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1. 发明申请

WO2014174397A3 METHOD OF SYNTHESIS MOLECULES USING CATALYST AND COMPOSITES THEREOF 审中-公开
标题翻译：使用催化剂及其复合材料的合成分子的方法
公开(公告)号：WO2014174397A3
公开(公告)日：2015-04-02
申请号：PCT/IB2014060537
申请日：2014-04-08
申请人： MANDAL DR SWADHIN K , SANTRA SUBHANKAR
发明人： MANDAL DR SWADHIN K , SANTRA SUBHANKAR
IPC分类号： C07C25/24 , C07F5/02
CPC分类号： C07C45/68 , B01J23/44 , C07B37/04 , C07C1/321 , C07C17/263 , C07C25/18 , C07C37/18 , C07C41/30 , C07C51/353 , C07C67/343 , C07C201/12 , C07C209/68 , C07C253/30 , C07D209/42 , C07D213/16 , C07D213/30 , C07D213/82 , C07D215/04 , C07D235/08 , C07D257/04 , C07D333/08 , C07D493/22 , C07C205/11 , C07C211/45 , C07C255/50 , C07C255/55 , C07C205/04 , C07C49/784 , C07C39/15 , C07C47/546 , C07C69/76 , C07C43/205 , C07C63/331 , C07C15/14
摘要： A method to synthesis molecules is provided. The method employs a catalyst for a cross- coupling react ion to obtain the molecule. The method comprises coupling boronic acid and halide in presence of the catalyst having graphite oxide supported palladium nanoparticles, a solvent and a base by heating. The heating is performed at a temperature lower than the temperature at which the graphite oxide deforms. The molecule is a biaryl. The method further provides obtaining complexs such as boscalid, telmisartan, valsartan, and SPPARMγ.
摘要翻译：提供了合成分子的方法。该方法采用交联偶联反应离子的催化剂获得分子。该方法包括在具有氧化钯载体的钯纳米颗粒，溶剂和碱的催化剂存在下，使硼酸和卤化物偶合。加热在比石墨氧化物变形的温度低的温度下进行。分子是联芳基。该方法进一步提供获得复合物，例如boscalid，替米沙坦，缬沙坦和SPPARMγ。

2. 发明申请

WO2010117435A2 NO-CARRIER-ADDED NUCLEOPHILIC [F-18] FLUORINATION OF AROMATIC COMPOUNDS 审中-公开
标题翻译： NO-CARRIER-ADDED NUCLEOPHILIC [F-18]芳香化合物的氟化
公开(公告)号：WO2010117435A2
公开(公告)日：2010-10-14
申请号：PCT/US2010/001012
申请日：2010-04-01
申请人： THE REGENTS OF THE UNIVERSITY OF CALIFORNIA , SATYAMURTHY, Nagichettiar , BARRIO, Jorge, R.
发明人： SATYAMURTHY, Nagichettiar , BARRIO, Jorge, R.
IPC分类号： C07D319/06 , C07D263/04 , C07D239/10
CPC分类号： C07D319/06 , C07B59/00 , C07B2200/05 , C07C201/12 , C07C227/16 , C07C229/36 , C07D233/32 , C07D241/08 , C07D263/18 , C07D405/12 , C07D413/12 , C07C205/11
摘要： Phenyliodonium ylide derivatives substituted with electron donating as well as electron withdrawing groups on the aromatic ring are shown for use as precursors in aromatic nucleophilic substitution reactions. The iodonium ylide group is substituted by nucleophiles such as halide ions to provide the corresponding haloaryl derivatives. No- carrier-added [F-18]fluoride ion exclusively substitutes the iodonium ylide moiety in these derivatives and provides high specific activity F- 18 labeled fluoro derivatives. Protected L-dopa-6-iodonium ylide derivative have been synthesized as a precursors for the preparation of no-carrier-added 6-[F- 18]fluoro-L-dopa. The iodonium ylide group in this L-dopa.derivative is nucleophilically substituted by no-carrier-added [F-18]fluoride ion to provide a [F-18]fluoro intermediates which upon acid hydrolysis yielded 6-[F- 18]fluoro-L-dopa.
摘要翻译：显示了用芳族亲环取代反应的前体作为芳环上的给电子基团和吸电子基团取代的苯基碘鎓衍生物衍生物。碘鎓叶立德基团被诸如卤素离子的亲核试剂取代，得到相应的卤代芳基衍生物。无载体添加的[F-18]氟离子仅在这些衍生物中代替碘鎓叶立德，并提供高比活性F-18标记的氟衍生物。已经合成了保护的左旋多巴-6-碘鎓叶立德衍生物作为制备无载体添加的6- [F-18]氟-L-多巴的前体。该L-多巴胺衍生物中的碘鎓叶立德碱通过无载体添加的[F-18]氟离子进行亲核取代，得到[F-18]氟中间体，其在酸水解时产生6- [F-18]氟 -L-DOPA。

