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1. 发明申请

WO2004069880A1 CATALYST SYSTEM FOR PREPARING STYRENE POLYMER AND METHOD FOR PREPARING OF STYRENE POLYMER USING THE SAME 审中-公开
标题翻译：用于制备苯乙烯聚合物的催化剂体系及其制备苯乙烯聚合物的方法
公开(公告)号：WO2004069880A1
公开(公告)日：2004-08-19
申请号：PCT/KR2004/000213
申请日：2004-02-05
申请人： LG CHEM, LTD. , HONG, Moo-Ho , WOO, Boo-Gon , SON, Young-Suk
发明人： HONG, Moo-Ho , WOO, Boo-Gon , SON, Young-Suk
IPC分类号： C08F4/60
CPC分类号： C08F12/08 , C08F4/65908 , C08F4/65912 , C08F4/65916 , Y10S526/904
摘要： The present invention relates to a catalyst system for preparing styrene polymer and a method of preparing styrene polymer using the same, more particularly to a catalyst system for preparing styrene polymer capable of preventing coagulation of polymer to the reactor by preventing gelation, offering high conversion ratio, simplifying polymer production and enabling product size control, and a method of preparing styrene polymer using the same.
摘要翻译：本发明涉及一种制备苯乙烯聚合物的催化剂体系，以及使用其制备苯乙烯聚合物的方法，更具体地说，涉及一种制备苯乙烯聚合物的催化剂体系，该催化剂体系能够防止聚合物通过防止凝胶化而凝聚聚合反应器，提供高转化率，简化聚合物生产并实现产品尺寸控制，以及使用其制备苯乙烯聚合物的方法。

2. 发明申请

WO2004041906A1 PREPARATION METHOD OF HIGH MOLECULAR WEIGHT POLYCARBONATE RESIN 审中-公开
标题翻译：高分子量聚碳酸酯树脂的制备方法
公开(公告)号：WO2004041906A1
公开(公告)日：2004-05-21
申请号：PCT/KR2003/002070
申请日：2003-10-08
申请人： LG CHEM, LTD. , KIM, Jong-Hun , WOO, Boo-Gon , PARK, Eun-Duck , HONG, Mi-Jeung
发明人： KIM, Jong-Hun , WOO, Boo-Gon , PARK, Eun-Duck , HONG, Mi-Jeung
IPC分类号： C08G64/20
CPC分类号： C08G64/20 , C08G64/04 , C08G64/307 , C08G64/40
摘要： The present invention relates to a method for the preparation of a high molecular weight polycarbonate resin, and more particularly to a method for preparing a high molecular weight polycarbonate resin using a solid state polymerization method after the preparation of a crystalline polycarbonate or conducting the preparation of the crystalline polycarbonate and the solid state polymerization thereof simultaneously. According to the method for the preparation of a high molecular weight polycarbonate resin of the invention, it is possible to produce a high molecular weight polycarbonate resin having a narrow molecular weight distribution and uniform properties and that is applicable to injection and extrusion in large quantities with a low cost within a short time.
摘要翻译：制备高分子量聚碳酸酯树脂的方法技术领域本发明涉及一种制备高分子量聚碳酸酯树脂的方法，并且更具体地涉及在制备高分子量聚碳酸酯树脂之后使用固态聚合方法制备高分子量聚碳酸酯树脂的方法，结晶聚碳酸酯或同时进行结晶聚碳酸酯的制备和其固态聚合。根据本发明的高分子量聚碳酸酯树脂的制备方法，可以制备具有窄分子量分布和均匀性能的高分子量聚碳酸酯树脂，并且该聚碳酸酯树脂可适用于大量注入和挤出短时间内成本低。

