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1. 发明申请

WO2012158832A2 METHOD FOR PREPARING SEMICONDUCTOR NANOCRYSTALS 审中-公开
标题翻译：制备半导体纳米晶体的方法
公开(公告)号：WO2012158832A2
公开(公告)日：2012-11-22
申请号：PCT/US2012/038198
申请日：2012-05-16
申请人： QD VISION, INC. , BREEN, Craig , LIU, Wenhao
发明人： BREEN, Craig , LIU, Wenhao
CPC分类号： C01B19/04 , B82Y30/00 , B82Y40/00 , C01B19/007 , C01P2002/84 , C01P2004/64 , C01P2006/60 , H01L21/0237 , H01L21/02428 , H01L21/02557 , H01L21/0256 , H01L21/02601 , H01L21/02628
摘要： A method for making semiconductor nanocrystais is disclosed, the method comprising adding a secondary phosphine chalcogenide to a solution including a metal source and a liquid medium at a reaction temperature to form a reaction product comprising a semiconductor comprising a metal and a chalcogen, and quenching the reaction mixture to form quantum dots. Methods for overcoating are also disclosed. Semiconductor nanocrystais are also disclosed.
摘要翻译：公开了一种制备半导体纳米晶体的方法，该方法包括在反应温度下向包含金属源和液体介质的溶液中加入次膦硫属化物，以形成包含金属和硫属元素的半导体的反应产物，并淬灭反应混合物形成量子点。还公开了外敷方法。半导体纳米晶体也被公开。

2. 发明申请

WO2012138410A1 DEVICE INCLUDING QUANTUM DOTS 审中-公开
标题翻译：包括量子的设备
公开(公告)号：WO2012138410A1
公开(公告)日：2012-10-11
申请号：PCT/US2012/023674
申请日：2012-02-02
申请人： QD VISION, INC. , COX, Marshall , BREEN, Craig , ZHOU, Zhaoqun , STECKEL, Jonathan, S.
发明人： COX, Marshall , BREEN, Craig , ZHOU, Zhaoqun , STECKEL, Jonathan, S.
IPC分类号： H01L21/20
CPC分类号： H01L33/04 , H01L21/02439 , H01L21/02491 , H01L21/02502 , H01L21/02521 , H01L21/0256 , H01L21/02601 , H01L33/005 , H01L33/0087 , H01L33/06 , H01L33/28 , H01L33/30 , H01L51/502
摘要： A method for making a device, the method comprising: depositing a layer comprising quantum dots over a first electrode, the quantum dots including ligands attached to the outer surfaces thereof; treating the surface of the deposited layer comprising quantum dots to remove the exposed ligands; and forming a device layer thereover. Also disclosed is a device made in accordance with the disclosed method. Another aspect of the invention relates to a device comprising a first electrode and a second electrode, and a layer comprising quantum dots between the two electrodes, the layer comprising quantum dots deposited from a dispersion that have been treated to remove exposed ligands after formation of the layer in the device. Another aspect of the invention relates to a device comprising a first electrode and a second electrode, a layer comprising a first inorganic semiconductor material disposed between the first and second electrodes, and a plurality of quantum dots disposed between the first and second electrodes, the outer surface of the quantum dots comprising a second inorganic semiconductor material, wherein the composition of the first inorganic semiconductor material and the second inorganic semiconductor material is the same (without regard to any ligands on the outer surface of the quantum dot).
摘要翻译：一种制造器件的方法，所述方法包括：在第一电极上沉积包含量子点的层，所述量子点包括附着于其外表面的配体; 处理包含量子点的沉积层的表面以除去暴露的配体; 并在其上形成器件层。还公开了根据所公开的方法制造的装置。本发明的另一方面涉及一种包括第一电极和第二电极以及在两个电极之间包含量子点的层，该层包括从分散体沉积的量子点，所述分散体在形成之后已被处理以除去暴露的配体设备中的层。本发明的另一方面涉及包括第一电极和第二电极的装置，包括设置在第一和第二电极之间的第一无机半导体材料的层和设置在第一和第二电极之间的多个量子点，外部包括第二无机半导体材料的量子点的表面，其中第一无机半导体材料和第二无机半导体材料的组成相同（不考虑量子点的外表面上的任何配体）。

