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1. 发明申请

WO1998014524A1 AQUEOUS INK COMPOSITIONS 审中-公开
标题翻译：水份油墨组合物
公开(公告)号：WO1998014524A1
公开(公告)日：1998-04-09
申请号：PCT/GB1997002555
申请日：1997-09-19
申请人： ZENECA LIMITED , HOLBROOK, Mark , MEYRICK, Barry, Huston
发明人： ZENECA LIMITED
IPC分类号： C09D11/00
CPC分类号： C09D11/30 , C09B23/143 , C09B29/0037 , C09B29/0081 , C09B29/0809 , C09B53/02 , C09D11/328
摘要： An ink composition comprising water, a water-dissipatable polyester, a disperse dye or a solvent soluble dye or a mixture of such dyes, a water-immiscible organic solvent and a water miscible organic solvent. The inks are useful in ink jet printers.
摘要翻译：一种油墨组合物，其包含水，可水分散的聚酯，分散染料或溶剂可溶性染料或这些染料的混合物，与水不混溶的有机溶剂和水混溶性有机溶剂。油墨可用于喷墨打印机。

2. 发明申请

WO1994010248A1 DYES 审中-公开
标题翻译：染料
公开(公告)号：WO1994010248A1
公开(公告)日：1994-05-11
申请号：PCT/GB1993002158
申请日：1993-10-20
申请人： ZENECA LIMITED , CAVANAGH, Denise , JAMES, Mark, Robert , MEYRICK, Barry, Huston , WIGHT, Paul
发明人： ZENECA LIMITED
IPC分类号： C09B23/00
CPC分类号： C09B67/0034 , C09B23/0091 , Y10S8/921 , Y10S8/922 , Y10S8/924 , Y10S8/926
摘要： A pyrrolidone dye of Formula (1), wherein: D is a group of Formula (2), or a group of Formula (3), or a group of Formula (4), R is alkyl, cycloalkyl, aryl, alkenyl or aralkyl each of which may be optionally substituted; R is optionally substituted C7-20-alkyl; or R and R together with the nitrogen atom to which they are attached form a pyrrolidino or piperidino ring; R is alkyl, alkenyl or aralkyl each of which may be optionally substituted or -COR in which R is -H or alkyl, phenyl, cycloalkyl or aralkyl each of which may be optionally substituted or -H; and R is an electron withdrawing group; R is optionally substituted C1-6-alkyl; or R and R together with the nitrogen atom to which they are attached form a piperidino or pyrrolidino ring; R , R , R and R each independently is alkyl, cycloalkyl, aryl, alkenyl or aralkyl each of which may be optionally substituted or -H; W is oxygen or sulphur; Z is a direct link or N-R in which R is -H or optionally substituted alkyl; Ring A is unsubstituted apart from the -NR R group or is substituted by from 1 to 4 further groups; Ring B is unsubstituted or substituted by from 1 to 3 groups; provided that when D is a group of Formula (2) and R and R are both allyl that R is not -CN or that when D is a group of Formula (3) that R and R are different and R is not -C2H5, -C3H7 or -C4H9 when R is -C2H4phenyl, -C3H6phenyl and ethyl substituted by -OH, -CN, -OCH3, -NHCOCH3, -Ophenyl and -NHSO2CH3 or that at least one of R and R is branched chain alkyl except for 3-(4-(N-ethyl-N-ethoxyethoxyethylamino)phenyl)-4-cyano-5-dicyanomethylidene-2-oxo-2,5-dihydropyrrole and 3-(4-(N,N-di-n-octylamino)phenyl)-4-cyano-5-dicyanomethylidene-2-oxo-2,5-dihydropyrrole. The dyes and dye mixtures produce blue to green shades on synthetic textile materials such as polyester which have good build up and good light- and wet-fastness.
摘要翻译：式（1）的吡咯烷酮染料，其中：D是式（2）的基团，或式（3）的基团或式（4）的基团，R 1是烷基，环烷基，芳基，烯基或芳烷基，其各自可以任选被取代; R 2是任选取代的C 3-20 - 烷基; 或R 1和R 2与它们所连接的氮原子一起形成吡咯烷子基或哌啶子基环; R 3是烷基，烯基或芳烷基，其各自可以是任选取代的或-COR，其中R是-H或烷基，苯基，环烷基或芳烷基，其各自可以是任选取代的或-H; R 4为吸电子基团; R 6是任选取代的C 1-6 - 烷基; 或R 1和R 6与它们所连接的氮原子一起形成哌啶子基或吡咯烷子基环; R 7，R 8，R 9和R 10各自独立地是烷基，环烷基，芳基，烯基或芳烷基，其各自可以是任选取代的或-H; W是氧或硫; Z是直链或N-R 11，其中R 11是-H或任选取代的烷基; 除了-NR 1 R 2基团之外，环A是未取代的或被其它1至4个其它基团取代; 环B是未取代的或被1至3个基团取代; 条件是当D是式（2）的基团且R 1和R 2都是R 4不是-CN的烯丙基时，或当D是式（3）的基团时，R 1 >和R 6不同，当R 6为-C 2 H 4苯基，-C 3 H 6苯基和被-OH，-CN，-OCH 3，-NHCOCH 3取代的乙基时，R 1不为-C 2 H 5，-C 3 H 7或-C 4 H 9， - 苯基和-NHSO 2 CH 3，或者R 1和R 6中的至少一个是支链烷基，除了3-（4-（N-乙基-N-乙氧基乙氧基乙基氨基）苯基）-4-氰基-5-二氰基亚甲基 -2-氧代-2,5-二氢吡咯和3-（4-（N，N-二正辛基氨基）苯基）-4-氰基-5-二氰基亚甲基-2-氧代-2,5-二氢吡咯。染料和染料混合物在合成纺织材料如聚酯上产生蓝色至绿色的色调，其具有良好的聚集性和良好的耐光牢度和耐湿牢度。