3. 发明申请

WO2008006574A2 VERFAHREN ZUM HERSTELLEN VON IN 1'-STELLUNG UNVERZWEIGTEN ALKYLNITROBENZOLEN UND ALKYLANILINEN AUS NITOTOLUOLEN 审中-公开
标题翻译： PRODUCING IN POSITION 1'-直链烷基方法苯胺ALKYLNITROBENZOLEN AND OFF NITOTOLUOLEN
公开(公告)号：WO2008006574A2
公开(公告)日：2008-01-17
申请号：PCT/EP2007/006176
申请日：2007-07-12
申请人： BAYER CROPSCIENCE AG , STRAUB, Alexander
发明人： STRAUB, Alexander
IPC分类号： C07C205/06 , C07C205/12 , C07C209/36 , C07C209/70
CPC分类号： C07C205/06 , C07C205/11 , C07C205/12 , C07C205/34 , C07C209/32 , C07C209/70 , C07C211/52 , C07C2601/02 , C07C211/45 , C07C211/46
摘要： Die vorliegende Erfindung betrifft ein Verfahren zum Herstellen von Nitrobenzolderivaten und Anilinderivaten, die als Zwischenprodukte für fungizid wirksame Alkylanilide Bedeutung haben.
摘要翻译：本发明涉及一种用于制备硝基苯衍生物和其具有苯胺衍生物，中间体，用于杀真菌有效alkylanilides重要性的方法。