3. 发明申请

WO2012138409A2 DEVICES INCLUDING QUANTUM DOTS AND METHOD 审中-公开
标题翻译：包括量子和方法的设备
公开(公告)号：WO2012138409A2
公开(公告)日：2012-10-11
申请号：PCT/US2012/023671
申请日：2012-02-02
申请人： QD VISION, INC. , BREEN, Craig
发明人： BREEN, Craig
IPC分类号： H01B13/00 , H01B5/14 , H01B1/02 , F21Y101/02
CPC分类号： H01L33/06 , H01L51/502 , H01L51/5056 , H01L51/5072
摘要： A method for preparing a device, the method comprising: forming a first device layer over a first electrode, the layer comprising a metal oxide formed from a sol-gel composition that does not generate acidic by-products, and forming a second electrode over the first device layer, wherein the method further includes forming a layer comprising quantum dots over the fust electrode before or after formation of the first device layer. Also disclosed is a device comprising a first device layer formed over a first electrode, the first device layer comprising a metal oxide formed by sol-gel processing that does not include acidic by-products, a second electrode over the first device layer, and a layer comprising quantum dots disposed between the first device layer and one of the two electrodes. A device prepared by the method is also disclosed.
摘要翻译：一种制备器件的方法，所述方法包括：在第一电极上形成第一器件层，所述第一器件层包含由不产生酸性副产物的溶胶 - 凝胶组合物形成的金属氧化物，以及在第第一器件层，其中所述方法还包括在形成所述第一器件层之前或之后，在所述固体电极上形成包含量子点的层。还公开了一种包括形成在第一电极上的第一器件层的器件，所述第一器件层包括由不包含酸性副产物的溶胶 - 凝胶加工形成的金属氧化物，第一器件层上的第二电极和层包括设置在第一器件层和两个电极中的一个之间的量子点。还公开了通过该方法制备的器件。

4. 发明申请

WO2010014205A1 COMPOSITIONS, OPTICAL COMPONENT, SYSTEM INCLUDING AN OPTIONAL COMPONENT, DEVICES, AND OTHER PRODUCTS 审中-公开
标题翻译：组成，光学组件，包括可选组件，设备和其他产品的系统
公开(公告)号：WO2010014205A1
公开(公告)日：2010-02-04
申请号：PCT/US2009/004354
申请日：2009-07-28
申请人： QD VISION, INC. , BREEN, Craig , LINTON, John, R.
发明人： BREEN, Craig , LINTON, John, R.
IPC分类号： C30B11/00 , B82B1/00
CPC分类号： G01N33/588 , B82Y15/00 , G01N33/54373 , G02B6/0023 , G02B6/004 , G02B6/005 , H01S3/169
摘要： The present inventions relate to optical components which include quantum confined semiconductor nanoparticles, wherein at least a portion of the nanoparticles include a ligand attached to a surface thereof, the ligand being represented by the formula X-Sp-Z, wherein: X represents: a primary amine group, a secondary amine group, a urea, a thiourea, an imidizole group, an amide group, a carboxylic acid or carboxylate group; a phosphoric acid group, a phosphate group, a phosphite group, a phosphinic acid group, a phosphinate group, a phosphine oxide group, a phosphinite group, a phosphine group, an arsenic acid group, an arsenate group, an arsenous acid group, an arsenite group, an arsinic acid group, an arsine oxide group, or an arsine group; Sp represents a group capable of allowing a transfer of charge or an insulating group; and Z represents a multifunctional group including three or more functional groups capable of communicating a specific property or chemical reactivity to the nanoparticle, wherein at least three of the functional groups are chemically distinct, and wherein Z is not reactive upon exposure to light. As used herein, the term "optical components" includes, but is not limited to, optical components, systems including optical components, lamps including optical components, devices including optical components, films useful in the foregoing, inks useful in making the foregoing, and compositions useful in the foregoing.
摘要翻译：本发明涉及包括量子限制半导体纳米颗粒的光学部件，其中至少一部分纳米颗粒包括与其表面连接的配体，该配体由式X-Sp-Z表示，其中：X表示：a 伯胺基，仲胺基，脲，硫脲，亚氨基咪唑基，酰胺基，羧酸或羧酸酯基; 磷酸基，磷酸酯基，亚磷酸酯基，次膦酸基，次膦酸基，氧化膦基，膦基，膦基，砷酸基，砷酸酯基，亚砷酸基，亚砷酸盐基团，亚砷酸基团，氧化胂基团或胂基团; Sp表示能够允许电荷转移或绝缘组的组; Z表示包括三个或更多个能够与纳米颗粒通过特定性质或化学反应性的官能团的多官能团，其中至少三个官能团在化学上不同，并且其中Z在暴露于光时不具有反应性。如本文所用，术语“光学部件”包括但不限于光学部件，包括光学部件的系统，包括光学部件的灯，包括光学部件的装置，可用于前述的膜，用于制造前述的油墨，以及可用于上述的组合物。

