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1. 发明申请

WO2008038856A1 METHOD AND APPARATUS FOR FABRICATION OF THIN FILM SUPERCONDUCTOR BY SPRAY PYROLYSIS CHEMICAL VAPOR DEPOSITION METHOD 审中-公开
标题翻译：通过喷雾热分解化学蒸气沉积法制备薄膜超导体的方法和装置
公开(公告)号：WO2008038856A1
公开(公告)日：2008-04-03
申请号：PCT/KR2006/005148
申请日：2006-12-01
申请人： KOREA POLYTECHNIC UNIVERSITY , HONG, Gye-Won , LEE, Hee-Gyoun , KIM, Ho-Jin
发明人： HONG, Gye-Won , LEE, Hee-Gyoun , KIM, Ho-Jin
IPC分类号： H01L21/205
CPC分类号： C30B29/22 , C23C4/123 , C23C8/02 , C30B25/02 , H01L39/2451
摘要： Disclosed herein is a method and apparatus for fabrication of a thin film superconductor. Specifically, provided is a method and apparatus for fabrication of a thin film superconductor using spray pyrolysis chemical vapor deposition, comprising dissolving an inorganometallic compound as a raw material in distilled water to prepare a precursor solution, spraying the resulting precursor solution in a state of fine droplets, and coating an epitaxial thin film on a substrate (such as a ceramic material, a nickel metal, a nickel alloy, stainless steel or the like) via a pyrolysis process. The method comprises dissolving an inorganometallic compound having a water-solubility in distilled water to prepare a precursor solution; processing the precursor solution into droplets having a size of several μm to several tens of μm and storing the droplets in a raw material storage; transferring the droplets in the storage to a main pipe via a pump and simultaneously supplying the droplets, in conjunction with carrier and reactant gases supplied by operation of a valve, to a nozzle; heating the droplets sprayed from the nozzle by an auxiliary heat source to evaporate the distilled water, thereby preparing fine-sized particles of the inorganometallic compound; elevating a temperature of a heater formed in a table, such that the resulting particles react with the reactant gas to form an oxide; uniformly forming a film of the oxide at opposite sides on a single crystal substrate having a certain texture provided to the table via conveyers, by a ∧ shaped stainless steel plate, thereby forming an oxide template having a certain texture on the upper part of the substrate, and sufficiently heating the single crystal substrate prepared by forming an oxide buffer layer on the resulting oxide template to form an oxide thin film; and subjecting the resulting oxide thin film to an oxygen heat-treatment to complete a thin film superconductor having superconducting properties. That is, the present invention provides a method for fabrication of a thin film superconductor made of REBa2Cu3O7-x (RE = a rare-earth element selected from the group consisting of Y, La, Nd, Sm, Eu, Gd, Tb, Dy, Ho, Er, Tm, Yb, Lu and any combination thereof), using a precursor solution prepared by dissolving an inexpensive inorganometallic compound in distilled water. Therefore, the present invention enables production of superconductors at a significantly lower cost, as compared to the use of a conventional expensive β-chelate compound, i.e., 2,2,6,6-tetramethyl-3,5-heptanedione (tmhd).
摘要翻译：本文公开了一种用于制造薄膜超导体的方法和装置。具体地，提供了使用喷雾热解化学气相沉积制造薄膜超导体的方法和装置，其包括将作为原料的无机金属化合物溶解在蒸馏水中以制备前体溶液，将所得前体溶液以精细状态并通过热解法在基底（例如陶瓷材料，镍金属，镍合金，不锈钢等）上涂覆外延薄膜。该方法包括将具有水溶性的无机金属化合物溶解在蒸馏水中以制备前体溶液; 将前体溶液处理成具有几μm至几十μm的液滴并将液滴储存在原料储存器中; 通过泵将存储器中的液滴转移到主管道，同时将液滴与通过操作阀供应的载体和反应物气体一起供应到喷嘴; 通过辅助热源加热从喷嘴喷射的液滴以蒸发蒸馏水，从而制备无机金属化合物的细小颗粒; 升高形成在台上的加热器的温度，使得所得到的颗粒与反应气体反应形成氧化物; 在具有通过输送机提供给桌子的具有特定纹理的单晶基板上的相对侧的氧化物膜均匀地形成，从而在基板的上部形成具有一定质地的氧化物模板，并且通过在所得到的氧化物模板上形成氧化物缓冲层而制备的单晶基板充分加热以形成氧化物薄膜; 并对所得氧化物薄膜进行氧热处理，以完成具有超导特性的薄膜超导体。也就是说，本发明提供一种制造由REBa2Cu3O7-x制成的薄膜超导体的方法（RE =选自Y，La，Nd，Sm，Eu，Gd，Tb，Dy的稀土元素，Ho，Er，Tm，Yb，Lu及其任意组合），使用通过将廉价无机金属化合物溶解在蒸馏水中制备的前体溶液。因此，与使用常规的昂贵的β-螯合化合物即2,2,6,6-四甲基-3,5-庚二酮（tmhd）相比，本发明能够以显着更低的成本生产超导体。

