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1. 发明授权

US08889888B2 Sulfonic acid salt and derivative thereof, photo-acid generator, and process for production of sulfonic acid salt 有权
标题翻译：磺酸盐及其衍生物，光酸发生剂，以及磺酸盐的制备方法
公开(公告)号：US08889888B2
公开(公告)日：2014-11-18
申请号：US13000643
申请日：2009-07-06
申请人： Masashi Nagamori , Masaki Fujiwara , Kazunori Mori , Satoru Narizuka
发明人： Masashi Nagamori , Masaki Fujiwara , Kazunori Mori , Satoru Narizuka
IPC分类号： C07D209/96 , C07C309/70 , C07C303/22 , C07D311/78 , C07D333/46 , G03F7/039 , C07C381/12 , C07D335/02 , C07C309/82 , G03F7/004 , C07C309/12 , C07C25/18 , C07D209/76
CPC分类号： C07C381/12 , C07C25/18 , C07C303/22 , C07C309/12 , C07C309/82 , C07C2603/74 , C07D209/76 , C07D311/78 , C07D333/46 , C07D335/02 , G03F7/0045 , G03F7/0046 , G03F7/0397
摘要： A fluorine-containing sulfonic acid salt or a compound having a fluorine-containing sulfonic acid group, either of which having a structure represented by the following general formula (1), is provided. Such a salt or compound can act as a suitable photo-acid generator, and can form a resist pattern having excellent sensitivity, resolution and mask-dependence. [In general formula (1), R represents a substituted or unsubstituted linear or branched monovalent hydrocarbon group having 1 to 30 carbon atoms, a substituted or unsubstituted monovalent hydrocarbon group having 3 to 30 carbon atoms and a cyclic or a partially cyclic structure, a substituted or unsubstituted aryl group having 6 to 30 carbon atoms, or a substituted or unsubstituted monovalent heterocyclic organic group having 4 to 30 carbon atoms.]
摘要翻译：提供含氟磺酸盐或具有含氟磺酸基的化合物，其具有由以下通式（1）表示的结构。这样的盐或化合物可以用作合适的光酸发生剂，并且可以形成具有优异的灵敏度，分辨率和掩模依赖性的抗蚀剂图案。 [通式（1）中，R表示取代或未取代的碳原子数1〜30的直链或支链一价烃基，取代或未取代的碳原子数3〜30的一价烃基和环状或部分环状结构，取代或未取代的碳原子数为6〜30的芳基，取代或未取代的碳原子数为4〜30的1价杂环有机基。

2. 发明申请

US20120184763A1 METHOD FOR PRODUCING PERFLUOROSULFONIC ACID HAVING ETHER STRUCTURE AND DERIVATIVE THEREOF, AND SURFACTANT CONTAINING FLUORINE-CONTAINING ETHER SULFONIC ACID COMPOUND AND DERIVATIVE THEREOF 审中-公开
标题翻译：生产具有其结构和衍生物的全氟代酸的方法，以及含有含氟的含硫磺酸化合物及其衍生物的表面活性剂
公开(公告)号：US20120184763A1
公开(公告)日：2012-07-19
申请号：US13498710
申请日：2010-09-29
申请人： Mitsuo Kurumaya , Tsunetoshi Honda , Kota Omori
发明人： Mitsuo Kurumaya , Tsunetoshi Honda , Kota Omori
IPC分类号： C07C303/28 , C07C303/02 , C25B3/08 , C07C309/68 , C07C309/10 , C07C303/22 , C07C309/82
CPC分类号： C07C303/22 , C07C303/02 , C07C303/28 , C07C303/32 , C07C303/44 , C25B3/08 , C07C309/82 , C07C309/10 , C07C309/68
摘要： In this method, RH2ORH1SO2F is added to hydrofluoric acid so as to form a thick solution (hydrogen bonded complex), and the solution is directly supplied to a liquid phase reaction system in which an F2 gas is used. Alternatively, RH2ORH1SO2Cl is added to hydrofluoric acid so as to be converted into RH1ORH2SO2F by discharging HCl, and the RH1ORH2SO2F is directly supplied to a liquid phase reaction system in which an F2 gas is used. Consequently, fluorination can be carried out safely and a compound having an objective structure can be produced at low cost without causing isomerization or the like.
摘要翻译：在该方法中，将RH2ORH1SO2F加入到氢氟酸中以形成稠溶液（氢键合复合物），并将溶液直接供给到使用F2气体的液相反应体系中。或者，将RH2ORH1SO2Cl加入氢氟酸中，通过排出HCl转化为RH1ORH2SO2F，将RH1ORH2SO2F直接供给到使用F2气体的液相反应体系中。因此，可以安全地进行氟化，可以以低成本制造具有目标结构的化合物，而不会引起异构化等。

