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1. 发明申请

WO2005111187A1 FACILITY PARTS CLEANING SOLUTION FOR PROCESSING OF (METH)ACRYLIC ACID AND/OR (METH)ACRYLIC ESTERS AND CLEANING METHOD USING SAID CLEANING SOLUTION 审中-公开
标题翻译：用于加工（甲基）丙烯酸和/或（甲基）丙烯酸酯的清洁溶液的清洁溶液和使用清洁溶液的清洁方法
公开(公告)号：WO2005111187A1
公开(公告)日：2005-11-24
申请号：PCT/KR2005/001437
申请日：2005-05-17
申请人： LG CHEM, LTD. , CHOI, Seok-Hwan , KANG, Seong-Pil , HA, Kyoung-Su , KIM, Geon-Yong , WOO, Boo-Gon
发明人： CHOI, Seok-Hwan , KANG, Seong-Pil , HA, Kyoung-Su , KIM, Geon-Yong , WOO, Boo-Gon
IPC分类号： C11D7/06
CPC分类号： C11D7/06 , C11D7/32 , C11D7/3245 , C11D7/3263 , C11D11/0041 , F28G9/00
摘要： The present invention relates to a facility parts cleaning solution for the processing of (meth)acrylic acid and/or (meth)acrylic esters and a cleaning method using the cleaning solution. An aqueous cleaning composition comprising 5 to 50 wt% of at least one alkali metal hydroxide selected from the group consisting of sodium hydroxide and potassium hydroxide, 0.01 to 1 wt% of a water-soluble amino acid, 0.001 to 0.05 wt% of N.N'-methylene bisacrylamide, and 0.001 to 0.05 wt% of azobisisobutyronitrile is used to clean facility parts for manufacturing (meth)acrylic acid and/or (meth)acrylic esters in order to easily remove polymers and deposits.
摘要翻译：本发明涉及用于处理（甲基）丙烯酸和/或（甲基）丙烯酸酯的设备部件清洗液和使用该清洗溶液的清洗方法。含有5〜50重量％的选自氢氧化钠和氢氧化钾的至少一种碱金属氢氧化物，0.01〜1重量％的水溶性氨基酸，0.001〜0.05重量％的N， N'-亚甲基双丙烯酰胺和0.001〜0.05重量％的偶氮二异丁腈用于清洗用于制造（甲基）丙烯酸和/或（甲基）丙烯酸酯的设备部件，以便容易地除去聚合物和沉积物。

