an X-ray diffraction method, each obtained disc-like sample 20 is disposed in a position where Bragg reflection from a Miller index face is detected and in-plane rotated at a rotational angle φ with the center of the disc-like sample 20 as the center of rotation, so that an X-ray-radiated region defined by a slit φ-scans over the principal surface of the disc-like sample 20, to determine a chart representing the dependence of the intensity of Bragg reflection from the Miller index face on the rotational angle (φ) of the disc-like sample 20, a baseline is determined from the chart, and the diffraction intensity value of the baseline is used as an estimative index of the degree of crystalline orientation.
摘要翻译：当多晶硅的结晶取向度被评价为X射线衍射法，对得到的各圆盘状样品20在从一个密勒指数面布拉格反射之被检测和在平面内以转动的位置被设置的旋转角度与Æ作为旋转中心的圆盘状的样品20的中心，所以没有由狭缝AE-扫描在所述圆盘状样品20的确定性矿的主表面限定的X射线辐射区域表示布拉格反射从密勒指数面之上的圆盘状样品20的旋转角度（AE）的强度的相关性的图表，基线是确定性从图表开采，以及基线的衍射强度值作为在结晶取向度的蒋梅鑫索引。

8. 发明公开

EP2736837A2 NANOSTRUCTURED BATTERY ACTIVE MATERIALS AND METHODS OF PRODUCING SAME 有权转让
标题翻译：活性物质用于生产纳米结构电池和方法
公开(公告)号：EP2736837A2
公开(公告)日：2014-06-04
申请号：EP12817748.2
申请日：2012-07-24
申请人： Oned Material LLC
发明人： CAO, Wanqing , ROBBINS, Virginia
IPC分类号： B82B3/00 , B82B1/00 , B01J23/72 , C01B31/02 , H01M4/04
CPC分类号： H01M4/366 , B01J21/18 , B01J23/72 , B01J37/0211 , C01B33/02 , C01B33/021 , C01B33/029 , C01P2004/16 , C01P2004/64 , C30B11/12 , C30B25/005 , C30B29/06 , C30B29/60 , H01M4/0428 , H01M4/0495 , H01M4/134 , H01M4/386 , H01M4/622
摘要： Methods for producing nanostructures from copper-based catalysts on porous substrates, particularly silicon nanowires on carbon-based substrates for use as battery active materials, are provided. Related compositions are also described. In addition, novel methods for production of copper-based catalyst particles are provided. Methods for producing nanostructures from catalyst particles that comprise a gold shell and a core that does not include gold are also provided.

10. 发明公开

EP2590248A3 Negative electrode active material for non-aqueous electrolyte secondary battery and method for manufacturing the same 有权
标题翻译：用于与非水电解质及其制造方法二次电池用负极活性物质
公开(公告)号：EP2590248A3
公开(公告)日：2014-01-01
申请号：EP12007399.4
申请日：2012-10-29
申请人： Shin-Etsu Chemical Co., Ltd.
发明人： Tetsuo, Nakanishi , Yoshiyasu, Yamada , Kazuyuki, Taniguchi
IPC分类号： H01M4/66 , H01M4/134 , H01M10/0525 , H01M4/1395 , H01M4/62 , C01B33/021 , H01M4/38 , B82Y30/00 , H01M4/04 , H01M4/02
CPC分类号： H01M4/386 , B82Y30/00 , C01B33/021 , C01P2002/72 , C01P2004/62 , C01P2004/64 , C01P2006/12 , H01M4/0421 , H01M4/134 , H01M4/622 , H01M10/0525 , Y02E60/122 , Y02P70/54
摘要： The present invention provides a method for manufacturing a negative electrode active material for a secondary battery that uses a non-aqueous electrolyte, including the steps of: depositing silicon according to an electron beam vapor-deposition method with metallic silicon as a raw material on a substrate of which temperature is controlled from 800 to 1100°C at a vapor deposition rate exceeding 1 kg/hr in the range of film thickness of 2 to 30 mm; and pulverizing and classifying the deposited silicon to obtain the negative electrode active material. As a result, there is provided a method for manufacturing a negative electrode active material of silicon particles as an active material useful for a negative electrode of a non-aqueous electrolyte secondary battery that is, while maintaining high initial efficiency and battery capacity of silicon, excellent in the cycle characteristics and has a reduced volume change during charge/discharge.

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