3. 发明申请

WO2004007064A1 CATALYTIC OXIDATION REACTOR WITH ENHANCED HEAT EXCHANGING SYSTEM 审中-公开
标题翻译：具有增强热交换系统的催化氧化反应器
公开(公告)号：WO2004007064A1
公开(公告)日：2004-01-22
申请号：PCT/KR2002/002074
申请日：2002-11-08
申请人： LG CHEM, LTD. , HA, Kyoung-Su , KIM, Geon-Yong , KANG, Seong-Pil , WOO, Boo-Gon
发明人： HA, Kyoung-Su , KIM, Geon-Yong , KANG, Seong-Pil , WOO, Boo-Gon
IPC分类号： B01J8/06
CPC分类号： B01J19/0013 , B01J8/067 , B01J2208/00212 , B01J2208/00221 , B01J2208/00548 , B01J2219/00006 , B01J2219/0004
摘要： A heat exchange-type reactor includes a reaction chamber (1) having mounted therein a plurality of contact tubes (5) filled with a catalyst material; at least one shield plate (11) mounted within the reaction chamber to partition an inner space of the reaction chamber into at least two separate spaces (1d, 1e); a plurality of conduits (13, 15, 17, 19) having entrance (15a, 17a) and exit (13a, 17a) openings through which a heat transfer medium respectively enters and exits, and being mounted to an outer circumference of the reaction chamber (1) corresponding to the partitioned spaces (1d, 1e); and a heat exchange unit connected to the conduits (13, 15, 17, 19) to perform heat exchange of the heat transfer medium, in which the heat exchange unit includes a single heat exchanger that performs the exchange of heat of the heat transfer medium in accordance with the partitioned spaces.
摘要翻译：热交换型反应器包括：反应室（1），其安装有多个填充有催化剂材料的接触管（5）; 至少一个屏蔽板（11），其安装在所述反应室内以将所述反应室的内部空间分隔成至少两个分开的空间（1d，1e）; 具有入口（15a，17a）和出口（13a，17a）开口的多个管道（13,15,17,19），传热介质通过该开口分别进入和离开并安装到反应室的外周（1）对应于分隔空间（1d，1e）; 以及连接到导管（13,15,17,19）的热交换单元，以进行传热介质的热交换，其中，热交换单元包括单个热交换器，该热交换器执行传热介质的热交换按照分区空间。

4. 发明申请

WO2003066569A1 CONTINUOUS METHOD FOR PREPARING AROMATIC CARBONATE USING A HETEROGENEOUS CATALYST AND A REACTION APPARATUS FOR THE SAME 审中-公开
标题翻译：使用异构催化剂制备芳族碳酸酯的连续方法及其相应的反应装置
公开(公告)号：WO2003066569A1
公开(公告)日：2003-08-14
申请号：PCT/KR2003/000237
申请日：2003-02-03
申请人： LG CHEM, LTD. , WOO, Boo-Gon , KWAK, Ja-Hun , HONG, Moo-Ho , HONG, Mi-Jeung
发明人： WOO, Boo-Gon , KWAK, Ja-Hun , HONG, Moo-Ho , HONG, Mi-Jeung
IPC分类号： C07C68/06
CPC分类号： C07C68/06 , C07C68/08 , C07C69/96
摘要： The present invention relates to a continuous method for the preparation of an aromatic carbonate by reacting a dialkyl carbonate and an aromatic hydroxy compound in the presence of a heterogeneous catalyst, and a reaction apparatus for the same. The continuous method comprises the step of reacting dialkyl carbonate and an aromatic hydroxy compound in the presence of the heterogeneous catalyst in a loop-type, catalyst-containing reaction apparatus, wherein a reactor equipped with a filter in which the catalyst is contained is connected with a heat exchanger portion for providing necessary heat during the reaction, reaction solution is circulated between the catalyst-containing portion and heat exchanger via a circulation pump, and by-products can be eliminated via a distillation column connected with the reactor.
摘要翻译：本发明涉及在多相催化剂存在下使碳酸二烷基酯和芳族羟基化合物反应制备芳族碳酸酯的连续方法及其用途。连续方法包括在非均相催化剂存在下，在环状含催化剂的反应装置中使碳酸二烷基酯和芳族羟基化合物反应的步骤，其中装有其中含有催化剂的过滤器的反应器与用于在反应期间提供必要热量的热交换器部分，反应溶液通过循环泵在含催化剂的部分和热交换器之间循环，副产物可以通过与反应器连接的蒸馏塔除去。