3. 发明申请

US20050177001A1 Process for producing fluorinated fluorosulfonylalkyl vinyl ether 有权
标题翻译：制备氟化氟磺酰基烷基乙烯基醚的方法
公开(公告)号：US20050177001A1
公开(公告)日：2005-08-11
申请号：US10515338
申请日：2003-05-23
申请人： Akinari Sugiyama , Tatsuya Ohtsuka , Kazuyoshi Ichihara , Toshiya Mantani
发明人： Akinari Sugiyama , Tatsuya Ohtsuka , Kazuyoshi Ichihara , Toshiya Mantani
IPC分类号： C07C303/22 , C07C309/82 , C07C39/82
CPC分类号： C07C303/22 , C07C309/82
摘要： The present invention provides a process for producing a fluorinated fluorosulfonylalkyl vinyl ether represented by general formula (2): CF2=CFO(CF2CF(CF3)O)nCF2CF2SO2F (2) wherein n is an integer from 0 to 10, comprising fluorinating a perfluorovinylether sulfonate with SF4 and HF, the perfluorovinylether sulfonate being represented by general formula (1): CF2=CFO(CF2CF(CF3)O)nCF2CF2SO3M (1) wherein M is Ma or Mb1/2, provided that Ma is an alkali metal and Mb is an alkaline earth metal; and n is as defined above. According to the process of the invention, the fluorinated fluorosulfonylalkyl vinyl ether can be produced in high yield in an industrially advantageous manner.
摘要翻译：本发明提供一种制备由通式（2）表示的氟化氟磺酰基烷基乙烯基醚的方法：<？in-line-formula description =“In-line formula”end =“lead”？> CF 2 SUB> = CFO（CF 2 CF（CF 3 O）O）2 CF 2 CF 2 其中n为0至10的整数，包括：（1）（式中，n为0〜10的整数，氟化全氟乙烯基醚磺酸盐与SF 4和HF氟化，全氟乙烯基醚磺酸盐由通式（1）表示：<？in-line-formula description =“In-line Formulas”end =“lead”？ CF 2 CF 2 CF 2 CF 2 CF 2 CF 2 CF 2 CF 2 CF 2 CF 2 CF 2 CF 2 CF 2 CF 2 CF 2 CF 2 CF 2 CF 2 CF 3 （1）<？in-line-formula description =“In-line Formulas”end =“tail”？>其中M是 Ma或Mb <1/2>，条件是Ma是碱金属，Mb是碱土金属; 和n如上所定义。根据本发明的方法，氟化氟磺酰基烷基乙烯基醚可以以工业上有利的方式以高产率制备。

4. 发明授权

US4962282A Direct fluorination of fluoro-beta-sultones in order to produce the corresponding fluorooxy-fluorosulfonyl-fluoro-compounds 失效
标题翻译：直接氟化氟-β-磺内酯以产生相应的氟氧基 - 氟磺酰氟化合物
公开(公告)号：US4962282A
公开(公告)日：1990-10-09
申请号：US479518
申请日：1990-02-13
申请人： Antonio Marraccini , Gabriele Perego
发明人： Antonio Marraccini , Gabriele Perego
IPC分类号： B01J27/12 , C07B61/00 , C07C303/02 , C07C309/80 , C07C309/82
CPC分类号： C07C303/02
摘要： Preparation of fluorooxy-fluorosulfonyl-fluorocompounds by means of the direct fluorination with elemental fluorine of various .beta.-sultones according to the following reaction scheme: ##STR1## wherein R.sub.1 and R.sub.2, which can be either equal to, or different from, each other, represent a fluorine or chlorine atom, or an alkyl radical partially or totally halogenated with fluorine and/or chlorine.The reaction takes place in continuous in the presence of a fluorination catalyst, preferably constituted by an alkali-metal fluoride preferably supported on a metal material, at temperatures comprised within the range of from -30.degree. C. to +100.degree. C., and under the pressure comprised within the range of from 50 to 800 kPa; said catalyst is a fixed-bed catalyst, or is suspended in a reaction medium inert under the operating conditions.

