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11. 发明公开

EP3296261A1 METHOD FOR REGENERATING WEAKLY BASIC ION-EXCHANGE RESIN 有权
标题翻译：再生弱碱性离子交换树脂的方法
公开(公告)号：EP3296261A1
公开(公告)日：2018-03-21
申请号：EP17196935.5
申请日：2014-01-15
申请人： Shin-Etsu Chemical Co., Ltd.
发明人： ISHIDA, Masahiko , SAITO, Hiroshi , YOSHIDA, Atsushi
IPC分类号： C01B33/107 , B01J20/26 , B01J20/34 , C01B33/04 , B01J49/00 , B01J41/08 , B01J41/04 , B01J49/57 , B01J41/09 , B01J41/07 , C01B35/02
CPC分类号： B01J49/57 , B01J41/07 , B01J41/09 , C01B33/046 , C01B33/1071 , C01B33/10778 , C01B33/10784
摘要： The present invention provides a technique which allows stable use of an ion-exchange resin for removing boron impurities over a long period of time in the purification step of a silane compound or a chlorosilane compound. In the present invention, a weakly basic ion-exchange resin used for the purification of a silane compound and a chlorosilane compound is cleaned with a gas containing hydrogen chloride. When this cleaning treatment is used for the initial activation of the weakly basic ion-exchange resin, a higher impurity-adsorbing capacity can be obtained. Further, use of the cleaning treatment for the regeneration of the weakly basic ion-exchange resin allows stable use of the ion-exchange resin for a long time. This allows reduction in the amount of the resin used in a long-term operation and reduction in the cost of used resin disposal.
摘要翻译：本发明提供一种技术，其能够在硅烷化合物或氯硅烷化合物的纯化步骤中长期稳定地使用用于除去硼杂质的离子交换树脂。在本发明中，用含氯化氢的气体清洗用于硅烷化合物和氯硅烷化合物的纯化的弱碱性离子交换树脂。当该清洁处理用于弱碱性离子交换树脂的初始活化时，可以获得更高的杂质吸附能力。此外，使用弱碱性离子交换树脂再生的清洁处理可以长时间稳定地使用离子交换树脂。这允许减少长期操作中使用的树脂的量并降低使用的树脂处理的成本。

12. 发明公开

EP3156364A4 METHOD AND DEVICE FOR PRODUCING SODIUM BOROHYDRIDE 审中-公开
公开(公告)号：EP3156364A4
公开(公告)日：2018-01-10
申请号：EP15805904
申请日：2015-06-05
申请人： HYDRIC POWER SYSTEMS CO LTD
发明人： YOSHIZAKI ATSUHIRO
IPC分类号： C01B6/21 , C01B35/02
CPC分类号： C01B35/02 , B01J8/0015 , B01J8/085 , B01J8/10 , B01J2208/00752 , C01B3/00 , C01B3/001 , C01B6/21
摘要： A method and an apparatus for producing sodium borohydride that have excellent energy efficiency and production efficiency are provided. Using a production apparatus 20 comprising: a cylindrical reaction container 21; a cylindrical reaction portion 22 which is rotatably held in this reaction container 21 and in which sodium metaborate that is a raw material 1 and granular aluminum are housed together with a grinding medium 2; and a hydrogen introduction portion 23 for introducing hydrogen gas into the reaction portion 22 directly or via the reaction container 21, the sodium metaborate and the granular aluminum are reacted under a hydrogen atmosphere, while being rolled and ground with the grinding medium, to obtain sodium borohydride.