5. 发明申请

WO2006135189A1 TEMPERATURE MEASURING DEVICE 审中-公开
标题翻译：温度测量装置
公开(公告)号：WO2006135189A1
公开(公告)日：2006-12-21
申请号：PCT/KR2006/002261
申请日：2006-06-14
申请人： LG CHEM, LTD.
发明人： HA, Kyoung-Su , KO, Jun-Seok , WOO, Boo-Gon , KANG, Seong-Pil , CHOI, Seok-Hwan , LEE, Sang-Youn , KIM, Young-Bae
IPC分类号： G01K1/14
CPC分类号： G01K3/14 , G01K1/14 , G01K7/02
摘要： Disclosed is a temperature measuring device. The temperature measuring device includes: a thermo-well tube; and a cable or wire type temperature measuring means which is installed in a thermo-well tube, wherein temperature measuring means has temperature detecting sensors disposed at an intermediate portion thereof, and the temperature detecting sensors can be moved axially in the thermo-well tube by applying tension to both ends of the cable or wire type temperature measuring means. The present invention also provides a reaction tube in which the temperature measuring device is disposed axially, and a reactor including at least one temperature measuring device or reaction tube as described above.
摘要翻译：公开了一种温度测量装置。所述温度测量装置包括：热井管; 以及安装在热井管中的电缆或线型温度测量装置，其中温度测量装置具有设置在其中间部分的温度检测传感器，并且温度检测传感器可以在热井管中轴向移动，对电缆或电线式温度测量装置的两端施加张力。本发明还提供一种反应管，其中温度测量装置轴向设置，反应器包括如上所述的至少一个温度测量装置或反应管。

6. 发明申请

WO2005111187A1 FACILITY PARTS CLEANING SOLUTION FOR PROCESSING OF (METH)ACRYLIC ACID AND/OR (METH)ACRYLIC ESTERS AND CLEANING METHOD USING SAID CLEANING SOLUTION 审中-公开
标题翻译：用于加工（甲基）丙烯酸和/或（甲基）丙烯酸酯的清洁溶液的清洁溶液和使用清洁溶液的清洁方法
公开(公告)号：WO2005111187A1
公开(公告)日：2005-11-24
申请号：PCT/KR2005/001437
申请日：2005-05-17
申请人： LG CHEM, LTD. , CHOI, Seok-Hwan , KANG, Seong-Pil , HA, Kyoung-Su , KIM, Geon-Yong , WOO, Boo-Gon
发明人： CHOI, Seok-Hwan , KANG, Seong-Pil , HA, Kyoung-Su , KIM, Geon-Yong , WOO, Boo-Gon
IPC分类号： C11D7/06
CPC分类号： C11D7/06 , C11D7/32 , C11D7/3245 , C11D7/3263 , C11D11/0041 , F28G9/00
摘要： The present invention relates to a facility parts cleaning solution for the processing of (meth)acrylic acid and/or (meth)acrylic esters and a cleaning method using the cleaning solution. An aqueous cleaning composition comprising 5 to 50 wt% of at least one alkali metal hydroxide selected from the group consisting of sodium hydroxide and potassium hydroxide, 0.01 to 1 wt% of a water-soluble amino acid, 0.001 to 0.05 wt% of N.N'-methylene bisacrylamide, and 0.001 to 0.05 wt% of azobisisobutyronitrile is used to clean facility parts for manufacturing (meth)acrylic acid and/or (meth)acrylic esters in order to easily remove polymers and deposits.
摘要翻译：本发明涉及用于处理（甲基）丙烯酸和/或（甲基）丙烯酸酯的设备部件清洗液和使用该清洗溶液的清洗方法。含有5〜50重量％的选自氢氧化钠和氢氧化钾的至少一种碱金属氢氧化物，0.01〜1重量％的水溶性氨基酸，0.001〜0.05重量％的N， N'-亚甲基双丙烯酰胺和0.001〜0.05重量％的偶氮二异丁腈用于清洗用于制造（甲基）丙烯酸和/或（甲基）丙烯酸酯的设备部件，以便容易地除去聚合物和沉积物。