4. 发明申请

WO2007048556A1 HETEROCYCLIC AMIDE DERIVATIVES USEFUL AS MICROBIOCIDES 审中-公开
标题翻译：杂环酰胺衍生物作为微生物有用
公开(公告)号：WO2007048556A1
公开(公告)日：2007-05-03
申请号：PCT/EP2006/010185
申请日：2006-10-23
申请人： SYNGENTA PARTICIPATIONS AG , TOBLER, Hans , WALTER, Harald , EHRENFREUND, Josef , CORSI, Camilla
发明人： TOBLER, Hans , WALTER, Harald , EHRENFREUND, Josef , CORSI, Camilla
IPC分类号： C07D277/56 , C07D231/14 , C07D213/89 , C07D207/46 , C07D207/34 , C07C211/61 , C07C205/45 , C07C205/37 , C07C205/12 , C07C205/06 , A01N43/36 , A01N43/40 , A01N43/56 , A01N43/78
CPC分类号： C07C205/06 , A01N43/32 , A01N43/36 , A01N43/40 , A01N43/56 , A01N43/647 , A01N43/76 , A01N43/78 , C07C205/11 , C07C205/12 , C07C205/37 , C07C205/45 , C07C211/61 , C07C2603/66 , C07D207/34 , C07D207/46 , C07D213/89 , C07D231/14 , C07D249/04 , C07D263/34 , C07D277/56 , C07D327/06
摘要： The invention relates to a fungicidally active compound of formula (I): where Het is a 5- or 6-membered heterocyclic ring containing one to three heteroatoms, each independently selected from oxygen, nitrogen and sulphur, the ring being substituted by the groups R 6 , R 7 and R 8 ; R 1 is hydrogen, C 1-4 alkyl, C 1-4 haloalkyl, C 1-4 alkoxy, C 1-4 haloalkoxy, CH 2 C≡CR 9 , CH 2 CR 10 =CHR 11 , CH=C=CH 2 or COR 12 ; R 2 and R 3 are each, independently, hydrogen, halo, C 1-4 alkyl, C 1-4 alkoxy, C 1-4 haloalkyl or C 1-4 haloalkoxy; R 4 and R 5 are each independently selected from halo, cyano and nitro; or one of R 4 and R 5 is hydrogen and the other is selected from halo, cyano and nitro; R 6 , R 7 and R 8 are each, independently, hydrogen, halo, cyano, nitro, C 1-4 alkyl, C 1-4 haloalkyl, C 1-4 alkoxy(C 1-4 )alkyl, C 1-4 haloalkoxy(C 1-4 )alkyl or C 1-4 haloalkoxy, provided that at least one of R 6 , R 7 and R 8 is not hydrogen; R 9 , R 10 and R 11 are each, independently, hydrogen, halo, C 1-4 alkyl, C 1-4 haloalkyl or C 1-4 alkoxy(C 1-4 )alkyl; and R 12 is hydrogen, C 1-6 alkyl, C 1-6 haloalkyl, C 1-4 alkoxy(C 1-4 )alkyl, C 1-4 alkylthio(C 1-4 )- alkyl, C 1-4 alkoxy or aryl; to the preparation of these compounds, to novel intermediates used in the preparation of these compounds, to agrochemical compositions which comprise at least one of the novel compounds as active ingredient, to the preparation of the compositions mentioned and to the use of the active ingredients or compositions in agriculture or horticulture for controlling or preventing infestation of plants by phytopathogenic microorganisms, preferably fungi.
摘要翻译：本发明涉及式（I）的杀真菌活性化合物：其中Het是含有一至三个杂原子的5-或6-元杂环，各自独立地选自氧，氮和硫，该环被基团R R＆lt; 6＆gt;，＆lt; 7＆gt;和＆lt; 8＆gt; R 1是氢，C 1-4 - 烷基，C 1-4 - 卤代烷基，C 1-4 - 烷氧基 C 1-4卤代烷氧基，CH 2 C = CR 9，CH 2 CR 10， CH = CHR 11，CH = C = CH 2或COR 12; R 2和R 3各自独立地为氢，卤素，C 1-4烷基，C 1-4烷基， C 1-4烷氧基，C 1-4卤代烷基或C 1-4卤代烷氧基; R 4和R 5各自独立地选自卤素，氰基和硝基; 或者R 4和R 5中的一个是氢，另一个选自卤素，氰基和硝基; R 6，R 7和R 8各自独立地为氢，卤素，氰基，硝基，C 1-4烷基， C 1-4烷基，C 1-4卤代烷基，C 1-4烷氧基（C 1-4 - ）烷基，C 1 -4个卤代烷氧基（C 1-4 - ）烷基或C 1-4 - 卤代烷氧基，条件是R 6 - R 7和R 8不是氢; R 9，R 10和R 11各自独立地为氢，卤素，C 1-4烷基 C 1-4卤代烷基或C 1-4烷氧基（C 1-4 - ）烷基; R 12是氢，C 1-6烷基，C 1-6卤代烷基，C 1-4烷基，烷氧基（C 1-4-4烷基）烷基，C 1-4烷硫基（C 1-4烷基） - 烷基，C 1〜 4烷氧基或芳基; 涉及这些化合物的制备，用于制备这些化合物的新型中间体，包括至少一种新化合物作为活性成分的农用化学组合物，所述组合物的制备以及使用活性成分或用于通过植物病原微生物，优选真菌控制或预防植物感染的农业或园艺成分。