5. 发明申请

WO2009035657A1 FUNCTIONALIZED NANOPARTICLES AND METHOD 审中-公开
标题翻译：功能性纳米颗粒和方法
公开(公告)号：WO2009035657A1
公开(公告)日：2009-03-19
申请号：PCT/US2008/010651
申请日：2008-09-12
申请人： QD VISION, INC. , BREEN, Craig , COX, Marshall , STECKEL, Jonathan, S.
发明人： BREEN, Craig , COX, Marshall , STECKEL, Jonathan, S.
IPC分类号： C07K1/00
CPC分类号： A61K49/0067 , B82Y15/00 , G01N33/54353 , G01N33/588
摘要： A nanoparticle including an inorganic core comprising at least one metal and/or at least one semi-conductor compound comprising at least one metal includes a coating or shell disposed over at least a portion of a surface of the core. The coating can include one or more layers. Each layer of the coating can comprise a metal and/or at least one semiconductor compound. The nanoparticle further includes a ligand attached to a surface of the coating. The ligand is represented by the formula: X-Sp-Z, wherein X represents, e.g., a primary amine group, a secondary amine group, a urea, a thiourea, an imidizole group, an amide group, a phosphonic or arsonic acid group, a phosphinic or arsinic acid group, a phosphate or arsenate group, a phosphine or arsine oxide group; Sp represents a spacer group, such as a group capable of allowing a transfer of charge or an insulating group; and Z represents: (i) a reactive group capable of communicating specific chemical properties to the nanocrystal as well as provide specific chemical reactivity to the surface of the nanocrystal, and/or (ii) a group that is cyclic, halogenated, or polar a-protic. In certain embodiments, at least two chemically distinct ligands are attached to an surface of the coating, wherein the at least two ligands (I and II) are represented by the formula: X-Sp-Z. In ligand (I) X represents a phosphonic, phosphinic, or phosphategroup and in ligand (II) X represents a primary or secondary amine, or an imidizole, or an amide; In both ligands (I) and (II) Sp, which can be the same or different in the two compounds, represents a spacer group, such as a group capable of allowing a transfer of charge or an insulating group; Z, which can be the same or different in the two compounds, is a group chosen from among groups capable of communicating specific chemical properties to the nanoparticle as well as provide specific chemical reactivity to the surface of the nanoparticle. In preferred embodiments, the nanoparticle includes a core comprising a semiconductor material.
摘要翻译：包括包含至少一种金属和/或至少一种包含至少一种金属的半导体化合物的无机芯的纳米颗粒包括设置在芯的表面的至少一部分上的涂层或壳。涂层可以包括一层或多层。涂层的每个层可以包含金属和/或至少一种半导体化合物。纳米颗粒还包括附着在涂层表面上的配体。配体由下式表示：X-Sp-Z，其中X表示例如伯胺基，仲胺基，脲，硫脲，亚氨基咪唑基，酰胺基，膦酸或仲磺酸基，次膦酸或亚砷酸基，磷酸盐或砷酸盐基，膦或砷化胂基; Sp表示间隔基，例如可以允许电荷转移或绝缘组的基团; 并且Z表示：（i）能够与纳米晶体传递特定化学性质的反应性基团，并且提供对纳米晶体的表面的特定的化学反应性，和/或（ii）环状，卤化的或极性的基团 -protic。在某些实施方案中，至少两个化学上不同的配体连接到涂层的表面，其中至少两个配体（I和II）由下式表示：X-Sp-Z。在配体（I）中，X表示膦酸，次膦酸或膦酸酯基团，在配位体（II）中，X表示伯胺或仲胺，或亚氨基咪唑或酰胺; 在两种化合物中可以相同或不同的配体（I）和（II）Sp中，表示间隔基团，例如能够允许电荷转移或绝缘基团的基团; Z可以在两种化合物中相同或不同，是选自能够与纳米颗粒通信特定化学性质的基团以及为纳米颗粒的表面提供具体的化学反应性的基团。在优选实施方案中，纳米颗粒包括包含半导体材料的芯。