2. 发明申请

WO2006121299A2 METHOD FOR PREPARING ORGANOMETALLIC PRECURSOR SOLUTION, ORGANOMETALLIC PRECURSOR SOLUTION PREPARED BY THE METHOD, AND METHOD FOR PRODUCING OXIDE SUPERCONDUCTING THIN FILM BY METALORGANIC DEPOSITION USING THE ORGANOMETALLIC PRECURSOR SOLUTION 审中-公开
标题翻译：用于制备有机质前体溶液的方法，通过该方法制备的有机前体溶液以及使用有机前体溶液通过金属沉积生产氧化物超导薄膜的方法
公开(公告)号：WO2006121299A2
公开(公告)日：2006-11-16
申请号：PCT/KR2006/001771
申请日：2006-05-12
申请人： KOREA POLYTECHNIC UNIVERSITY , HONG, Gye-Won , LEE, Hee-Gyoun , KIM, Byeong-Joo
发明人： HONG, Gye-Won , LEE, Hee-Gyoun , KIM, Byeong-Joo
IPC分类号： H01B12/06 , C23C18/12 , C04B35/01 , C04B35/40 , C04B35/45
CPC分类号： C23C18/1279 , C23C18/1216 , H01L39/2425
摘要： Disclosed herein are a method for preparing an organometallic precursor solution, an organometallic precursor solution prepared by the method, and a method for producing an oxide superconducting thin film by metalorganic deposition using the organometallic precursor solution. The organometallic precursor solution is essential for the production of an oxide superconductor by metalorganic deposition. The organometallic precursor solution is applied to a substrate whose surface is textured (a ceramic single crystal substrate or a metal-ceramic composite substrate in which a textured ceramic thin film is formed on a metal substrate) to produce an oxide superconductor. According to the method for preparing the organometallic precursor solution, an organic solvent is used as a raw material other than trifluoroacetates, thereby enabling production of an oxide superconducting thin film with excellent superconductivity at reduced costs without being largely affected by the presence of moisture in air even during storage and processing, such as coating, in air.
摘要翻译：本文公开了一种制备有机金属前体溶液的方法，通过该方法制备的有机金属前驱体溶液和通过使用有机金属前体溶液的金属有机沉积来生产氧化物超导薄膜的方法。有机金属前体溶液是通过金属有机沉积生产氧化物超导体所必需的。将有机金属前驱体溶液施加到表面纹理化的基板（陶瓷单晶基板或金属基板上形成纹理陶瓷薄膜的金属 - 陶瓷复合基板）上以制造氧化物超导体。根据制备有机金属前体溶液的方法，使用有机溶剂作为除三氟乙酸盐以外的原料，从而能够以低成本制造具有优异的超导性的氧化物超导薄膜，而不受空气中的水分的大量影响即使在储存和加工过程中，例如在空气中涂覆。

3. 发明申请

WO2008044863A1 STRUCTURE OF PERSISTENT CURRENT SWITCH AND THAT OF CONTROL METHOD 审中-公开
标题翻译：不间断电流开关结构及其控制方法
公开(公告)号：WO2008044863A1
公开(公告)日：2008-04-17
申请号：PCT/KR2007/004931
申请日：2007-10-10
申请人： KOREA POLYTECHNIC UNIVERSITY , LEE, Hee-Gyoun , HONG, Gye-Won , CHOI, Kyeong Dal , LEE, Seung Wook
发明人： LEE, Hee-Gyoun , HONG, Gye-Won , CHOI, Kyeong Dal , LEE, Seung Wook
IPC分类号： H01H36/00
CPC分类号： H01L39/20
摘要： Disclosed is the structure of a persistent current switch and a control method for the same. In the switch structure, a portion of a superconducting wire to be used as a switch is formed with slits such that the flow of current is controlled by the switch, to facilitate a transition between the superconducting state and the normal state of the superconducting wire. The structure of the persistent current switch includes a first slit longitudinally extending from a first point on one end of a superconducting wire to a second point and from a third point to a fourth point, the second, third, and fourth points being arranged sequentially in a longitudinal line, and second and third slits provided at opposite sides of a region between the second point and the third point where no first slit exists, the second and third slits having a length longer than a distance between the second point and the third point. As a result of providing the switch with the slits to facilitate a transition between the superconducting state and the normal state of the superconducting wire by controlling the flow of current through the superconducting wire, the superconducting wire can be easily changed from the superconducting state to the normal state even by slight heat. Accordingly, in an actual use thereof, the superconducting wire can reduce thermal load to be applied to a cooling system and assure easy regulation in the position of the switch.
摘要翻译：公开了持续电流开关的结构及其控制方法。在开关结构中，用作开关的超导线的一部分由狭缝形成，使得电流的流动由开关控制，以促进超导状态和超导线的正常状态之间的转变。持续电流开关的结构包括从超导线的一端的第一点向第二点纵向延伸的第一狭缝，从第三点到第四点，第二，第三和第四点依次布置在纵向线，以及第二和第三狭缝，设置在第二点和第三点之间的区域的相对侧，其中没有第一狭缝，第二和第三狭缝的长度比第二点和第三点之间的距离长。作为通过控制通过超导线的电流的流动来为开关提供狭缝以促进超导线的超导状态和正常状态之间的转变的结果，超导线可以容易地从超导状态改变为正常状态甚至轻微加热。因此，在实际使用中，超导线材可以减少施加到冷却系统的热负荷，并且确保开关位置容易调节。