5. 发明申请

WO2006092429A1 VERFAHREN ZUR HERSTELLUNG SUBSTITUIERTER BIPHENYLE 审中-公开
标题翻译：用于生产取代BIPHENYLS
公开(公告)号：WO2006092429A1
公开(公告)日：2006-09-08
申请号：PCT/EP2006/060400
申请日：2006-03-02
申请人： BASF AKTIENGESELLSCAHFT , ENGEL, Stefan , OBERDING, Tanja
发明人： ENGEL, Stefan , OBERDING, Tanja
IPC分类号： C07C201/12 , C07C205/12
CPC分类号： C07C209/68 , C07C201/12 , C07C211/52 , C07C205/11
摘要： Verfahren zur Herstellung substituierter Biphenyle (I) wobei R 1 = Nitro, Amino oder NHR 3 . R 2 = CN, NO 2 , Halogen, C 1 C 6 -Alkyl, C 2 -C 6 -Alkenyl, C 2 -C 6 -Alkiny,C 1 -C 6 Alkoxy, C 1 -C 6 Haloalkyl -C 1 -C 6 -Alkylcarbonyl oder Phenyl; R 3 = C 1 -C 4 -AIkYl, C 2 -C 4 -Alkenyl oder C 2 -C 4 -Al kinyl; m = 1 oder 2; n = 0 bis 3; dadurch gekennzeichnet, dass man eine Verbindung (II) in Gegenwart einer Base und eines Palladium-Katalysators ausgewählt aus der Gruppe: a) Palladium-Triaryl- oder Trialkylphosphinkomplex mit Palladium in der Oxidationsstufe Null, b) Salz des Palladiums in Gegenwart von Triaryl- oder Trialkylphosphin als Komplexligand oder c) gegebenenfalls auf Träger aufgezogenes metallisches Palladium, in Gegenwart von Triaryl- oder Trialkylphosphin in einem Lösungsmittel mit einer Diphenylborinsäure (III) umsetzt.
摘要翻译：用于制备取代的联苯（I）方法，其中R ^{1 =硝基，氨基或NHR ^{3 。 [R ^{2 = CN，NO _{2 ，卤素，C _{1 C _{6 烷基，C _{2 -C _{6 烯基，C _{2 -C _{6 -Alkiny，C _{1 -C _{6 烷氧基，C _{1 -C _{6 卤代烷基，-C _{1 -C _{6 烷基羰基或苯基; [R _{3 = C _{1 -C _{4 - 烷基，C _{2 -C _{4 链烯基或C _{2 -C _{4 -Al kinyl; M = 1或2; n = 0至3; 其特征在于，在碱和钯催化剂选自存在下化合物（II）：a）以零氧化态的钯 - 三芳基膦或Trialkylphosphinkomplex用钯，b）中钯的盐在三芳基的存在或三烷基膦作为配位体复合物或c）任选应用于支持金属钯，在三芳基或三烷基的存在下，在溶剂中与一个二苯基硼酸（III）。}}}}}}}}}}}}}}}}}}}}}}}

6. 发明申请

WO2005061417A3 FLUORODENITROGENATION METHOD 审中-公开
标题翻译：荧光法
公开(公告)号：WO2005061417A3
公开(公告)日：2005-11-17
申请号：PCT/FR2004003241
申请日：2004-12-15
申请人： RHODIA CHIMIE SA , SAINT-JALMES LAURENT , VIDAL THIERRY
发明人： SAINT-JALMES LAURENT , VIDAL THIERRY
IPC分类号： C07B39/00 , C07C17/093 , C07C205/11
CPC分类号： C07B39/00 , C07C17/093 , C07C201/12 , C07C22/08 , C07C205/11
摘要： The invention relates to a fluorodenitrogenation method which aims to eliminate nitrogen from carbon-nitrogen multiple bonds. The inventive method consists in subjecting a substrate bearing said carbon-nitrogen multiple bond to the action of a reagent comprising a compound that can form a precursor of nitrosonium (NO ) and comprising hydrofluoric acid or one of the acid complexes thereof. The invention also relates to the applications of said method for functionalisation into fluoromethyl or difluoromethyl groups.
摘要翻译：本发明涉及旨在从碳 - 氮重复键中除去氮的氟代脱氮方法。本发明的方法在于使具有所述碳 - 氮多重键的基材经受包含可形成亚硝鎓（NO +）前体且包含氢氟酸或其酸复合物之一的化合物的试剂的作用。本发明还涉及所述用于官能化成氟甲基或二氟甲基基团的方法的应用。