3. 发明申请

WO1996034919A1 INK JET PRINTING INK 审中-公开
标题翻译：喷墨打印墨水
公开(公告)号：WO1996034919A1
公开(公告)日：1996-11-07
申请号：PCT/GB1996000995
申请日：1996-04-26
申请人： ZENECA LIMITED , GUNN, Janet , HOLBROOK, Mark , LAVERY, Aidan, Joseph
发明人： ZENECA LIMITED
IPC分类号： C09D11/00
CPC分类号： C09D11/38
摘要： Ink compositions comprising an aqueous medium containing: (1) at least one water-soluble dye; (2) at least one cyclic ester or amide of formula (1), wherein m is a whole number from 3 to 5 and X represents -O- or -N(R)- in which R represents hydrogen, alkyl or substituted alkyl; (3) at least one hydroxy compound selected from polyhydroxy compounds having at least four hydroxy groups, optionally substituted cycloalkanols, cyclohexane dimethanol, benzyl alcohol, benzene dimethanol, phenol and polyhydroxybenzenes, and (4) at least one water-soluble organic solvent selected from alkanediols, alkanetriols, ether glycols and thioether glycols and suitable for use in ink jet printing processes for coloration of substrates such as paper or overhead projector slides.
摘要翻译：包含水性介质的油墨组合物含有：（1）至少一种水溶性染料; （2）至少一种式（1）的环酯或酰胺，其中m是3至5的整数，X表示-O-或-N（R） - ，其中R表示氢，烷基或取代的烷基; （3）选自具有至少四个羟基的多羟基化合物，任选取代的环烷醇，环己烷二甲醇，苄醇，苯二甲醇，苯酚和多羟基苯的至少一种羟基化合物，和（4）至少一种选自以下的水溶性有机溶剂：链烷二醇，烷三醇，醚二醇和硫醚二醇，适用于喷墨印刷工艺，用于着色诸如纸或高架投影仪载玻片的基材。

4. 发明申请

WO1995034024A1 PRINTING PROCESS 审中-公开
标题翻译：印刷工艺
公开(公告)号：WO1995034024A1
公开(公告)日：1995-12-14
申请号：PCT/GB1995001122
申请日：1995-05-18
申请人： ZENECA LIMITED , CARR, Kathryn , HOLBROOK, Mark , FERGUSON, Ian
发明人： ZENECA LIMITED
IPC分类号： G03C07/06
CPC分类号： C09D11/30 , B41M3/003 , C03C17/32 , C08F8/30 , C09B29/0037 , C09B29/3656 , G02B5/223
摘要： A process for preparing an optical filter comprising a coloured cross-linked polymeric coating on a transparent substrate, which comprises applying to the substrate, by a printing process, a mixture comprising one or more polymer precursor(s), and one or more dye(s) having one or more heterocyclic NH group(s) or one or more substituent(s) capable of forming a covalent bond with the polymeric precursor, and thereafter curing the mixture. The invention also provides formulations comprising one or more polymer precursors and dyes, optical filters, and a novel dye.
摘要翻译：一种制备光学滤光器的方法，包括在透明基底上的着色的交联聚合物涂层，其包括通过印刷方法将包含一种或多种聚合物前体和一种或多种染料（ s），其具有一个或多个杂环NH基团或一个或多个能够与聚合物前体形成共价键的取代基，然后固化该混合物。本发明还提供包含一种或多种聚合物前体和染料，光学过滤器和新型染料的配方。

