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1. 发明申请

WO2012158832A2 METHOD FOR PREPARING SEMICONDUCTOR NANOCRYSTALS 审中-公开
标题翻译：制备半导体纳米晶体的方法
公开(公告)号：WO2012158832A2
公开(公告)日：2012-11-22
申请号：PCT/US2012/038198
申请日：2012-05-16
申请人： QD VISION, INC. , BREEN, Craig , LIU, Wenhao
发明人： BREEN, Craig , LIU, Wenhao
CPC分类号： C01B19/04 , B82Y30/00 , B82Y40/00 , C01B19/007 , C01P2002/84 , C01P2004/64 , C01P2006/60 , H01L21/0237 , H01L21/02428 , H01L21/02557 , H01L21/0256 , H01L21/02601 , H01L21/02628
摘要： A method for making semiconductor nanocrystais is disclosed, the method comprising adding a secondary phosphine chalcogenide to a solution including a metal source and a liquid medium at a reaction temperature to form a reaction product comprising a semiconductor comprising a metal and a chalcogen, and quenching the reaction mixture to form quantum dots. Methods for overcoating are also disclosed. Semiconductor nanocrystais are also disclosed.
摘要翻译：公开了一种制备半导体纳米晶体的方法，该方法包括在反应温度下向包含金属源和液体介质的溶液中加入次膦硫属化物，以形成包含金属和硫属元素的半导体的反应产物，并淬灭反应混合物形成量子点。还公开了外敷方法。半导体纳米晶体也被公开。

2. 发明申请

WO2013078249A1 METHOD OF MAKING QUANTUM DOTS 审中-公开
标题翻译：制作量子点的方法
公开(公告)号：WO2013078249A1
公开(公告)日：2013-05-30
申请号：PCT/US2012/066147
申请日：2012-11-20
申请人： QD VISION INC.
发明人： LIU, Wenhao , BREEN, Craig
IPC分类号： H01L21/20
CPC分类号： C30B7/14 , B22F1/0018 , B22F1/025 , B22F9/24 , B82Y20/00 , B82Y30/00 , B82Y40/00 , C22C1/1026 , C22C20/00 , C30B7/005 , C30B7/08 , C30B19/12 , C30B29/48 , C30B29/68 , H01L21/02557 , H01L21/0256 , H01L21/02601 , H01L21/02628 , H01L33/28 , Y10S977/774 , Y10S977/892 , Y10S977/896 , Y10S977/95
摘要： Quantum dots and methods of making quantum dots are provided.
摘要翻译：提供量子点和制造量子点的方法。

3. 发明申请

WO2013078247A1 METHODS OF COATING SEMICONDUCTOR NANOCRYSTALS, SEMICONDUCTOR NANOCRYSTALS, AND PRODUCTS INCLUDING SAME 审中-公开
标题翻译：涂覆半导体纳米晶体，半导体纳米晶体和包括其的产品的方法
公开(公告)号：WO2013078247A1
公开(公告)日：2013-05-30
申请号：PCT/US2012/066145
申请日：2012-11-20
申请人： QD VISION, INC.
发明人： BREEN, Craig , LIU, Wenhao
IPC分类号： C09K11/54
CPC分类号： H01L29/151 , C09D11/52 , C09K11/595 , C09K11/883 , H01L21/02406 , H01L21/02422 , H01L21/02521 , H01L21/02557 , H01L21/0256 , H01L21/02601 , H01L21/02628 , H01L29/225
摘要： The present invention relates to quantum dots including an overcoating, methods for overcoating quantum dots, materials and products including quantum dots taught herein, and materials and products including quantum dots made by a method taught herein. In accordance with one aspect of the present invention, there is provided a method of forming one or more coatings or layers or shells on quantum dots wherein amine species are not present or are not substantially present during formation of at least the outermost coating or layer or shell on core quantum dots.
摘要翻译：本发明涉及包括外涂层的量子点，量子点的外涂方法，包括本文所述的量子点的材料和产品，以及包括通过本文教导的方法制造的量子点的材料和产品。根据本发明的一个方面，提供了一种在量子点上形成一个或多个涂层或层或壳的方法，其中在至少最外层的涂层或层的形成过程中胺类不存在或基本不存在，或者壳上的核心量子点。