5. 发明授权

US4835323A Hydroquinones 失效
标题翻译：氢醌类
公开(公告)号：US4835323A
公开(公告)日：1989-05-30
申请号：US906111
申请日：1986-09-11
申请人： Frederick H. Howell
发明人： Frederick H. Howell
IPC分类号： C07C69/007 , C07C27/00 , C07C37/11 , C07C37/14 , C07C39/11 , C07C41/00 , C07C43/178 , C07C51/00 , C07C51/347 , C07C59/11 , C07C59/48 , C07C67/00 , C07C67/30 , C07C69/612 , C07C69/66 , C07C213/00 , C07C215/48 , C07C231/00 , C07C231/12 , C07C233/18 , C07C235/34 , C07C253/00 , C07C255/36 , C07C301/00 , C07C303/22 , C07C303/26 , C07C303/36 , C07C309/24 , C07C309/82 , C07D307/06 , C07D307/12 , C07D307/42 , C07D307/46 , C07D309/12 , C07F9/32 , C07F9/38 , C07F9/40 , G03C1/34 , G03C7/392
CPC分类号： G03C7/39216 , C07C37/14 , C07C39/11 , C07C43/1783 , C07C67/293 , C07C67/347 , C07D309/12 , C07F9/4006 , C07F9/4056 , C07C2101/14
摘要： New hydroquinones have the formula: ##STR1## wherein p is 1 or 2 and q is 0 or 1, provided that p+q is 1 or 2; R is a residue of formula: ##STR2## wherein Q is (i) -OX or (ii) -PO(OR.sub.11)((O).sub.x R.sub.11); and salts thereof with organic or inorganic acid bases.The groups X and R.sub.11 and x are defined hereinafter.The compounds of formula I are useful as stabilisers in photographic materials.
摘要翻译：新的氢醌具有下式：其中p为1或2，q为0或1，条件是p + q为1或2; R是下式的残基：其中Q是（i）-OX或（ii）-PO（OR11）（（O）xR11）; 及其盐与有机或无机酸碱。基团X和R 11和x在下文中定义。式I的化合物可用作照相材料中的稳定剂。

6. 发明授权

US4801409A Hypofluorites and bis-hypofluorites, and process for preparing same 失效
标题翻译：次氟酸亚铁和二 - 次氟化物，及其制备方法
公开(公告)号：US4801409A
公开(公告)日：1989-01-31
申请号：US93700
申请日：1987-09-08
申请人： Antonio Marraccini , Giorgio Guglielmo , Alessandro Malacrida , Lamberto Roberti
发明人： Antonio Marraccini , Giorgio Guglielmo , Alessandro Malacrida , Lamberto Roberti
IPC分类号： B01J27/12 , B01J27/00 , C07B61/00 , C07C20060101 , C07C67/00 , C07C71/00 , C07C201/00 , C07C301/00 , C07C303/22 , C07C309/78 , C07C309/80 , C07C309/82 , C07C143/70
CPC分类号： C07C71/00 , C07C309/00
摘要： Mono- and bis-hypofluorites respectively of formula: FO.sub.2 S--R.sub.f --CF.sub.2 OF and FOCF.sub.2 --R'.sub.f --CF.sub.2 OF wherein R.sub.f is perfluoroalkylene or perfluorochloroalkylene and R'.sub.f is a perfluoroalkylene or perfluorooxyalkylene, and process for preparing them, which is conducted continuously, at a temperature from 0.degree. to 60.degree. C. and comprises starting from the respective acyl fluorides ##STR1## by reaction of fluorine in the gas phase in the presence of a catalyst consisting of K, Rb, Cs or Ba fluoride, preferably supported on a metal material.
摘要翻译：分子式为：FO2S-Rf-CF2OF和FOCF2-R'f-CF2OF的单 - 和二 - 次氟化物，其中Rf是全氟亚烷基或全氟氯亚烷基，R'f是全氟亚烷基或全氟代亚烷基，以及其连续进行的制备方法，在0℃至60℃的温度下进行，并且包括由相应的酰基氟化物通过氟在气相中在由K，Rb，Cs或Ba氟化物组成的催化剂存在下反应而优选地载于一种金属材料。