7. 发明申请

WO2005080310A1 METHOD FOR PRODUCING (METH)ACRYLIC ACID 审中-公开
标题翻译：生产（甲基）丙烯酸的方法
公开(公告)号：WO2005080310A1
公开(公告)日：2005-09-01
申请号：PCT/KR2005/000427
申请日：2005-02-18
申请人： LG CHEM, LTD.
发明人： KANG, Seong-Pil , CHOI, Seok-Hwan , HA, Kyoung-Su , KIM, Geon-Yong , WOO, Boo-Gon , LEE, Sang-Youn , KIM, Young-Bae , KANG, Koo-Hyun
IPC分类号： C07C51/43
CPC分类号： C07C51/48 , C07C57/04
摘要： The present invention relates to a method for producing (meth)acrylic acid comprising a process of recovering (meth)acrylic acid as an aqueous (meth)acrylic acid from a (meth)acrylic acid-containing gas mixture produced by the catalytic gas phase oxidation of at least one reactant selected from the group consisting of propane, propylene, isobutylene and (meth)acrolein, and a system usable for the method. The recovery process comprises the steps of: (1) feeding the (meth)acrylic acid-containing gas mixture into a quenching tower and condensing it in the quenching tower so as to recover an aqueous (meth)acrylic acid solution from the bottom of the quenching tower, in which some of the recovered aqueous solution of (meth)acrylic acid is recycled to the top part of the quenching tower so as to condense the (meth)acrylic acid-containing gas mixture; (2) passing the uncondensed part of the (meth)acrylic acid-containing gas mixture from the quenching tower through the top of the quenching tower to an absorption column; (3) absorbing (meth)acrylic acid contained in the uncondensed part of the (meth)acrylic acid-containing gas mixture in the absorption column with a absorption solvent; (4) feeding the (meth)acrylic acid solution resulting from the absorption in the step (3) to a desorption column; and (5) separating the solvent used in the step (3) from the (meth)acrylic acid solution in the desorption column, so that the substance from which the solvent has been removed in the desorption column is fed to the quenching tower, and the separated solvent is recycled to the absorption column. The inventive method is an efficient and economic method which allows a reduction in energy consumption in subsequent purification processed by maximizing the concentration of an aqueous solution of (meth)acrylic solution recovered at the bottom of the quenching tower and minimizing the concentration of (meth)acrylic acid lost from the vent gas of the absorption column.
摘要翻译：本发明涉及一种生产（甲基）丙烯酸的方法，包括从由（甲基）丙烯酸的气体混合物通过催化气相氧化制备的（甲基）丙烯酸水溶液回收（甲基）丙烯酸的方法的至少一种选自丙烷，丙烯，异丁烯和（甲基）丙烯醛的反应物，以及可用于该方法的系统。回收方法包括以下步骤：（1）将含（甲基）丙烯酸的气体混合物进料到淬火塔中，并将其冷凝在淬火塔中，以从底部回收（甲基）丙烯酸水溶液淬火塔，其中一些回收的（甲基）丙烯酸水溶液被再循环到淬火塔的顶部，以冷凝（甲基）丙烯酸的气体混合物; （2）将来自淬火塔的（甲基）丙烯酸混合气体的未冷凝部分通过淬火塔的顶部通入吸收塔; （3）用吸收溶剂吸收吸收塔中含（甲基）丙烯酸的气体混合物的未缩合部分中所含的（甲基）丙烯酸; （4）在步骤（3）中将由吸收产生的（甲基）丙烯酸溶液进料到解吸塔; 和（5）将步骤（3）中使用的溶剂与解吸塔中的（甲基）丙烯酸溶液分离，使得在解吸塔中除去溶剂的物质被供给至淬火塔，将分离的溶剂再循环至吸收塔。本发明的方法是一种有效和经济的方法，其允许通过使在淬火塔底部回收的（甲基）丙烯酸溶液的水溶液的浓度最大化并使（甲基）丙烯酸从吸收塔的排气中流失。