4. 发明申请

WO2013078245A1 METHOD OF MAKING QUANTUM DOTS 审中-公开
标题翻译：制作量子的方法
公开(公告)号：WO2013078245A1
公开(公告)日：2013-05-30
申请号：PCT/US2012/066140
申请日：2012-11-20
申请人： QD VISION, INC.
发明人： LIU, Wenhao , BREEN, Craig
IPC分类号： H01L21/20
CPC分类号： C30B7/14 , B22F1/0018 , B22F9/24 , B82Y30/00 , B82Y40/00 , C30B7/005 , C30B7/08 , C30B19/12 , C30B29/48 , C30B29/68 , H01L21/02521 , H01L21/02557 , H01L21/0256 , H01L21/02601 , H01L21/02628 , H01L21/10
摘要： Quantum dots and methods of making quantum dots are provided.
摘要翻译：提供量子点和制造量子点的方法。

5. 发明申请

WO2013162646A1 COATED SEMICONDUCTOR NANOCRYSTALS AND PRODUCTS INCLUDING SAME 审中-公开
标题翻译：包覆的半导体纳米晶体和包括它们的产品
公开(公告)号：WO2013162646A1
公开(公告)日：2013-10-31
申请号：PCT/US2012/066158
申请日：2012-11-20
申请人： QD VISION, INC.
发明人： BREEN, Craig , LIU, Wenhao
IPC分类号： H01L31/00
CPC分类号： H01L31/035218 , H01L31/055 , Y02E10/52
摘要： A coated quantum dot is provided wherein the quantum dot is characterized by having a solid state photoluminescence external quantum efficiency at a temperature of 90°C or above that is at least 95% of the solid state photoluminescence external quantum efficiency of the semiconductor nanocrystal at 25°C. Products including quantum dots described herein are also disclosed.
摘要翻译：提供了一种涂覆的量子点，其中量子点的特征在于在90℃或更高的温度下具有固态光致发光外部量子效率，其为25nm时半导体纳米晶体的固态光致发光外部量子效率的至少95％ C。还公开了包括本文所述的量子点的产品。

6. 发明申请

WO2013115898A2 SEMICONDUCTOR NANOCRYSTALS, METHODS FOR MAKING SAME, COMPOSITIONS, AND PRODUCTS 审中-公开
标题翻译：半导体纳米晶体，其制备方法，组合物和产品
公开(公告)号：WO2013115898A2
公开(公告)日：2013-08-08
申请号：PCT/US2012/066154
申请日：2012-11-20
申请人： QD VISION, INC.
发明人： LIU, Wenhao , BREEN, Craig , COE-SULLIVAN, Seth
IPC分类号： H01L33/16
CPC分类号： H01L33/06 , B82Y20/00 , C09D11/52 , C09K11/02 , C09K11/565 , C09K11/883 , H01L33/0029 , H01L33/28 , H01L33/502 , Y10S977/774
摘要： A semiconductor nanocrystal characterized by having a solid state photoluminescence external quantum efficiency at a temperature of 90°C or above that is at least 95% of the solid state photoluminescence external quantum efficiency of the semiconductor nanociystal at 25°C is disclosed. A semiconductor nanociystal having a multiple LO phonon assisted charge thermal escape activation energy of at least 0.5eV is also disclosed. A semiconductor nanociystal capable of emitting light with a maximum peak emission at a wavelength in a range from 590 nm to 650 nm characterized by an absorption spectrum, wherein the absorption ratio of OD at 325 nm to OD at 450 nm is greater than 5.5. A semiconductor nanociystal capable of emitting light with a maximum peak emission at a wavelength in a range from 545 nm to 590 nm characterized by an absorption spectrum, wherein the absorption ratio of OD at 325 nm to OD at 450 nm is greater than 7. A semiconductor nanocrystal capable of emitting light with a maximum peak emission at a wavelength in a range from 495 nm to 545 nm characterized by an absorption spectrum, wherein the absorption ratio of OD at 325 nm to OD at 450 nm is greater than 10. A composition comprising a plurality of semiconductor nanocrystals wherein the solid state photoluminescence efficiency of the composition at a temperature of 90°C or above is at least 95% of the solid state photoluminescence efficiency of the composition 25°C is further disclosed. A method for preparing semiconductor nanocrystals comprises introducing one or more first shell chalcogenide precursors and one or more first shell metal precursors to a reaction mixture including semiconductor nanociystal cores, wherein the first shell chalcogenide precursors are added in an amount greater than the first shell metal precursors by a factor of at least about 2 molar equivalents and reacting the first shell precursors at a first reaction temperature of at least 300°C to form a first shell on the semiconductor nanocrystal cores. Populations, compositions, components and other products including semiconductor nanocrystals of the invention are disclosed. Populations, compositions, components and other products including semiconductor nanocrystals made in accordance with any method of the invention is also disclosed.
摘要翻译：公开了一种半导体纳米晶体，其特征在于在90℃以上的温度下具有固态光致发光外部量子效率，其为25℃时半导体纳米晶体的固态光致发光外部量子效率的至少95％。还公开了具有至少0.5eV的多个LO声子辅助电荷热逸散活化能的半导体纳米晶体。能够以590nm至650nm范围内的波长发射具有最大峰值发射的光的半导体纳米晶体，其特征在于吸收光谱，其中325nm处的OD与450nm处的OD的吸收比大于5.5。能够以545nm〜590nm范围内的波长发射具有最大峰值发射的光的半导体纳米晶体，其特征在于吸收光谱，其中325nm处的OD与450nm处的OD的吸收比大于7. 能够以495nm至545nm范围内的波长发射具有最大峰值发射的光的半导体纳米晶体，其特征在于吸收光谱，其中325nm处的OD与450nm处的OD的吸收比大于10。包括多个半导体纳米晶体，其中组合物在90℃或更高的温度下的固态光致发光效率至少为组合物25℃的固态光致发光效率的95％。制备半导体纳米晶体的方法包括将一种或多种第一壳硫属元素前体和一种或多种第一壳金属前体引入包含半导体纳米晶核的反应混合物中，其中第一壳硫属元素前体的加入量大于第一壳金属前体至少约2摩尔当量的因子，并且在至少300℃的第一反应温度下使第一壳前体反应，以在半导体纳米晶核上形成第一壳。公开了包括本发明的半导体纳米晶体的种群，组合物，组分和其它产品。还公开了根据本发明的任何方法制备的包含半导体纳米晶体的种群，组合物，组分和其它产品。