7. 发明授权

US4358412A Preparation of vinyl ethers 失效
标题翻译：乙烯基醚的制备
公开(公告)号：US4358412A
公开(公告)日：1982-11-09
申请号：US158427
申请日：1980-06-11
申请人： Bobby R. Ezzell , William P. Carl , William A. Mod
发明人： Bobby R. Ezzell , William P. Carl , William A. Mod
IPC分类号： C07C69/708 , B01J27/232 , C07B61/00 , C07C41/24 , C07C43/17 , C07C51/00 , C07C51/38 , C07C59/135 , C07C67/00 , C07C67/32 , C07C69/734 , C07C309/10 , C07C309/65 , C07C309/68 , C07C309/80 , C07C309/82 , C07F9/40 , C07F9/113 , C07C69/73 , C07C143/70
CPC分类号： C07C309/00 , C07F9/4006
摘要： The invention relates to a process to produce compounds represented by the general formulaY--(CFR.sub.f).sub.a --(CFR.sub.f ').sub.b --O--CF.dbd.CF.sub.2by decarboxylation of compounds represented by the general formula ##STR1## where a=0-3; b=0-3;provided a+b=2 or 3;Y.dbd.an acid derivative;X.dbd.Cl, I, or Br;M.dbd.OR, F, Cl, Br, I, OA;A.dbd.alkali metal, alkali earth metal, a quaternary nitrogen and hydrogen;R.sub.f ' and R.sub.f are independently selected from the group consisting of F, Cl, perfluoroalkyls and fluorochloroalkylsR.dbd.an alkyl having one or more carbon atoms or an aryl.
摘要翻译：本发明涉及通过通式（I）= 0-3表示的化合物的脱羧反应生成由通式Y-（CFRf）a-（CFRf'）b-O-CF = CF2表示的化合物的方法。 b = 0-3; 提供+ b = 2或3; Y =酸衍生物; X = Cl，I或Br; M = OR，F，Cl，Br，I，OA; A =碱金属，碱土金属，季氮和氢; Rf'和Rf独立地选自F，Cl，全氟烷基和氟氯烷基R =具有一个或多个碳原子的烷基或芳基。

8. 发明授权

US4329434A Novel fluorinated cation exchange membrane and process for producing the same 失效
标题翻译：新型氟化阳离子交换膜及其制备方法
公开(公告)号：US4329434A
公开(公告)日：1982-05-11
申请号：US152847
申请日：1980-05-23
申请人： Kyoji Kimoto , Hirotsugu Miyauchi , Jukichi Ohmura , Mikio Ebisawa , Toshioki Hane
发明人： Kyoji Kimoto , Hirotsugu Miyauchi , Jukichi Ohmura , Mikio Ebisawa , Toshioki Hane
IPC分类号： C07C309/82 , C07C309/84 , C07C317/18 , C07C323/12 , C07D327/04 , C08F8/04 , C08F8/12 , C08F214/18 , C08F214/26 , C08F216/14 , C08J5/22 , B01J39/00
CPC分类号： C07D327/04 , C07C309/82 , C07C309/84 , C07C317/18 , C07C323/12 , C08F214/184 , C08F214/262 , C08F216/1466 , C08F8/04 , C08F8/12 , C08J5/2237 , C08J2327/12
摘要： A novel fluorinated cation exchange membrane containing carboxylic acid groups and sulfonic acid groups, both in the form of a specific pendant structure, the carboxylic acid groups being at least 20% on one surface of the membrane and gradually decreasing toward the innerside of the membrane, which membrane is useful in electrolysis of an aqueous alkali metal halide solution with advantageously stable performance for a long term under more severe operational conditions than those conventionally used. The membrane can be prepared from a novel copolymer of a fluorinated olefin with a novel sulfur containing fluorinated vinylether of the formula: ##STR1## wherein k is 0 or 1, l is an integer of 3 to 5, Z is --S-- or --SO.sub.2 -- and R is C.sub.1 -C.sub.10 alkyl, an aryl, Cl or C.sub.1 -C.sub.10 perfluoroalkyl.
摘要翻译：一种含有羧酸基团和磺酸基团的新颖的氟化阳离子交换膜，两者都是特定侧挂结构的形式，羧酸基团在膜的一个表面上至少为20％，并逐渐朝向膜的内层减少，所述膜可用于电解碱金属卤化物水溶液，其在比常规使用的操作条件更严格的操作条件下长期具有稳定的性能。膜可以由氟化烯烃与新型含硫氟化乙烯基醚的新型共聚物制备，其具有下式：其中k为0或1，l为3至5的整数，Z为-S-或 - SO2-和R是C1-C10烷基，芳基，C1或C1-C10全氟烷基。