5. 发明申请

WO1997019948A1 COMPOUND, PREPARATION AND USE 审中-公开
标题翻译：化合物，制备和使用
公开(公告)号：WO1997019948A1
公开(公告)日：1997-06-05
申请号：PCT/GB1996002545
申请日：1996-10-18
申请人： ZENECA LIMITED , THETFORD, Dean , HOLBROOK, Mark
发明人： ZENECA LIMITED
IPC分类号： C07F09/09
CPC分类号： B01F17/005 , C07F9/091 , C08G63/6922 , C09D7/45 , C09D11/03
摘要： A dispersant which is a phosphate ester of a block copolymer of formula MeO(C2H4O)m(PES)n-H wherein PES is derived from epsilon -caprolactone, m is 5-60, n is 2-30 and the MW of MeO(C2H4O)m is greater than the MW of (PES)n and use in aqueous-based paints and printing inks.
摘要翻译：作为式MeO（C 2 H 4 O）m（PES）nH的嵌段共聚物的磷酸酯的分散剂，其中PES衍生自ε-己内酯，m为5-60，n为2-30，MeO（C 2 H 4 O） m大于（PES）n的MW，并用于水性油漆和印刷油墨。

6. 发明申请

WO1998014525A1 AQUEOUS INK COMPOSITIONS 审中-公开
标题翻译：水份油墨组合物
公开(公告)号：WO1998014525A1
公开(公告)日：1998-04-09
申请号：PCT/GB1997002557
申请日：1997-09-19
申请人： ZENECA LIMITED , HOLBROOK, Mark , MEYRICK, Barry , BRADBURY, Roy
发明人： ZENECA LIMITED
IPC分类号： C09D11/00
CPC分类号： C09D11/328 , C09B23/143 , C09B29/0037 , C09B29/0081 , C09B29/0809 , C09B29/081 , C09B53/02
摘要： An ink comprising water, a water-dissipatable polymer and a dye, wherein the dye carries a group of formula (1) wherein: R is optionally substituted branched chain alkyl; and R is H, optionally substituted alkyl or optionally substituted aryl. The inks are useful in ink jet printers.
摘要翻译：一种包含水，可水分散的聚合物和染料的油墨，其中所述染料含有式（1）的基团，其中：R 1是任选取代的支链烷基; 和R 2是H，任选取代的烷基或任选取代的芳基。油墨可用于喷墨打印机。

7. 发明申请

WO1998014523A1 AQUEOUS INK COMPOSITIONS 审中-公开
标题翻译：水份油墨组合物
公开(公告)号：WO1998014523A1
公开(公告)日：1998-04-09
申请号：PCT/GB1997002547
申请日：1997-09-19
申请人： ZENECA LIMITED , HOLBROOK, Mark , MEYRICK, Barry , BRADBURY, Roy
发明人： ZENECA LIMITED
IPC分类号： C09D11/00
CPC分类号： C09D11/328 , C09B23/143 , C09B29/0037 , C09B29/0081 , C09B29/0809 , C09B53/02
摘要： An ink comprising water, a water-dissipatable polymer and a dye of formula (1), wherein R is optionally substituted alkyl or optionally substituted aryl; R is H, optionally substituted alkyl or optionally substituted aryl; R is H or optionally substituted alkyl; and R and R are each independently optionally substituted alkyl or optionally substituted aryl, or R and R together with the CH group to which they are attached from an optionally substituted 5- or 6-membered ring. Also claimed are dyes and ink jet printing processes.
摘要翻译：一种包含水，水分散性聚合物和式（1）染料的油墨，其中R 1为任选取代的烷基或任选取代的芳基; R 2是H，任选取代的烷基或任选取代的芳基; R 5是H或任选取代的烷基; 并且R 3和R 4各自独立地是任选取代的烷基或任选取代的芳基，或者R 3和R 4与它们所连接的CH基团可任意取代的5-或6-元杂环，元环。还要求的是染料和喷墨印刷方法。