4. 发明申请

WO2007004787A3 SUPERCONDUCTIVE MAGNET FOR PERSISTENT CURRENT AND METHOD FOR MANUFACTURING THE SAME 审中-公开
公开(公告)号：WO2007004787A3
公开(公告)日：2007-01-11
申请号：PCT/KR2006/002017
申请日：2006-05-26
申请人： KOREA POLYTECHNIC UNIVERSITY , HONG, Gye-Won , LEE, Hee-Gyoun
发明人： HONG, Gye-Won , LEE, Hee-Gyoun
IPC分类号： H01F41/04 , H01F6/06
摘要： Disclosed are a superconductive magnet manufactured by winding a thin superconductive rod wire in a coil without joint for maintaining a persistent current mode, and a method for manufacturing the same. The method includes winding both ends of a superconductive rod wire (10) on a first bobbin (21) and a second bobbin (22) respectively; forming a first unit rod wire (10a) and a second unit rod wire (10b) by slitting the superconductive rod wire (10) i n the lengthwise direction; producing a pancake coil by winding the first and second unit rod wires (10a, 10b) on third bobbins (25) in one direction; and arranging the first and second unit rod wires (10a, 10b) such that magnetic fields (B, B') in t he same direction are generated from the pancake coil, by reversing one of the third bobbins (25) on which the first and second unit rod wires (10a, 10b) are wound.

5. 发明申请

WO2007004820A1 METHOD FOR PROVIDING METAL ORGANIC PRECURSOR SOLUTION AND OXIDE SUPERCONDUCTING FILM FABRICATED THEREOF 审中-公开
标题翻译：提供金属有机前驱体溶液的方法及其制备的氧化物超导膜
公开(公告)号：WO2007004820A1
公开(公告)日：2007-01-11
申请号：PCT/KR2006/002563
申请日：2006-06-30
申请人： KOREA INSTITUTE OF MACHINERY & MATERIALS , LEE, Hee-Gyoun , HONG, Gye-Won , YOO, Jai-Moo , KIM, Young-Kuk , KO, Jae-Woong , CHUNG, Kook-Chae
发明人： LEE, Hee-Gyoun , HONG, Gye-Won , YOO, Jai-Moo , KIM, Young-Kuk , KO, Jae-Woong , CHUNG, Kook-Chae
IPC分类号： H01L39/00
CPC分类号： H01L39/2425 , C23C18/1208 , C23C18/1216 , C23C18/1279 , C23C18/1283
摘要： The present invention relates to a method for preparing a metal-organic precursor solution and a method for fabricating an oxide superconducting thin film through metalorganic deposition using the solution, and more particularly to a method for preparing a precursor solution essential for a process for fabricating an oxide superconductor using a metalorganic deposition method, as well as a method for fabricating an epitaxial oxide superconducting thin film on a surface- textured substrate using said solution. The invention provides a method for preparing a metal-organic precursor solution capable of being used to make a superconducting thin film having excellent properties in a cost-effective manner, by making a coating solution using a trifluoroacetate organic solvent as a raw material, starting with a composition having a cationic composition ratio deviating from RE:Ba:Cu = 1 :2:3, and then performing fabrication steps such as coating, as well as a method for fabricating an oxide superconducting thin film using said precursor solution according to the metalorganic deposition method.
摘要翻译：本发明涉及一种制备金属 - 有机前体溶液的方法和通过使用该溶液的金属有机沉积来制造氧化物超导薄膜的方法，更具体地涉及一种制备用于制备使用金属有机沉积方法的氧化物超导体，以及使用所述溶液在表面织构化衬底上制造外延氧化物超导薄膜的方法。本发明提供一种制备金属有机前体溶液的方法，该方法能够以成本有效的方式制备具有优异性能的超导薄膜，通过以三氟乙酸酯有机溶剂为原料制备涂布溶液，以具有偏离RE:Ba:Cu = 1:2:3的阳离子组成比的组合物，然后进行诸如涂层的制造步骤，以及使用根据金属有机物的所述前体溶液制造氧化物超导薄膜的方法沉积法。