7. 发明申请

WO01012577A1 MOLYBDENUM TRIOXIDE CATALYZED FLUORINATION REACTIONS 审中-公开
标题翻译：三氧化钼催化氧化反应
公开(公告)号：WO01012577A1
公开(公告)日：2001-02-22
申请号：PCT/GB2000/002195
申请日：2000-06-07
IPC分类号： C07B39/00 , C07C17/20 , C07C205/11 , C07C22/04 , C07C22/06
CPC分类号： C07C205/11 , C07B39/00 , C07C17/206 , C07C22/08
摘要： Disclosed is a method of fluorinating a substrate having general formulae (I) or (II) where each R is independently selected from halogen, alkyl from C1 to C12, aryl from C6 to C12, alkoxide from C1 to C12, aryloxide from C6 to C12, nitro, amino, alkylamino from C1 to C12, and arylamino from C6 to C12, each X is independently selected from halogen and at least one X is chlorine or bromine, each m is independently selected from 0 to 5, n is 0 or 1, p is 0 or 1, q is 0 or 1 and n + p + q is 1. The substrate is heated to a temperature of about 40 to about 100 DEG C and is reacted with a fluorinating agent in the presence of about 0.05 to about 2 wt% molybdenum trioxide. The composition of the substrate, the catalyst and the fluorinating agent is also dislosed.
摘要翻译：公开了一种氟化具有通式（I）或（II）的底物的方法，其中每个R独立地选自卤素，C1至C12的烷基，C6至C12的芳基，C1至C12的烷氧基，C6至C12的芳氧基硝基，氨基，C1至C12的烷基氨基和C6至C12的芳基氨基，每个X独立地选自卤素，至少一个X为氯或溴，m各自独立地选自0至5，n为0或1 ，p为0或1，q为0或1，n + p + q为1.将基材加热至约40至约100℃的温度，并与氟化剂在约0.05至约2重量％的三氧化钼。底物，催化剂和氟化剂的组成也被封闭。

8. 发明申请

WO99006373A1 METHOD FOR PRODUCING 2-(3-PYRAZOLYL-OXYMETHYLENE) NITROBENZENES 审中-公开
标题翻译：用于生产2-（3-吡唑基 - 氧亚甲基）硝基苯
公开(公告)号：WO99006373A1
公开(公告)日：1999-02-11
申请号：PCT/EP1998/004490
申请日：1998-07-20
IPC分类号： C07D231/20 , C07B39/00 , C07C205/11 , C07D231/08 , C07D231/22
CPC分类号： C07D231/08 , C07C201/12 , C07C205/11
摘要： The invention relates to a method for producing 2-(3-pyrazolyl-oxymethylene) nitrobenzene derivatives of formula (I), wherein the substituents and indices have the meaning given in the Description, by bromination of an o-nitrotoluene of formula (II) and subsequent reaction with a 3-hydroxypyrazol of formula (IV).
摘要翻译：一种用于式（I），其中取代基和指数具有说明书中给出的含义的2-（3-吡唑基 - 氧亚甲基）硝基苯衍生物的制备过程中，由式（II）的邻硝基甲苯的溴化，并用随后的反应下式的3-羟基吡（IV）。