6. 发明申请

WO2013078249A1 METHOD OF MAKING QUANTUM DOTS 审中-公开
标题翻译：制作量子点的方法
公开(公告)号：WO2013078249A1
公开(公告)日：2013-05-30
申请号：PCT/US2012/066147
申请日：2012-11-20
申请人： QD VISION INC.
发明人： LIU, Wenhao , BREEN, Craig
IPC分类号： H01L21/20
CPC分类号： C30B7/14 , B22F1/0018 , B22F1/025 , B22F9/24 , B82Y20/00 , B82Y30/00 , B82Y40/00 , C22C1/1026 , C22C20/00 , C30B7/005 , C30B7/08 , C30B19/12 , C30B29/48 , C30B29/68 , H01L21/02557 , H01L21/0256 , H01L21/02601 , H01L21/02628 , H01L33/28 , Y10S977/774 , Y10S977/892 , Y10S977/896 , Y10S977/95
摘要： Quantum dots and methods of making quantum dots are provided.
摘要翻译：提供量子点和制造量子点的方法。

7. 发明申请

WO2013078247A1 METHODS OF COATING SEMICONDUCTOR NANOCRYSTALS, SEMICONDUCTOR NANOCRYSTALS, AND PRODUCTS INCLUDING SAME 审中-公开
标题翻译：涂覆半导体纳米晶体，半导体纳米晶体和包括其的产品的方法
公开(公告)号：WO2013078247A1
公开(公告)日：2013-05-30
申请号：PCT/US2012/066145
申请日：2012-11-20
申请人： QD VISION, INC.
发明人： BREEN, Craig , LIU, Wenhao
IPC分类号： C09K11/54
CPC分类号： H01L29/151 , C09D11/52 , C09K11/595 , C09K11/883 , H01L21/02406 , H01L21/02422 , H01L21/02521 , H01L21/02557 , H01L21/0256 , H01L21/02601 , H01L21/02628 , H01L29/225
摘要： The present invention relates to quantum dots including an overcoating, methods for overcoating quantum dots, materials and products including quantum dots taught herein, and materials and products including quantum dots made by a method taught herein. In accordance with one aspect of the present invention, there is provided a method of forming one or more coatings or layers or shells on quantum dots wherein amine species are not present or are not substantially present during formation of at least the outermost coating or layer or shell on core quantum dots.
摘要翻译：本发明涉及包括外涂层的量子点，量子点的外涂方法，包括本文所述的量子点的材料和产品，以及包括通过本文教导的方法制造的量子点的材料和产品。根据本发明的一个方面，提供了一种在量子点上形成一个或多个涂层或层或壳的方法，其中在至少最外层的涂层或层的形成过程中胺类不存在或基本不存在，或者壳上的核心量子点。

8. 发明申请

WO2013078245A1 METHOD OF MAKING QUANTUM DOTS 审中-公开
标题翻译：制作量子的方法
公开(公告)号：WO2013078245A1
公开(公告)日：2013-05-30
申请号：PCT/US2012/066140
申请日：2012-11-20
申请人： QD VISION, INC.
发明人： LIU, Wenhao , BREEN, Craig
IPC分类号： H01L21/20
CPC分类号： C30B7/14 , B22F1/0018 , B22F9/24 , B82Y30/00 , B82Y40/00 , C30B7/005 , C30B7/08 , C30B19/12 , C30B29/48 , C30B29/68 , H01L21/02521 , H01L21/02557 , H01L21/0256 , H01L21/02601 , H01L21/02628 , H01L21/10
摘要： Quantum dots and methods of making quantum dots are provided.
摘要翻译：提供量子点和制造量子点的方法。