13. 发明授权

EP2707754B1 PROCEDE DE DEPOT DE BORE SUR UNE TOLE METALLIQUE POUR APPAREIL DE DETECTION DE NEUTRONS OU CHAMBRE D'IONISATION 有权
标题翻译： PROCESS FOR BOR对板中子探测器分隔法或电离室
公开(公告)号：EP2707754B1
公开(公告)日：2015-03-04
申请号：EP12716391.3
申请日：2012-04-19
申请人： O.T.N.D. - ONET TECHNOLOGIES NUCLEAR DECOMMISSIONING
发明人： ROTTNER, Bernard , PARTYKA, Stanislas
IPC分类号： G01T3/00 , C01B35/02
CPC分类号： G01T3/00 , C01B35/023 , G01T3/008

14. 发明公开

EP2735544A2 A reactor designed for chemical vapor deposition method and method of producing elemental boron and advanced ceramic powders with this reactor 有权转让
标题翻译：用于化学气相沉积方法设计反应器和方法用于生产单质硼和与该反应器先进的陶瓷粉末，
公开(公告)号：EP2735544A2
公开(公告)日：2014-05-28
申请号：EP13194718.6
申请日：2013-11-27
申请人： Ulusal Bor Arastirma Enstitusu (Boren)
发明人： Duman, Ismail , Agaogullari, Duygu , Balci, Ozge , Ovecoglu, Lufti
IPC分类号： C01B35/02 , C23C16/28 , C23C16/34 , C23C16/04 , C23C16/32 , C23C16/44 , C23C16/46 , F16L53/00 , F16L59/08 , C04B35/626 , B01J19/18 , C01B21/064 , C01B21/068
摘要： The invention relates to a reactor (1) designed for the chemical vapor deposition method employed in the production of elemental boron and advanced ceramic powders. The objective of the present invention is to provide a reactor design; which enables homogenous temperature distribution in the inner tube (2) where the reaction takes place thanks to its reflector (5), minimizes the energy losses occurring due to radiation; enables production of uniform, mono/multi-structured products in higher amounts compared to the conventional applications by means of the homogenous temperature distribution; and enables removal of the impurities in the product easily and completely; and to provide a production method for elemental boron and advanced ceramic powders by means of this reactor.
摘要翻译：本发明涉及一种设计用于在生产单质硼和先进的陶瓷粉末的使用的化学气相沉积法的反应器（1）。本发明的目的是提供一种反应器设计; 这使得在所述内管（2）其中发生反应由于其均匀的反射器的温度分布（5）最小化能量损失发生的由于辐射; 能够生产的均匀的，单/多结构性产品在相对于由所述均匀的温度分布的装置中的常规应用较高量; 启用和去除杂质在产品的轻松，完全通话; 并通过该反应器的装置，以提供对元素硼和先进的陶瓷粉末的制造方法。