9. 发明申请

WO9728122A3 PROCESS FOR PREPARING DIKETONE COMPOUNDS 审中-公开
标题翻译：制备二酮化合物的方法
公开(公告)号：WO9728122A3
公开(公告)日：1997-10-02
申请号：PCT/EP9700370
申请日：1997-01-28
申请人： RHONE POULENC AGROCHIMIE , PEVERE VIRGINIE , GADRAS ALAIN , CRAMP SUSAN MARY , ELLWOOD CHARLES WALTER
发明人： PEVERE VIRGINIE , GADRAS ALAIN , CRAMP SUSAN MARY , ELLWOOD CHARLES WALTER
IPC分类号： B01J31/02 , C07B61/00 , C07C201/12 , C07C205/11 , C07C205/45 , C07C319/14 , C07C319/20 , C07C323/22
CPC分类号： C07C205/11 , C07C205/45 , C07C319/20 , C07C2601/02 , C07C323/22
摘要： The invention relates to a process for preparing compounds of formula (I), wherein R2 is lower alkyl; or phenyl optionally substituted by from one to five groups which may be the same or different selected from lower alkyl, lower haloalkyl, halogen and -SR4; R3 is halogen, lower alkyl, lower haloalkyl, lower alkoxy, lower haloalkoxy, -S-alkyl, cycloalkyl having from 3 to 7 carbon atoms in the ring, alkenyl or alkynyl having from 3 to 7 carbon atoms, or -(CR5R6)q-SR2 wherein q is one or two; R4 is lower alkyl; R5 and R6 independently represent hydrogen, lower alkyl or lower haloalkyl; and n is zero or an integer from one to three; to intermediate compounds used in preparing compounds of formula (II), and processes for preparing such compounds.
摘要翻译：一种制备下式化合物的方法：其中R2是低级烷基; 或任选被一至五个相同或不同的基团取代的苯基，它们是低级烷基，低级卤代烷基，卤素或-SR 4; 或R 3为卤素，低级烷基，低级卤代烷基，低级烷氧基，低级卤代烷氧基，-S-烷基，环中具有3-7个碳原子的环烷基，具有3-7个碳原子的烯基或炔基，或 - （CR5R6） - 其中q是1或2; R4是低级烷基; R5和R6独立地表示氢，低级烷基或低级卤代烷基; 并且n为0或1至3的整数; 下式的中间体化合物及其制备方法。

10. 发明申请

WO1997033846A1 PROCESS FOR PREPARING NITROBIPHENYLENE 审中-公开
标题翻译：用于生产nitrobiphenyls
公开(公告)号：WO1997033846A1
公开(公告)日：1997-09-18
申请号：PCT/EP1997001128
申请日：1997-03-06
申请人： BASF AKTIENGESELLSCHAFT , EICKEN, Karl , GEBHARDT, Joachim , RANG, Harald , RACK, Michael , SCHÄFER, Peter
发明人： BASF AKTIENGESELLSCHAFT
IPC分类号： C07B37/04
CPC分类号： C07B37/04 , C07C201/12 , C07C253/30 , C07C205/11
摘要： The invention concerns a process for preparing nitrobiphenylene of formula (I) wherein m stands for 1 or 2, R means halogen, R' or OR', R' being a C-organic group which can carry groups which are inert in the reaction conditions, n stands for 0, 1, 2 or 3 and, if n is 2 or 3, the R groups can also be different. According to the invention, a chloronitrobenzene of formula (II) is reacted in the presence of a palladium catalyst and a base in a solvent with a phenyl boric acid (IIIa), one of its alkyl esters of formula (IIIb), R meaning C1-C6 alkyl, or one of its anhydrides. The compounds (I) are suitable as initial products for biphenylamines which are in turn intermediate products for fungicidal plant-growth substances.
摘要翻译：一种用于制备式（I），其中m是1或2的nitrobiphenyls方法中，R是卤素，R“或OR”，其中R“是一个C-有机基团，其可以携带在反应条件下惰性的基团，其中 n为0，1，2或3，且在n为2或3的情况下，基团R可以是不同的，由式（II）的氯硝基苯在钯催化剂的存在下和在碱反应溶剂中与苯基硼酸（IIIA）式（IIIb）的烷基酯，其中，R <1>的含义C1-C6烷基，或其酸酐反应。化合物（I）是作为中间体联苯胺类，这又是用于杀真菌的作物保护活性成分的中间体是有用的。

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