7. 发明申请

WO2013078242A1 METHODS FOR COATING SEMICONDUCTOR NANOCRYSTALS 审中-公开
标题翻译：涂覆半导体纳米晶的方法
公开(公告)号：WO2013078242A1
公开(公告)日：2013-05-30
申请号：PCT/US2012/066137
申请日：2012-11-20
申请人： QD VISION, INC.
发明人： BREEN, Craig , LIU, Wenhao
IPC分类号： C09K11/02
CPC分类号： H01L29/151 , B82Y10/00 , B82Y20/00 , B82Y40/00 , C09K11/02 , C09K11/883 , H01L21/02409 , H01L21/02521 , H01L21/02557 , H01L21/0256 , H01L21/02601 , H01L21/02628 , H01L29/0665 , H01L29/127 , H01L29/20 , H01L29/225 , Y10S977/774 , Y10S977/892 , Y10S977/95
摘要： The present invention relates to quantum dots including an overcoating, methods for overcoating quantum dots, materials and products including quantum dots taught herein, and materials and products including quantum dots made by a method taught herein. Embodiments of the present invention are directed to methods of providing one or more coatings or layers or shells on quantum dots. According to one aspect, a quantum dot to be provided with a coating or layer or shell may be referred to as a "core" particle or a "core" quantum dot. According to an additional aspect, the core particle is subjected to a high temperature process that forms a coating or layer or shell on the core particle to produce a core-shell quantum dot. According to one aspect, free, unbound phosphonic acid or metal phosphonate species are not present or are not substantially present in the core quantum dots prior to providing a coating or layer or shell on the core quantum dots.
摘要翻译：本发明涉及包括外涂层的量子点，量涂点覆盖的方法，包括本文所述的量子点的材料和产品，以及包括通过本文教导的方法制造的量子点的材料和产品。本发明的实施例涉及在量子点上提供一个或多个涂层或层或壳的方法。根据一个方面，提供有涂层或层或壳的量子点可以被称为“芯”颗粒或“芯”量子点。根据另一方面，核心颗粒经受在核心颗粒上形成涂层或层或壳的高温过程以产生核 - 壳量子点。根据一个方面，在核心量子点上提供涂层或层或壳之前，游离的未结合的膦酸或金属膦酸盐物质不存在或基本上不存在于核心量子点中。