6. 发明申请

WO2006022860A2 A CHEMICAL VAPOR DEPOSITION (CVD) APPARATUS USABLE IN THE MANUFACTURE OF SUPERCONDUCTING CONDUCTORS 审中-公开
标题翻译：超导体导体制造中使用的化学气相沉积（CVD）装置
公开(公告)号：WO2006022860A2
公开(公告)日：2006-03-02
申请号：PCT/US2005/009561
申请日：2005-03-22
申请人： SUPERPOWER, INC. , LEE, Hee-Gyoun , SELVAMANICKAM, Venkat
发明人： LEE, Hee-Gyoun , SELVAMANICKAM, Venkat
IPC分类号： H01L39/24 , G01N27/407 , C23C16/54 , C23C16/40 , C23C16/455
CPC分类号： C23C16/45572 , C23C16/408 , C23C16/4481 , C23C16/4557 , C23C16/545 , H01L39/2441 , Y10S505/726 , Y10T29/49014
摘要： A chemical vapor deposition (CVD) apparatus including a reactor, at least one substrate heater, at least one precursor supply system, at least one precursor injector, and at least one precursor composition monitor. The precursor supply system includes at least one precursor source, at least one a delivery mechanism including at least one assist vehicle, at least one vaporizer for vaporizing a precursor provided by at least the at least one precursor source, and at least one vehicle for transporting at least the vaporized precursor from the precursor supply to the precursor injector of the CVD apparatus.
摘要翻译：一种化学气相沉积（CVD）装置，包括反应器，至少一个基板加热器，至少一个前体供应系统，至少一个前体喷射器和至少一个前体组合物监测器。前体供应系统包括至少一个前体源，至少一个输送机构，其包括至少一个辅助载体，至少一个用于蒸发由至少一个前体源提供的前体的蒸发器，以及至少一个用于输送的载体至少从前体供应物蒸发的前体至CVD设备的前体注入器。

7. 发明申请

WO2006004579A2 A CHEMICAL VAPOR DEPOSITION (CVD) APPARATUS USABLE IN THE MANUFACTURE OF SUPERCONDUCTING CONDUCTORS 审中-公开
标题翻译：超导体导体制造中使用的化学气相沉积（CVD）装置
公开(公告)号：WO2006004579A2
公开(公告)日：2006-01-12
申请号：PCT/US2005/009560
申请日：2005-03-22
申请人： SUPERPOWER, INC. , SELVAMANICKAM, Venkat , LEE, Hee-Gyoun
发明人： SELVAMANICKAM, Venkat , LEE, Hee-Gyoun
IPC分类号： C23C16/54 , C23C16/40 , C23C16/455
CPC分类号： C23C16/45565 , C23C16/408 , C23C16/455 , C23C16/45517 , C23C16/45591 , C23C16/545 , H01L39/2441 , Y10T29/49014
摘要： A chemical vapor deposition (CVD) apparatus usable in the manufacture of a superconducting conductor on an elongate substrate is disclosed. The CVD apparatus includes a reactor, at least one substrate heater, and at least one precursor injector having a longitudinal flow distributor. Optionally, the CVD apparatus may include one of a transverse lateral flow restrictor, a shield for protecting a low-temperature region of the substrate, and both.
摘要翻译：公开了可用于在细长衬底上制造超导导体的化学气相沉积（CVD）装置。 CVD装置包括反应器，至少一个基板加热器和至少一个具有纵向流分配器的前驱物喷射器。可选地，CVD装置可以包括横向横向限流器，用于保护衬底的低温区域的屏蔽件和两者。

8. 发明申请

WO2005007918A2 ION BEAM-ASSISTED HIGH-TEMPERATURE SUPERCONDUCTOR (HTS) DEPOSITION FOR THICK FILM TAPE 审中-公开
标题翻译：离子束辅助高温超导体（HTS）沉积厚膜胶带
公开(公告)号：WO2005007918A2
公开(公告)日：2005-01-27
申请号：PCT/US2004/016597
申请日：2004-05-25
申请人： SUPERPOWER, INC. , SELVAMANICKAM, Venkat , LEE, Hee-Gyoun
发明人： SELVAMANICKAM, Venkat , LEE, Hee-Gyoun
IPC分类号： C23C
CPC分类号： H01L39/2448 , C23C14/087 , C23C14/22 , C23C14/28 , C23C16/408 , C23C16/486 , H01L39/2441
摘要： An ion source impinging on the surface of the substrate to be coated is used to enhance a MOCVD, PVD or other process for the preparation of superconducting materials.
摘要翻译：用于照射待涂覆的基底表面上的离子源用于增强用于制备超导材料的MOCVD，PVD或其它方法。

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