15. 发明公开

EP2631217A1 Method for cyclically preparing boron and coproducing sodium cryolite using sodium fluoborate as intermediate material 失效
标题翻译：一种用于硼和同时生产钠的环状制造方法与氟硼酸钠冰晶石作为中间
公开(公告)号：EP2631217A1
公开(公告)日：2013-08-28
申请号：EP12195388.9
申请日：2012-12-04
申请人： Shenzhen Sunxing Light Alloys Materials Co., Ltd
发明人： Chen, Xuemin , Yu, Yueming , Ye, Qingdong , Yang, Jun , Zhou, Zhi
IPC分类号： C01B35/06 , C01B35/02 , C01B31/20
CPC分类号： C01B35/023 , B82Y30/00 , B82Y40/00 , C01B32/50 , C01B35/06 , C01F7/54 , C01F7/762 , C25C3/18
摘要： The disclosure discloses a method for cyclically preparing monomer boron and coproducing sodium cryolite using sodium fluoborate as an intermediate material, which includes the following steps: A) adding hydrofluoric acid to boric acid or boron oxide to enable a reaction to form fluoboric acid; B) adding a sodium carbonate aqueous solution to the fluoboric acid to enable a reaction to form the sodium fluoborate; C) putting the sodium fluoborate into a reactor, adding aluminium to react with the sodium fluoborate to form the monomer boron and sodium cryolite, or, putting the aluminium into the reactor, and adding the sodium fluoborate to react with the aluminium to form the monomer boron and sodium cryolite; D) extracting the sodium cryolite, sending the sodium cryolite to a rotary reaction kettle together with concentrated sulphuric acid to enable a reaction to form hydrogen fluoride gas and aluminium sodium sulphate, collecting the hydrogen fluoride gas and dissolving it into water to obtain the hydrofluoric acid; E) recycling the obtained hydrofluoric acid to Step A to leach the boric acid or boron oxide. The disclosure can recycle the coproduct sodium cryolite, thereby shortening the process of preparing monomer boron, reducing the comprehensive cost of production, improving the production efficiency and reducing environmental pollution.
摘要翻译：本公开盘松的方法用于循环地制备单体硼和氟硼酸使用钠作为中间材料，其包括以下步骤联产钠冰晶石：a）将氢氟酸与硼酸或氧化硼，以使反应以形成氟硼酸; B）加入碳酸钠溶液至wässrige氟硼酸，以使反应以形成氟硼酸钠; C）把氟硼酸钠到反应器中，添加铝与氟硼酸钠反应以形成单体硼和钠冰晶石，或者，把铝进入反应器，并添加氟硼酸钠，以与铝反应以形成所述单体硼和钠冰晶石; D）提取钠冰晶石，用浓硫酸一起发送钠冰晶石到旋转式反应釜中，以使反应形成氟化氢气体和硫酸铝钠，收集氟化氢气体，并将其溶解在水中以获得氢氟酸 ; E）回收获得的步骤A到浸出硼酸或氧化硼的氢氟酸。本发明可以回收副产物冰晶石钠，从而缩短制备单体硼，降低了生产成本全面，提高生产效率和减少环境污染的过程。

16. 发明公开

EP2294299A4 MONETIZING REMOTE GAS USING HIGH ENERGY MATERIALS 审中-公开
标题翻译：远能气体在高能材料上的单元化
公开(公告)号：EP2294299A4
公开(公告)日：2011-10-05
申请号：EP09758863
申请日：2009-04-09
申请人： EXXONMOBIL UPSTREAM RES CO
发明人： KELLEY BRUCE T , DECKMAN HARRY W , DAVIS STEPHEN MARK , HERSHKOWITZ FRANK
IPC分类号： F02C6/18 , C01B3/26 , C01B3/34 , C01B31/02 , C01B33/02 , C01B35/02 , F02C3/26
CPC分类号： C01B31/02 , C01B3/26 , C01B3/34 , C01B32/05 , C01B33/02 , C01B35/02 , C01B2203/0233 , C01B2203/0266 , C01B2203/0277 , C01B2203/1241 , G06Q99/00
摘要： The present application is directed to a method and system for monetizing energy. More specifically, the invention is directed to the economically efficient utilization of remote or stranded natural gas resources. The invention includes importing a high energy density material into an energy market and distributing the high energy density material (HEDM) therein. The HEDM is produced from reduction of a material oxide such as boria into the HEDM, which may be boron. The reduction utilizes remote hydrocarbon resources such as stranded natural gas resources.
摘要翻译：本申请涉及一种用于从能量获利的方法和系统。更具体地，本发明涉及经济上有效利用远程或搁浅天然气资源。本发明包括将高能量密度材料输入能源市场并在其中分配高能量密度材料（HEDM）。 HEDM通过将诸如硼酸的材料氧化物还原成可以是硼的HEDM来制备。减排利用遥远的碳氢化合物资源，如搁浅的天然气资源。

17. 发明授权

EP1893320B1 MATERIALS PURIFICATION BY TREATMENT WITH HYDROGEN-BASED PLASMA 有权
标题翻译：清洁材料通过用氢等离子体基
公开(公告)号：EP1893320B1
公开(公告)日：2009-12-09
申请号：EP06753692.0
申请日：2006-05-17
申请人： MPG Max-Planck-Gesellschaft zur Förderung der Wissenschaften e.V.
发明人： ALEKSEEVA, Anastasia , KOVNIR, Kirill , CHIZHOV, Pavel , BAITINGER, Michael , GRIN, Yuri
IPC分类号： B01D53/32 , C01B35/02 , B01D53/46
CPC分类号： B01D53/32 , B01D53/46 , B01D2251/202 , B01D2257/104 , B01D2259/818 , C01B35/023