2. 发明申请

WO2005021149A1 METHOD OF PRODUCING UNSATURATED ALDEHYDE AND UNSATURATED ACID IN FIXED-BED CATALYTIC PARTIAL OXIDATION REACTOR WITH ENHANCED HEAT CONTROL SYSTEM 审中-公开
标题翻译：在固体床催化部分氧化反应器中生产不饱和醛和不饱和酸的方法，具有增强的热控制
公开(公告)号：WO2005021149A1
公开(公告)日：2005-03-10
申请号：PCT/KR2004/002193
申请日：2004-09-01
申请人： LG CHEM, LTD. , HA, Kyoung-Su , KIM, Geon-Yong , KANG, Seong-Pil , CHOI, Seok-Hwan , WOO, Boo-Gon
发明人： HA, Kyoung-Su , KIM, Geon-Yong , KANG, Seong-Pil , CHOI, Seok-Hwan , WOO, Boo-Gon
IPC分类号： B01J8/06
CPC分类号： C07C51/252 , C07C57/04
摘要： The present invention provides a process of producing unsaturated aldehydes and unsaturated acids from olefins by fixed-bed catalytic partial oxidation in a shell-and-tube heat exchanger-type reactor. In this process, the reactor comprises a first-step reaction zone of mainly producing the unsaturated aldehydes, a second-step reaction zone of mainly producing the unsaturated acids, or both the two zones. The first-step reaction zone is divided into two or more zones by a partition. Each of the divided shell spaces is filled with a heat transfer medium, and the heat transfer medium in each shell space is maintained at isothermal temperature or a temperature difference of 0-5 °C. The temperatures of the heat transfer media in each of the divided shell spaces are set to increase in the moving direction of reactants. In order to facilitate the removal of heat generation at a location where the partition is placed, a reaction inhibition layer is disposed in the first-step reaction zone. Also, in order to protect the catalyst layer from a highly exothermic reaction, the process is performed at a limited temperature difference between the temperature in a hot spot and the temperature of a molten salt. If the improved heat control system according to the present invention is used, the heat stability of the catalyst layer will be secured and the yields of intermediate and final products can be increased.
摘要翻译：本发明提供了一种在壳管式热交换器型反应器中通过固定床催化部分氧化从烯烃生产不饱和醛和不饱和酸的方法。在该方法中，反应器包括主要产生不饱和醛的第一步反应区，主要产生不饱和酸的第二步反应区或两个区。第一步反应区通过隔板分成两个或多个区域。每个分开的壳体空间填充有传热介质，并且每个壳体空间中的传热介质保持在等温温度或0-5℃的温差。在每个分开的壳体空间中的传热介质的温度被设定为在反应物的移动方向上增加。为了便于在放置隔板的位置除去发热，反应抑制层设置在第一步反应区中。此外，为了保护催化剂层免受高度放热反应，该过程在热点温度与熔融盐温度之间的有限温度差下进行。如果使用根据本发明的改进的热控制系统，则将确保催化剂层的热稳定性，并且可以提高中间产品和最终产品的产率。

3. 发明申请

WO2004007064A1 CATALYTIC OXIDATION REACTOR WITH ENHANCED HEAT EXCHANGING SYSTEM 审中-公开
标题翻译：具有增强热交换系统的催化氧化反应器
公开(公告)号：WO2004007064A1
公开(公告)日：2004-01-22
申请号：PCT/KR2002/002074
申请日：2002-11-08
申请人： LG CHEM, LTD. , HA, Kyoung-Su , KIM, Geon-Yong , KANG, Seong-Pil , WOO, Boo-Gon
发明人： HA, Kyoung-Su , KIM, Geon-Yong , KANG, Seong-Pil , WOO, Boo-Gon
IPC分类号： B01J8/06
CPC分类号： B01J19/0013 , B01J8/067 , B01J2208/00212 , B01J2208/00221 , B01J2208/00548 , B01J2219/00006 , B01J2219/0004
摘要： A heat exchange-type reactor includes a reaction chamber (1) having mounted therein a plurality of contact tubes (5) filled with a catalyst material; at least one shield plate (11) mounted within the reaction chamber to partition an inner space of the reaction chamber into at least two separate spaces (1d, 1e); a plurality of conduits (13, 15, 17, 19) having entrance (15a, 17a) and exit (13a, 17a) openings through which a heat transfer medium respectively enters and exits, and being mounted to an outer circumference of the reaction chamber (1) corresponding to the partitioned spaces (1d, 1e); and a heat exchange unit connected to the conduits (13, 15, 17, 19) to perform heat exchange of the heat transfer medium, in which the heat exchange unit includes a single heat exchanger that performs the exchange of heat of the heat transfer medium in accordance with the partitioned spaces.
摘要翻译：热交换型反应器包括：反应室（1），其安装有多个填充有催化剂材料的接触管（5）; 至少一个屏蔽板（11），其安装在所述反应室内以将所述反应室的内部空间分隔成至少两个分开的空间（1d，1e）; 具有入口（15a，17a）和出口（13a，17a）开口的多个管道（13,15,17,19），传热介质通过该开口分别进入和离开并安装到反应室的外周（1）对应于分隔空间（1d，1e）; 以及连接到导管（13,15,17,19）的热交换单元，以进行传热介质的热交换，其中，热交换单元包括单个热交换器，该热交换器执行传热介质的热交换按照分区空间。

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