8. 发明申请

WO2003100206A1 METHOD FOR PREPARING HIGH MOLECULAR WEIGHT POLYCARBONATE 审中-公开
标题翻译：制备高分子量聚碳酸酯的方法
公开(公告)号：WO2003100206A1
公开(公告)日：2003-12-04
申请号：PCT/KR2003/001048
申请日：2003-05-28
申请人： LG CHEM, LTD. , KIM, Jong-Hun , WOO, Boo-Gon , PARK, Eun-Duck , HONG, Mi-Jeung
发明人： KIM, Jong-Hun , WOO, Boo-Gon , PARK, Eun-Duck , HONG, Mi-Jeung
IPC分类号： E21B17/042
CPC分类号： C08G64/307 , Y10T428/31504 , Y10T428/31507
摘要： The present invention relates to a process for preparing high molecular weight polycarbonate resin, particularly to a process for preparing high molecular weight polycarbonate resin, which conducts condensation polymerization of low molecular weight amorphous polycarbonate prepolymer prepared by transesterification of dialkyl(aryl)carbonate and aromatic hydroxy compound and solid state polymerization within short time to increase molecular weight. The present invention introduces condensation polymerization to lower mole fractions of arylcarbonate existing in unreacted diarylcarboante, end groups of reaction by products of polymerization degree less than 3, and polycarbonate prepolymer obtained by transesterification, and thus can maximize molecular weight increase of polycarbonate after solid state polymerization and remarkably reduce time required for preparing polycarbonate of the same molecular weight. In addition, since the present invention does not use toxic substance phosgene, it has no danger and it can prevent deterioration, and it can prepare high molecular weigh polycarbonate that can be used for injection and extrusion.
摘要翻译：本发明涉及一种制备高分子量聚碳酸酯树脂的方法，特别涉及一种制备高分子量聚碳酸酯树脂的方法，该方法进行低分子量无定形聚碳酸酯预聚物的缩聚，其通过二烷基（芳基）碳酸酯和芳族羟基化合物和固态聚合在短时间内增加分子量。本发明将存在于未反应的二芳基羧酸酯中的芳基碳酸酯的摩尔比低，聚合度小于3的产物的反应端基和通过酯交换反应得到的聚碳酸酯预聚物进行缩聚，从而可以使固态聚合后的聚碳酸酯的分子量增加最大化并且显着地减少了制备相同分子量的聚碳酸酯所需的时间。此外，由于本发明不使用有毒物质光气，因此没有危险，可以防止劣化，并且可以制备可用于注射和挤出的高分子量聚碳酸酯。