18. 发明公开

EP0130311A2 Stable suspensions of boron, phosphorus, antimony and arsenic dopants 失效
标题翻译：硼，磷，锑或掺杂剂含有砷的稳定悬浮液。
公开(公告)号：EP0130311A2
公开(公告)日：1985-01-09
申请号：EP84105124.6
申请日：1984-05-07
申请人： AlliedSignal Inc.
发明人： Gupta, Arunava (NMI) , West, Gary Allen , Donlan, Jeffrey Peter
IPC分类号： C01B21/064 , C01B33/06 , C01B35/02 , H01L21/225 , B01J13/00
CPC分类号： C30B31/02 , H01L21/2225 , H01L21/2254 , H01L21/2257 , Y10S252/95 , Y10S252/951
摘要： Semiconductor doping compositions comprising a suspension of (a) a dopant material, in the form of finely divided spherical particles, such as P x Siy or B,Siy wherein x and y vary from 0.001 to 99.999 mole percent, (b) an effective amount of a thermally degradable polymeric organic binder such as polymethyl methacrylate; and (c) an amount of an organic solvent, such a cyclohexanone, sufficient to dissolve said polymeric organic binder, such as polymethylmethacrylate, and to disperse said dopant material are disclosed. Three onestep diffusion processes using the semiconductor doping compositions of the present invention for preparation of semiconductor materials having a wide range of sheet resistances and junction depths are also disclosed. The dopant materials selected for the semiconductor compositions of the present invention are less sensitive to moisture and chemical degradation and thereby afford greater processing latitude, are more reproducible and are less prone to create damage to and/or staining of the semiconductor substrate.

19. 发明公开

EP0007599A1 Synthesis of tetradecahydroundecaborate(-1) from borohydride ion 失效
标题翻译：硼氢化物离子合成十四碳烯十硼酸盐（-1）
公开(公告)号：EP0007599A1
公开(公告)日：1980-02-06
申请号：EP79102579.4
申请日：1979-07-20
申请人： UNION CARBIDE CORPORATION
发明人： Dunks, Gary Burr , Beard, Charles David, Dr.
IPC分类号： C01B35/02
CPC分类号： C01B35/00
摘要： The tetradecahydroundecaborate (-1) anion is synthesized from a metal borohydride by heating a suspension of the borohydride ion in a solvent, such as diglyme, with agitation at a temperature of from 85°C. to about 135°C. and adding an alkyl halide. The B 11 H 14 -anion obtained is useful in the synthesis of decarborane, an intermediate in formation a carborane-based polymers.
摘要翻译：通过在85℃的温度下在搅拌下加热硼氢化物离子在溶剂如二甘醇二甲醚中的悬浮液，由金属硼氢化物合成十四碳氢十硼酸盐（-1）阴离子。到约135℃。并加入烷基卤化物。所得到的B11H14-阴离子可用于合成十硼烷，一种形成碳硼烷基聚合物的中间体。

20. 发明公开

EP4373655A1 DYNAMICALLY CROSSLINKED TOUGH ADHESIVE WITH RECYCLABILITY 审中-实审
公开(公告)号：EP4373655A1
公开(公告)日：2024-05-29
申请号：EP22846488.9
申请日：2022-07-19
申请人： UT-Battelle, LLC
发明人： SAITO, Tomonori , RAHMAN, Anisur
IPC分类号： B29C65/52 , B29C65/54 , B32B37/12 , C01B35/02 , C08J3/05 , C08J3/07 , C08J3/12
CPC分类号： C09J11/02 , C08K5/55 , C08K5/0025 , C08K3/22 , C09J153/025 , C08K2201/00520130101 , C08K2003/222720130101 , C08K2003/224420130101 , C08K2003/224120130101 , C08K3/36

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