9. 发明申请

WO2012134629A1 QUANTUM DOTS, METHOD, AND DEVICES 审中-公开
标题翻译：量子点，方法和设备
公开(公告)号：WO2012134629A1
公开(公告)日：2012-10-04
申请号：PCT/US2012/023467
申请日：2012-02-01
申请人： QD VISION, INC. , BREEN, Craig , STECKEL, Jonathan, S.
发明人： BREEN, Craig , STECKEL, Jonathan, S.
IPC分类号： C09K11/61 , H01L33/04
CPC分类号： H01L33/04 , C09K11/025 , C09K11/06 , C09K11/08 , C09K2211/14 , Y10T428/2998
摘要： A quantum dot including a fluorine-containing ligand attached to a surface thereof and having a coating comprising a fluoropolymer over at least a portion of the outer surface of the quantum dot, A method for preparing a quantum dot with a coating comprising a fluoropolymer over at least a portion of the outer surface of the quantum dot is also disclosed. The method comprises contacting a quantum dot having a fluorine-containing ligand attached to a surface thereof with a fluoropolymer to coat the fluoropolymer over at least a portion of the outer surface of the quantum dot. A device including the quantum dot taught herein is further disclosed. An emissive material including the quantum dot taught herein is further disclosed.
摘要翻译：一种量子点，其包含附着在其表面上的含氟配体，并且在该量子点的外表面的至少一部分上具有包含含氟聚合物的涂层。一种制备量子点的方法，所述涂层包含含氟聚合物还公开了量子点的外表面的至少一部分。该方法包括使具有附着在其表面上的含氟配体的量子点与含氟聚合物接触，以在该量子点的外表面的至少一部分上涂覆含氟聚合物。进一步公开了包括本文教导的量子点的装置。进一步公开了包括本文教导的量子点的发射材料。

10. 发明申请

WO2011100023A1 SEMICONDUCTOR NANOCRYSTALS AND METHODS OF PREPARATION 审中-公开
标题翻译：半导体纳米晶体及其制备方法
公开(公告)号：WO2011100023A1
公开(公告)日：2011-08-18
申请号：PCT/US2010/059931
申请日：2010-12-10
申请人： QD VISION, INC. , ZHU, Zhengguo , STECKEL, Jonathan, S. , BREEN, Craig , KAMPLAIN, Justin , SONG, Inja , WANG, Chunming
发明人： ZHU, Zhengguo , STECKEL, Jonathan, S. , BREEN, Craig , KAMPLAIN, Justin , SONG, Inja , WANG, Chunming
IPC分类号： C09D1/00
CPC分类号： C30B29/40 , B01J13/02 , B82Y30/00 , B82Y40/00 , C01P2004/64 , C30B7/14 , C30B28/04 , C30B29/48 , C30B29/60 , H01L21/02601 , H01L33/30 , H01L33/305
摘要： A method for preparing semiconductor nanocrystals: reacting cation precursor and anion precursor in a mixture including on or more acids, phenol compounds, and a solvent to produce semiconductor nanocrystals having a predetermined composition by reacting the reaction mixture at a temperature and for a period of time. A method for forming a coating on at Ieast a portion of a population of semiconductor nanocrystals: forming a first mixture including a population of semiconductor nanocrystals, one or more amine compounds, and a first solvent; adding cation precursor and anion precursor to the first mixture, wherein the temperature of the first mixture during addition of the precursors is sufficient for growing a semiconductor material comprising the cation and anion on at Ieast a portion of an outer surface of at Ieast a portion of the population of semiconductor nanocrystals.
摘要翻译：一种制备半导体纳米晶体的方法：使阳离子前体和阴离子前体在包含或多种酸，酚化合物和溶剂的混合物中反应，以通过在一段温度和一段时间内使反应混合物反应来制备具有预定组成的半导体纳米晶体。一种在半导体纳米晶体群体的一部分上形成涂层的方法：形成包含半导体纳米晶体群，一种或多种胺化合物和第一溶剂的第一混合物; 将阳离子前体和阴离子前体加入到第一混合物中，其中在添加前体期间第一混合物的温度足以在含有阳离子和阴离子的外部表面的一部分上生长包含阳离子和阴离子的半导体材料，半导体纳米晶体的人口。

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