9. 发明授权

US09153836B2 Electrolytic solutions and battery 有权
标题翻译：电解液和电池
公开(公告)号：US09153836B2
公开(公告)日：2015-10-06
申请号：US12183153
申请日：2008-07-31
申请人： Masayuki Ihara , Hiroyuki Yamaguchi , Tadahiko Kubota
发明人： Masayuki Ihara , Hiroyuki Yamaguchi , Tadahiko Kubota
IPC分类号： H01M10/0569 , H01M10/052 , C07C309/80 , C07C309/81 , C07C309/82 , C07C309/86 , H01M10/0567 , H01M10/0568
CPC分类号： H01M10/0569 , C07C309/80 , C07C309/81 , C07C309/82 , C07C309/86 , H01M10/052 , H01M10/0567 , H01M10/0568 , H01M2300/0034 , Y02E60/122
摘要： A battery capable of improving battery characteristics is provided. The battery includes a cathode, an anode and an electrolytic solution, and a separator arranged between the cathode and the anode is impregnated with the electrolytic solution. The solvent of the electrolytic solution includes a sulfone compound having a sulfonyl fluoride type structure in which a sulfonyl group and a fluorine group are bonded together, and at least one kind selected from the group consisting of a chain carbonate which includes a halogen and a cyclic carbonate which includes a halogen.
摘要翻译：提供了能够改善电池特性的电池。电池包括阴极，阳极和电解液，并且设置在阴极和阳极之间的隔膜被电解液浸渍。电解液的溶剂包括具有磺酰基和氟基结合在一起的磺酰氟型结构的砜化合物，以及选自包括卤素和环状的链状碳酸酯的至少一种包括卤素的碳酸酯。

10. 发明授权

US5530066A Monomers derived from perhalogenated sultones and polymers obtained from these monomers 失效
标题翻译：衍生自全卤代磺内酯的单体和从这些单体获得的聚合物
公开(公告)号：US5530066A
公开(公告)日：1996-06-25
申请号：US433014
申请日：1995-05-03
申请人： Michel Armand , Jean-Yves Sanchez , Salime Sylla
发明人： Michel Armand , Jean-Yves Sanchez , Salime Sylla
IPC分类号： C07C309/07 , C07C309/09 , C07C309/10 , C07C309/17 , C07C309/82 , C07C309/84 , C07C311/02 , C07D303/22 , C07F7/08 , C07F7/18 , C08G65/14 , C08G65/22 , C08G65/32 , C08G65/334 , C08G65/337 , C08G79/02 , H01B1/12 , H01M6/18 , H01M8/10 , H01M10/052 , H01M10/0565 , C08G75/00 , C07C303/08 , C08J5/20
CPC分类号： H01M10/052 , C07C309/07 , C07C309/09 , C07C309/17 , C07C309/82 , C07C309/84 , C07F7/0834 , C07F7/1836 , C08G65/14 , C08G65/22 , C08G65/226 , C08G65/3346 , C08G65/337 , C08G79/02 , H01B1/122 , H01M10/0565 , H01M6/181 , H01M8/1027 , H01M8/103 , H01M8/1032 , H01M8/1039 , H01M8/1072 , Y02P70/56
摘要： The invention relates to monomers derived from perhalogenated sultones, to a process for their preparation, to the polymers obtained from the said monomers and to their use for the production of ion-conductive materials.The monomers are compounds corresponding to the formula A--CFX--SO.sub.2 Z in which A denotes one group R.sup.3 --O--CF.sub.2 -- or R.sup.3 -- or R.sup.1 R.sup.2 N--CO--; Z denotes F, Cl, --OSi(CH.sub.3).sub.3 or an ionic group, Z being other than F when A denotes R.sup.3 --O--CF.sub.2 -- or R.sup.3 --; X denotes F, Cl, H or R.sub.F, X being R.sub.F when A denotes R.sup.3 --; the radicals R.sup.1, R.sup.2 and R.sup.3 are chosen from polymerizable nonperfluorinated organic radicals; R.sub.F is chosen from perfluoroalkyl radicals and perfluoroaryl radicals.The polymers obtained from these monomers can be employed for the production of ion-conductive materials.
摘要翻译：本发明涉及衍生自全卤代磺内酯的单体，其制备方法，从所述单体获得的聚合物及其用于生产离子导电材料的用途。单体是对应于式A-CFX-SO 2 Z的化合物，其中A表示一个R 3 -O-CF 2 - 或R 3 - 或R 1 R 2 N-CO-; Z表示F，Cl，-OSi（CH3）3或离子基团，当A表示R3-O-CF2-或R3-时，Z不同于F; X表示F，Cl，H或RF，X表示当A表示R3-时为RF; 基团R1，R2和R3选自可聚合的非全氟化有机基团; RF选自全氟烷基和全氟芳基。从这些单体获得的聚合物可用于制造离子传导材料。

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