9. 发明申请

WO2007007979A1 METHOD OF PRODUCING UNSATURATED ACID IN FIXED-BED CATALYTIC PARTIAL OXIDATION REACTOR WITH HIGH EFFICIENCY 审中-公开
标题翻译：固定床催化部分氧化反应器高效生产不饱和酸的方法
公开(公告)号：WO2007007979A1
公开(公告)日：2007-01-18
申请号：PCT/KR2006/002651
申请日：2006-07-07
申请人： LG CHEM, LTD.
发明人： HA, Kyoung-Su , WOO, Boo-Gon , KO, Jun-Seok , KANG, Seong-Pil , CHOI, Seok-Hwan , KIM, Young-Bae
IPC分类号： C07C45/27
CPC分类号： C07C45/34 , B01J8/0453 , B01J8/0457 , B01J8/067 , B01J2208/00212 , B01J2208/0053 , B01J2208/025 , B01J2219/0004 , C07C45/35 , C07C45/36 , C07C45/37 , C07C51/215 , C07C51/252 , C07C47/21 , C07C47/22 , C07C57/04
摘要： Disclosed is a process for producing unsaturated aldehydes and/or unsaturated acids from olefins or alkanes in a fixed bed shell-and-tube heat exchanger-type reactor by catalytic vapor phase oxidation. A heat exchanger-type reactor for use in such a process is also disclosed. In the process, at least one of the first-step reaction zone and the second-step reaction zone is divided into two or more shell spaces by at least one partition; each of the divided shell spaces is independently heat-controlled; a heat transfer medium in the first shell space of the first-step reaction zone or the first shell space of the second-step reaction zone has a temperature ranging from the lowest active temperature of a catalyst layer packed in a reaction tube corresponding to the first shell space of the first-step reaction zone or the first shell space of the second-step reaction zone to [the lowest active temperature + 20 °C], when referring to the two or more shell spaces corresponding to the first-step reaction zone sequentially as the first shell space of the first-step reaction zone, the second shell space of the first-step reaction zone, ..., the n th shell space of the first-step reaction zone, and the two or more shell spaces corresponding to the second-step reaction zone sequentially as the first shell space of the second-step reaction zone, the second shell space of the second-step reaction zone, ... , the n th shell space of the second-step reaction zone; and the first shell space of the first-step reaction zone or the first shell space of the second-step reaction zone is controlled in such a manner that the first shell space provides a reactant conversion contribution per length as defined in Equation 1 or 2 of 1.2∼2.5.
摘要翻译：公开了一种通过催化气相氧化在固定床管壳式热交换器型反应器中由烯烃或烷烃生产不饱和醛和/或不饱和酸的方法。还公开了一种用于这种方法的热交换器型反应器。在该过程中，至少一个第一步骤反应区和第二步反应区被至少一个隔板分成两个或多个壳层空间; 每个分开的壳空间是独立的热控制的; 在第一步骤反应区的第一壳体空间或第二阶段反应区的第一壳体空间中的传热介质的温度范围从填充在对应于第一步骤的反应管的反应管中的催化剂层的最低活性温度当第二步反应区的第一阶段反应区的壳层空间或第二阶段反应区的第一壳空间为最低活性温度+ 20℃时，依次作为第一步反应区的第一壳空间，第一步反应区的第二壳空间，第一步反应区的第n个第二壳空间，和对应于第二步反应区的两个或多个壳层空间依次作为第二步反应区的第一壳空间，第二步反应区的第二壳空间，第二步反应区的壳层空间; 并且以这样的方式控制第一步骤反应区或第二阶段反应区的第一壳层空间的第一壳层空间，使得第一壳空间提供如式1或2中定义的每个长度的反应物转化贡献 1.2〜2.5。

10. 发明申请

WO2006098601A1 METHOD OF PRODUCING UNSATURATED ACID FROM OLEFIN 审中-公开
标题翻译：从烯烃生产不饱和酸的方法
公开(公告)号：WO2006098601A1
公开(公告)日：2006-09-21
申请号：PCT/KR2006/000979
申请日：2006-03-17
申请人： LG CHEM, LTD.
发明人： WOO, Boo-Gon , KO, Jun-Seok , HA, Kyoung-Su , KANG, Seong-Pil , CHOI, Seok-Hwan , KIM, Young-Bae
IPC分类号： C07C51/16
CPC分类号： B01J8/067 , B01J2208/00212 , B01J2208/025 , C07C51/215 , C07C51/252 , C07C57/04
摘要： Disclosed is a shell-and-tube heat exchanger type reactor that can be used for a process of producing unsaturated acids from olefins via fixed-bed catalytic partial oxidation, which comprises at least one reaction tube, each including at least one first-step catalyst layer, in which olefins are oxidized by a first-step catalyst to mainly produce unsaturated aldehydes, and at least two second-step catalyst layers, in which the unsaturated aldehydes are oxidized by a second-step catalyst to produce unsaturated acids, wherein a first catalyst layer of the second-step catalyst layers, disposed right adjacent to the first-step catalyst layer, has an activity corresponding to 5∼ 30% of the activity of the catalyst layer having a highest activity among the second-step catalyst layers. A method of producing unsaturated acids from olefins by using the reactor is also disclosed.
摘要翻译：公开了一种壳管式热交换器型反应器，其可用于通过固定床催化部分氧化由烯烃生产不饱和酸的方法，其包括至少一个反应管，每个反应管包含至少一个第一步催化剂层，其中烯烃被第一步催化剂氧化以主要产生不饱和醛，以及至少两个第二阶段催化剂层，其中不饱和醛被第二步催化剂氧化以产生不饱和酸，其中第一与第一级催化剂层相邻设置的第二级催化剂层的催化剂层的活性相对于第二级催化剂层中具有最高活性的催化剂层的活性的5〜30％的活性。还公开了通过使用反应器由烯烃生产不饱和酸的方法。

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