8. 发明申请

WO2012027203A1 HIGHLY LUMINESCENT SEMICONDUCTOR NANOCRYSTALS 审中-公开
标题翻译：高亮度半导体纳米晶体
公开(公告)号：WO2012027203A1
公开(公告)日：2012-03-01
申请号：PCT/US2011/048299
申请日：2011-08-18
申请人： MASSACHUSETTS INSTITUTE OF TECHNOLOGY , GREYTAK, Andrew, B. , LIU, Wenhao , ALLEN, Peter, M. , BAWENDI, Moungi, G. , NOCERA, Daniel, G.
发明人： GREYTAK, Andrew, B. , LIU, Wenhao , ALLEN, Peter, M. , BAWENDI, Moungi, G. , NOCERA, Daniel, G.
IPC分类号： C09K11/58 , C09K11/88
CPC分类号： C09K11/584 , C09K11/883
摘要： A semiconductor nanocrystal can have a photoluminescent quantum yield of at least 90%, at least 95%, or at least 98%. The nanocrystal can be made by sequentially contacting a nanocrystal core with an M-containing compound and an X donor, where at least one of the M-containing compound and the X donor is substoichiometric with respect to forming a monolayer on the nanocrystal core.
摘要翻译：半导体纳米晶体可以具有至少90％，至少95％或至少98％的光致发光量子产率。纳米晶体可以通过使纳米晶核与含M化合物和X供体顺序接触来制备，其中至少一个含M化合物和X供体相对于在纳米晶核上形成单层是亚化学计量的。

9. 发明申请

WO2011119654A1 LIGANDS FOR SEMICONDUCTOR NANOCRYSTALS 审中-公开
标题翻译：半导体纳米晶体的配体
公开(公告)号：WO2011119654A1
公开(公告)日：2011-09-29
申请号：PCT/US2011/029492
申请日：2011-03-23
申请人： MASSACHUSETTS INSTITUTE OF TECHNOLOGY , HAN, Hee-sun , LIU, Wenhao , BAWENDI, Moungi, G.
发明人： HAN, Hee-sun , LIU, Wenhao , BAWENDI, Moungi, G.
IPC分类号： G01N33/58 , A61K49/00 , C09K11/00 , B82Y15/00 , B82Y5/00
CPC分类号： G01N33/588 , A61K49/0041 , A61K49/0054 , A61K49/0067 , B82Y15/00
摘要： In this invention, polyimidazole ligands (PILs) incorporating pendant imidazole moieties for nanocrystal binding and either sulfonatebetaine, carboxybetaine, or phosphocholinebetaine moieties for water-solubilization have been developed. Greatly enhanced stability of nanocrystals (both over time and in wide pH range) was achieved by incorporating multi-dentate imidazole moieties which provide strong coordination of the ligand to the nanocrystal surface and prevent aggregation of nanocrystals. Synthesis of betaine PILs was developed by modifying the synthesis of recently developed PEG containing poly imidazole ligands (PEG PILs). These nanocrystals are compact, water soluble, and biocompatible.
摘要翻译：在本发明中，已经开发了结合用于纳米晶体结合的侧基咪唑部分和磺酸甜菜碱，羧基甜菜碱或磷酸胆碱甜菜碱部分用于水溶性的聚咪唑配体（PIL）。纳米晶体的稳定性（随着时间的推移和宽pH范围的增加）都是通过引入多齿咪唑部分实现的，这些部分提供配体与纳米晶体表面的强配位，并防止纳米晶体的聚集。通过改变最近开发的含PEG多聚咪唑配体（PEG PIL）的合成开发了甜菜碱PIL的合成。这些纳米晶体是紧凑的，水溶性的和生物相容的。

10. 发明申请

WO2011022338A1 COPOLYMER-ASSOCIATED NANOMATERIAL 审中-公开
标题翻译：共聚物相关纳米材料
公开(公告)号：WO2011022338A1
公开(公告)日：2011-02-24
申请号：PCT/US2010/045640
申请日：2010-08-16
申请人： MASSACHUSETTS INSTITUTE OF TECHNOLOGY , LIU, Wenhao , ALLEN, Peter, Matthew , INSIN, Numpon , BAWENDI, Moungi, G.
发明人： LIU, Wenhao , ALLEN, Peter, Matthew , INSIN, Numpon , BAWENDI, Moungi, G.
IPC分类号： C08G65/332 , C08G65/333 , C08L71/02 , C30B7/00
CPC分类号： B82Y40/00 , B82Y30/00 , C08F220/54 , C08G65/3322 , C08G65/33306 , C08L71/02 , C08L2205/05 , C08L2666/04
摘要： A nanomaterial can include an outer layer including a ligand. The ligand can include a first monomer unit including a first moiety having affinity for a surface of the nanocrystal, a second monomer unit including a second moiety having a high water solubility, and a third monomer unit including a third moiety having a selectively reactive functional group or a selectively binding functional group. The ligand can be a random copolymer.
摘要翻译：纳米材料可以包括包含配体的外层。配体可以包括第一单体单元，其包括对纳米晶体的表面具有亲和性的第一部分，第二单体单元包括具有高水溶性的第二部分，第三单体单元包括具有选择性反应性官能团的第三部分或选择性结合的官能团。配体可以是无规共聚物。

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