8. 发明申请

WO1997019748A1 PHOSPHATE ESTERS OF POLYALKYLENE ETHER BLOCK COPOLYMERS AND THEIR USE AS DISPERSANTS 审中-公开
标题翻译：聚乙烯醚嵌段共聚物的磷酸酯及其作为分散剂的使用
公开(公告)号：WO1997019748A1
公开(公告)日：1997-06-05
申请号：PCT/GB1996002544
申请日：1996-10-18
申请人： ZENECA LIMITED , THETFORD, Dean , HOLBROOK, Mark
发明人： ZENECA LIMITED
IPC分类号： B01F17/00
CPC分类号： C07F9/091 , B01F17/0085 , C08G65/327 , C09B67/0085 , C09D7/45 , C09D11/03
摘要： A dispersant which is a phosphate ester of a polyalkylene ether block copolymer of formula MeO(C2H4O)m(C3H6O)n-H wherein m and n are each, independently, 2 to 60 and use in aqueous based paints and printing inks.
摘要翻译：作为式MeO（C 2 H 4 O）m（C 3 H 6 O）n -H的聚亚烷基醚嵌段共聚物的磷酸酯的分散剂，其中m和n各自独立地为2至60，并且用于水基涂料和印刷油墨。

9. 发明申请

WO1998029507A1 PLASTISOL COMPOSITIONS 审中-公开
标题翻译： PLASTISOL组合物
公开(公告)号：WO1998029507A1
公开(公告)日：1998-07-09
申请号：PCT/GB1996003246
申请日：1996-12-31
申请人： ZENECA LIMITED , OVEREND, Andrew, Stuart , PADGET, John, Christopher , COOPER, David, Henry
发明人： ZENECA LIMITED
IPC分类号： C08L33/06
CPC分类号： C08L33/06 , B29C2793/0081 , B29D2030/1685 , C09D133/06 , C08L2666/02 , C08L2666/28
摘要： Acrylic plastisol composition comprising a plasticiser component, a plasticiser compatible acrylic polymer powder component of primary particle size >/=0.4 mu m and preferably not more than 30 mu m, and Tg >/=65 DEG C, and a plasticiser incompatible polymer powder component, where both polymers are preformed, are present in the weight ratio 95:5 to 40:60, and in combination are compatibly formulated with the plasticiser component.
摘要翻译：丙烯酸增塑剂组合物，其包含增塑剂组分，一次粒径≥0.4μm，优选不大于30μm，Tg> = 65℃的增塑剂相容的丙烯酸类聚合物粉末组分和增塑剂不相容的聚合物粉末组分，其中两种聚合物都被预先形成，其重量比为95:5至40:60，并且与增塑剂组分配合使用。

10. 发明申请

WO1998028306A1 PROCESS FOR THE PREPARATION OF AN ORGANOZINC REAGENT 审中-公开
标题翻译：制备有机原料试剂的方法
公开(公告)号：WO1998028306A1
公开(公告)日：1998-07-02
申请号：PCT/GB1997003443
申请日：1997-12-15
申请人： ZENECA LIMITED , BLACKER, Andrew, John , FIELDEN, Jan, Michael
发明人： ZENECA LIMITED
IPC分类号： C07F03/06
CPC分类号： C07D213/30 , C07B53/00 , C07B2200/07 , C07C29/40 , C07F3/06 , C07C33/22 , C07C33/46 , C07C33/20
摘要： A process for the preparation of an aromatic organozinc compound is provided. The process comprises reacting a zinc chloride, bromide or iodide and an organometallic compoud of another metal comprising an aromatic moiety, producing a reaction product comprising an organozinc compound and a halide salt of the other metal. The reaction product is then contacted with a liquid hydrocarbon, in which the organozinc compound is soluble and the halide salt of the other metal is of low solubility. The halide salt of the other metal is separated from the hydrocarbon, and the organozinc compound can be recovered from the hydrocarbon. Organozinc compounds produced by this process can be employed to generate chiral centres in suitable substrates.
摘要翻译：提供了一种制备芳香族有机锌化合物的方法。该方法包括使氯化锌，溴化物或碘化物与包含芳族部分的另一种金属的有机金属化合物反应，产生包含有机锌化合物和另一种金属的卤化物盐的反应产物。然后使反应产物与液态烃接触，其中有机锌化合物是可溶的，另一种金属的卤化物盐的溶解度低。另一种金属的卤化物盐与烃分离，有机锌化合物可以从烃中回收。通过该方法制备的有机锌化合物可用于在合适的底物中产生手性中心。

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